Effect of Cold Rotary-Swaging Deformation on Microstructure and Tensile Properties of TB9 Titanium Alloy

doi:10.11900/0412.1961.2018.00241

Acta Metall Sin

2019, Vol. 55

Issue (4): 480-488 DOI: 10.11900/0412.1961.2018.00241

Current Issue | Archive | Adv Search

Effect of Cold Rotary-Swaging Deformation on Microstructure and Tensile Properties of TB9 Titanium Alloy

Dechun REN^1,²,Huhu SU^1,²,Huibo ZHANG¹,Jian WANG¹,Wei JIN^1,²(

),Rui YANG^1,²

1. Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
2. School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China

Cite this article:

Dechun REN, Huhu SU, Huibo ZHANG, Jian WANG, Wei JIN, Rui YANG. Effect of Cold Rotary-Swaging Deformation on Microstructure and Tensile Properties of TB9 Titanium Alloy. Acta Metall Sin, 2019, 55(4): 480-488.

Download:

HTML

PDF(19419KB)
Export: BibTeX | EndNote (RIS)

Abstract

TB9 titanium alloy has been widely used for aerospace due to it's superior low stiffness, corrosion resistance and workability. It has been reported that cold deformation can improve the comprehensive mechanical properties of titanium alloys. At the same time, the cold rotary-swaging deformation facilitates the production of small batches and the acquisition of special shape and size bars. However, current studies on the microstructure and properties of cold rotary-swaged titanium alloys are not systematic. So, the effects of cold deformation rate on the microstructure, texture evolution and mechanical property of TB9 alloy during cold rotary-swaging were investigated using OM, EBSD, XRD, TEM and tensile test. The results showed that the grain size of TB9 titanium was refined with the increase in diameter reduction. Meanwhile, with the deformation increases, the grains rotation along the swaging axis occurs, forming a preferred orientation, the textures change from initial {001}<110> and {001}<100> to α-fiber and γ-fiber {001}<110>, {112}<110> and {111}<110>. All of grains refinement, texture components and substructures contributed to the enhancement of strength after cold rotary-swaging. And the ductile kept on a high level after 70% cold working, which means the TB9 titanium has a great cold deformation ability.

Key words: TB9 titanium alloy cold rotary-swaging deformation microstructure texture tensile property

Received: 15 March 2018

ZTFLH:

TG146.2

	Service

	E-mail this article
	Add to citation manager
	E-mail Alert
	RSS
	（）
	Articles by authors
	Dechun REN
	Huhu SU
	Huibo ZHANG
	Jian WANG
	Wei JIN
	Rui YANG

URL:

https://www.ams.org.cn/EN/10.11900/0412.1961.2018.00241 OR https://www.ams.org.cn/EN/Y2019/V55/I4/480

Fig.1 OM image (a), TEM image and SAED pattern (b) and EBSD analyses (c~e) of the solution microstructure of TB9 titanium alloy (The red lines and green lines in Fig.1e indicate high-angle grain boundaries (HAGBs) with misorientation angles of over 15o and low-angle grain boundaries (LAGBs) with misorientation angles of 2o~15o, respectively. RD—rolling direction)

Fig.2

Fig.3 OM images (a~c) and EBSD analyses (d~f) of TB9 titanium alloy under cold rotary-swaging rates of 15% (a, d), 35% (b, e) and 70% (c, f) (RS—rotary-swaging direction)

Fig.4

Fig.5 TEM images of TB9 titanium alloy under cold rotary-swaging rates of 15% (a), 35% (b), 70% (c), and SAED pattern of bright band under 70% cold rotary-swaging rate (d) (Inset in Fig.5c show the SAED pattern of dark band)

Fig.6 EBSD contrast band map showing sheer bands of TB9 titanium alloy under cold rotary-swaging rate of 70% (a) and distribution of misorientation along the arrow in Fig.6a (b)

Fig.7 Pole figures of TB9 titanium alloy under cold rotary-swaging rates of 15% (a), 35% (b) and 70% (c)

