Effect of Shot Peening of Substrate Surface on Cyclic Oxidation Behavior of Sputtered Nanocrystalline Coating

doi:10.11900/0412.1961.2022.00183

Acta Metall Sin

2023, Vol. 59

Issue (5): 668-678 DOI: 10.11900/0412.1961.2022.00183

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Effect of Shot Peening of Substrate Surface on Cyclic Oxidation Behavior of Sputtered Nanocrystalline Coating

HUANG Ding¹, QIAO Yanxin¹(

), YANG Lanlan¹, WANG Jinlong², CHEN Minghui², ZHU Shenglong³, WANG Fuhui²

¹School of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang 212003, China
²Shenyang National Key Laboratory for Materials Science, Northeastern University, Shenyang 110819, China
³Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

Cite this article:

HUANG Ding, QIAO Yanxin, YANG Lanlan, WANG Jinlong, CHEN Minghui, ZHU Shenglong, WANG Fuhui. Effect of Shot Peening of Substrate Surface on Cyclic Oxidation Behavior of Sputtered Nanocrystalline Coating. Acta Metall Sin, 2023, 59(5): 668-678.

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Abstract

In addition to changing the surface roughness of the superalloy, the substrate surface treatment can also modify the microstructure of the surface, which affects the high-temperature oxidation behavior of the high-temperature protective coating. However, there are few reports about the effect of superalloy surface treatment on the oxidation behavior of nanocrystalline coatings. In this work, nanocrystalline coatings were sputtered on the nickel-based single crystal superalloy after two different surface treatments of polishing and shot peening, and their cyclic oxidation behavior at 1100^oC was investigated. The phase composition and microstructure of nanocrystalline coatings were characterized by SEM, XRD, and EDS. The results indicated that the cyclic oxidation kinetics of both nanocrystalline coatings at 1100^oC were similar. A dense oxide film could be formed on the surface of nanocrystalline coatings, showing excellent oxidation resistance. However, the microstructure evolution of the interface between the nanocrystalline coating and shot-peened superalloy substrate differed from that between the nanocrystalline coating and polished superalloy substrate. The sustained formation of the γ′ phase in the nanocrystalline coating near the polished substrate/coating interface was observed during high-temperature oxidation. This phenomenon was not found at the nanocrystalline coating near the shot peened substrate/coating interface, while the continuous growth of the γ' phase was observed at the substrate.

Key words: shot peening nanocrystalline coating cyclic oxidation magnetron sputtering

Received: 19 April 2022

ZTFLH:

TG172

Fund: National Natural Science Foundation of China(51801021);National Natural Science Foundation of China(52001142);Ministry of Industry and Information Technology Project(MJ-2017-J-99);Fundamental Research Funds for the Central Universities(N2102015)

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	HUANG Ding
	QIAO Yanxin
	YANG Lanlan
	WANG Jinlong
	CHEN Minghui
	ZHU Shenglong
	WANG Fuhui

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https://www.ams.org.cn/EN/10.11900/0412.1961.2022.00183 OR https://www.ams.org.cn/EN/Y2023/V59/I5/668

Fig.1 Cross-sectional (a, c) and surface (b, d) morphologies of the as-sputtered nanocrystalline coatings deposited on the polished (a, b) and shot peened (c, d) N5 single crystal superalloys

Fig.2 Cyclic oxidation kinetics of nanocrystalline coatings at 1100^oC (a) and lg(ΔM)-lgt fitting cu-rves (b) (ΔM—mass gain per unit area, t—oxidation time)

Fig.3 XRD spectra of the nanocrystalline coatings after cycle oxidation with different cycles at 1100^oC

Fig.4 Cross-sectional (a, c) and surface (b, d) morphologies of nanocrystalline coatings deposited on polished (a, b) and shot peened (c, d) superalloys after 100 cyc at 1100^oC

Fig.5 Microstructures (left) and EDS line scanning results along the dash lines (right) of the interface between the polished substrate and nanocrystalline coating after 0 (a), 5 (b), 20 (c), and 100 (d) cyc oxidation at 1100^oC

Fig.6 Microstructures (left) and EDS line scanning results along the dash lines (right) of the interface between the shot peened substrate and nanocrystalline coating after 0 (a), 5 (b), 20 (c), and 100 (d) cyc oxidation at 1100^oC

Table 1 EDS results of points 1-4 in Figs.5d and 6d

Fig.7 Cross-sectional microstructures of nanocrystalline coatings deposited on polished (a, c) and shot peened (b, d) superalloys after 20 (a, b) and 100 (c, d) cyc at 1100^oC

Table 2 EDS results of Al element at points 1-8 in Fig.7

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