Fig.8 Sections (φ₂=45o) of orientation distribution functions (ODFs) of solution treated TB9 titanium alloy (a) and under cold rotary-swaging rates of 10% (b), 30% (c) and 40% (d)

Fig.9

Table 1 Room temperature tensile properties of TB9 titanium alloy under different cold rotary-swaging rates

Fig.10 Distributions of grain size of TB9 titanium alloy under cold rotary-swaging rates of 10% (a), 35% (b) and 70% (c) with critical orientation angle 2o

1	Huang X, Cuddy J, Goel N, et al. Effect of heat treatment on the microstructure of a metastable β-titanium alloy [J]. J. Mater. Eng. Perform., 1994, 3: 560
2	Tian Y X, Li S J, Hao Y L, et al. High temperature deformation behavior and microstructure evolution mechanism transformation in Ti2448 alloy [J]. Acta Metall. Sin., 2012, 48: 837
2	田宇兴, 李述军, 郝玉琳等. Ti2448合金高温变形行为及组织演变机制的转变 [J]. 金属学报, 2012, 48: 837
3	Boyer R R, Brigge R D. The use of β titanium alloys in the aerospace industry [J]. J. Mater. Eng. Perform., 2005, 14: 681
4	Huang L J, Wang J, Zhang H B, et al. Effects of cold drawing deformation and aging temperature on microstructure and mechanical properties of TB9 titanium alloy [J]. Chin. J. Nonferrous Met., 2013, 23(Special 1): s11
4	黄鎏杰, 王健, 张慧博等. 冷拉拔变形量和时效温度对TB9钛合金丝材组织和性能的影响 [J]. 中国有色金属学报, 2013, 23(专辑1): s11)
5	Xu X, Dong L M, Ba H B, et al. Hot deformation behavior and microstructural evolution of beta C titanium alloy in β phase field [J]. Trans. Nonferrous Met. Soc. China, 2016, 26: 2874
6	Rack H J. Plastic deformation of unaged RMI 38644 [J]. Scr. Mater., 1976, 10: 739
7	Banumathy S, Mandal R K, Singh A K. Texture and anisotropy of hot rolled Ti-16Nb alloy [J]. J. Alloys Compd., 2010, 500: L26
8	Dai S J, Wang Y, Chen F, et al. Effect of cold deformation on microstructure and mechanical properties of Ti-35Nb-9Zr-6Mo-4Sn alloy for biomedical applications [J]. Mater. Sci. Eng., 2013, A575: 35
9	Zhang Z Q, Dong L M, Guan S X, et al. Microstructure and mechanical properties of TC16 titanium alloy by room temperature roller die drawing [J]. Acta Metall. Sin., 2017, 53: 415
9	张志强, 董利民, 关少轩等. TC16钛合金辊模拉丝过程中的显微组织和力学性能 [J].金属学报, 2017, 53: 415
10	Fang S M, Lei T, Zhang Y L, et al. Application study on swaging special-shaped non-ferrous metal wire of lower plasticity [J]. Forg. Stamp. Technol., 2007, 32(5): 69
10	方树铭, 雷霆, 张玉林等. 旋锻法加工低塑性有色金属异型材的应用研究 [J]. 锻压技术, 2007, 32(5): 69)
11	Zheng B Z, Tang X X, Tian X L, et al. Treatment methods on relative motion between clamp and hammer in numerical simulation of rotary forging for titanium alloy wire [J]. Forg. Stamp. Technol., 2017, 42(10): 195
11	郑帮智, 唐新新, 田晓琳等. 钛合金线材旋锻数值仿真中夹具与锤头相对运动的处理方法 [J]. 锻压技术, 2017, 42(10): 195)
12	Guo W Y, Xing H, Sun J. EBSD and TEM studies of deformation structure of metastable β-type titanium alloy after cold-swaging [J]. J. Chin. Electron Micros. Soc., 2008, 27: 469
12	郭文渊, 邢辉, 孙坚. 亚稳态β钛合金冷旋锻形变组织的EBSD和TEM研究 [J]. 电子显微学报, 2008, 27: 469
13	Pachla W, Kulczyk M, Przybysz S, et al. Effect of severe plastic deformation realized by hydrostatic extrusion and rotary swaging on the properties of CP Ti grade 2 [J]. J. Mater. Process.Technol., 2015, 221: 255
14	Alkhazraji H, El-Danaf E, Wollmann M, et al. Enhanced fatigue strength of commercially pure Ti processed by rotary swaging [J]. Adv. Mater. Sci. Eng., 2015, 2015: 301837
15	Wang H F, Han J T, Hao Q L. Influence of mandrel on the performance of titanium tube with cold rotary swaging [J]. Mater. Manuf. Processes, 2015, 30: 1251
16	Ide N, Morita T, Takahashi K, et al. Influence of cold rolling on fundamental properties of Ti-15V-3Cr-3Sn-3Al alloy [J]. Mater. Trans., 2015, 56: 1800
17	Sun J F, Zhang Z W, Zhang M L, et al. Microstructure evolution and their effects on the mechanical properties of TB8 titanium alloy [J]. J. Alloys Compd., 2016, 663: 769
18	Chung C C, Wang S W, Chen Y C, et al. Effect of cold rolling on structure and tensile properties of cast Ti-7.5Mo alloy [J]. Mater. Sci. Eng., 2015, A631: 52
19	Cai S, Bailey D M, Kay L E. Effect of annealing and cold work on mechanical properties of beta III titanium [J]. J. Mater. Eng. Perform., 2012, 21: 2559
20	Xu T W, Li J S, Zhang S S, et al. Cold deformation behavior of the Ti-15Mo-3Al-2.7Nb-0.2Si alloy and its effect on α precipitation and tensile properties in aging treatment [J]. J. Alloys Compd., 2016, 682: 404
21	Wu X, Tao N, Hong Y, et al. Microstructure and evolution of mechanically-induced ultrafine grain in surface layer of Al-alloy subjected to USSP [J]. Acta Mater., 2002, 50: 2075
22	Zhao H L, Ni S, Song M, et al. Grain refinement via formation and subdivision of microbands and thin laths structures in cold-rolled hafnium [J]. Mater. Sci. Eng., 2015, A645: 328
23	Engler O, Tomé C N, Huh M Y. A study of through-thickness texture gradients in rolled sheets [J]. Metall. Mater. Trans., 2000, 31A: 2299
24	Miyamoto H, Xiao T, Uenoya T, et al. Effect of simple shear deformation prior to cold rolling on texture and ridging of 16% Cr ferritic stainless steel sheets [J]. ISIJ Int., 2010, 50: 1653
25	Ray R K, Jonas J J, Hook R E. Cold rolling and annealing textures in low carbon and extra low carbon steels [J]. Int. Mater. Rev.,1994, 39: 129
26	Conrad H. Effect of interstitial solutes on the strength and ductility of titanium [J]. Prog. Mater. Sci., 1981, 26: 123
27	Zhang Y W, Li S J, Obbard E G, et al. Elastic properties of Ti-24Nb-4Zr-8Sn single crystals with bcc crystal structure [J]. Acta Mater., 2011, 59: 3081
28	Fang T H, Li W L, Tao N R, et al. Revealing extraordinary intrinsic tensile plasticity in gradient nano-grained copper [J]. Science, 2011, 331: 1587

[1]	GONG Shengkai, LIU Yuan, GENG Lilun, RU Yi, ZHAO Wenyue, PEI Yanling, LI Shusuo. Advances in the Regulation and Interfacial Behavior of Coatings/Superalloys[J]. 金属学报, 2023, 59(9): 1097-1108.
[2]	ZHANG Leilei, CHEN Jingyang, TANG Xin, XIAO Chengbo, ZHANG Mingjun, YANG Qing. Evolution of Microstructures and Mechanical Properties of K439B Superalloy During Long-Term Aging at 800^oC[J]. 金属学报, 2023, 59(9): 1253-1264.
[3]	LU Nannan, GUO Yimo, YANG Shulin, LIANG Jingjing, ZHOU Yizhou, SUN Xiaofeng, LI Jinguo. Formation Mechanisms of Hot Cracks in Laser Additive Repairing Single Crystal Superalloys[J]. 金属学报, 2023, 59(9): 1243-1252.
[4]	WANG Lei, LIU Mengya, LIU Yang, SONG Xiu, MENG Fanqiang. Research Progress on Surface Impact Strengthening Mechanisms and Application of Nickel-Based Superalloys[J]. 金属学报, 2023, 59(9): 1173-1189.
[5]	LIU Xingjun, WEI Zhenbang, LU Yong, HAN Jiajia, SHI Rongpei, WANG Cuiping. Progress on the Diffusion Kinetics of Novel Co-based and Nb-Si-based Superalloys[J]. 金属学报, 2023, 59(8): 969-985.
[6]	CHANG Songtao, ZHANG Fang, SHA Yuhui, ZUO Liang. Recrystallization Texture Competition Mediated by Segregation Element in Body-Centered Cubic Metals[J]. 金属学报, 2023, 59(8): 1065-1074.
[7]	LI Jingren, XIE Dongsheng, ZHANG Dongdong, XIE Hongbo, PAN Hucheng, REN Yuping, QIN Gaowu. Microstructure Evolution Mechanism of New Low-Alloyed High-Strength Mg-0.2Ce-0.2Ca Alloy During Extrusion[J]. 金属学报, 2023, 59(8): 1087-1096.
[8]	CHEN Liqing, LI Xing, ZHAO Yang, WANG Shuai, FENG Yang. Overview of Research and Development of High-Manganese Damping Steel with Integrated Structure and Function[J]. 金属学报, 2023, 59(8): 1015-1026.
[9]	SUN Rongrong, YAO Meiyi, WANG Haoyu, ZHANG Wenhuai, HU Lijuan, QIU Yunlong, LIN Xiaodong, XIE Yaoping, YANG Jian, DONG Jianxin, CHENG Guoguang. High-Temperature Steam Oxidation Behavior of Fe22Cr5Al3Mo-xY Alloy Under Simulated LOCA Condition[J]. 金属学报, 2023, 59(7): 915-925.
[10]	ZHANG Deyin, HAO Xu, JIA Baorui, WU Haoyang, QIN Mingli, QU Xuanhui. Effects of Y₂O₃ Content on Properties of Fe-Y₂O₃ Nanocomposite Powders Synthesized by a Combustion-Based Route[J]. 金属学报, 2023, 59(6): 757-766.
[11]	GUO Fu, DU Yihui, JI Xiaoliang, WANG Yishu. Recent Progress on Thermo-Mechanical Reliability of Sn-Based Alloys and Composite Solder for Microelectronic Interconnection[J]. 金属学报, 2023, 59(6): 744-756.
[12]	WU Dongjiang, LIU Dehua, ZHANG Ziao, ZHANG Yilun, NIU Fangyong, MA Guangyi. Microstructure and Mechanical Properties of 2024 Aluminum Alloy Prepared by Wire Arc Additive Manufacturing[J]. 金属学报, 2023, 59(6): 767-776.
[13]	FENG Aihan, CHEN Qiang, WANG Jian, WANG Hao, QU Shoujiang, CHEN Daolun. Thermal Stability of Microstructures in Low-Density Ti₂AlNb-Based Alloy Hot Rolled Plate[J]. 金属学报, 2023, 59(6): 777-786.
[14]	WANG Fa, JIANG He, DONG Jianxin. Evolution Behavior of Complex Precipitation Phases in Highly Alloyed GH4151 Superalloy[J]. 金属学报, 2023, 59(6): 787-796.
[15]	ZHANG Dongyang, ZHANG Jun, LI Shujun, REN Dechun, MA Yingjie, YANG Rui. Effect of Heat Treatment on Mechanical Properties of Porous Ti55531 Alloy Prepared by Selective Laser Melting[J]. 金属学报, 2023, 59(5): 647-656.

No Suggested Reading articles found!

Viewed

Full text

Abstract

Cited

Shared

Discussed