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Acta Metall Sin  2017, Vol. 53 Issue (2): 192-200    DOI: 10.11900/0412.1961.2016.00247
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Study on Grain Refinement Mechanism of Hypoeutectic Al-7%Si Alloy Under Low Voltage Alternating Current Pulse
Ning LI1,Rong ZHANG1,Limin ZHANG1,Hui XING1,Pengfei YIN2,Yaoyan WU1
1 Key Laboratory of Space Applied Physics and Chemistry, Ministry of Education, School of Science, Northwestern Polytechnical University, Xi'an 710072, China
2 College of Science, Sichuan Agricultural University, Ya'an 625014, China
Cite this article: 

Ning LI,Rong ZHANG,Limin ZHANG,Hui XING,Pengfei YIN,Yaoyan WU. Study on Grain Refinement Mechanism of Hypoeutectic Al-7%Si Alloy Under Low Voltage Alternating Current Pulse. Acta Metall Sin, 2017, 53(2): 192-200.

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Abstract  

The grain refinement mechanism of hypoeutectic Al-7%Si alloy under low voltage alternating current pulse (LACP) has been investigated in this work. In which LACP generated by the homemade low voltage modulation pulse generator is imposed in different solidification stages of the alloy and the wire mesh tubes of different diameters which have the effect of limiting the melt convection is embedded in sand mould. The experimental results show that the grains of casting alloy are evenly refined under LACP. The grain refinement will not appear, when LACP is imposed in the stages which are the alloy melt temperature is above 620 ℃ and late stages of crystal growth of primary phase. The grain refinement mainly occurs in nucleation stage and early growth stage of primary phase. The grains of inside and outside of wire mesh tube are refined together under LACP. But the grains of outside of wire mesh tube are much finer. The solidification microstructure of outside of wire mesh tube changes from large dendritic crystal to rose-shape crystal, nevertheless, it is still large dendritic crystal inside of wire mesh tube. Inocu lation effect and Joule heat effect of LACP have little effect on grain refinement of Al-7%Si alloy. The main reasons of grain refinement are the embryos fell off from chilling walls under LACP and the nucleation kinetics of the alloy was changed by LACP, which cause the nucleation rate of alloy increased. In addition, the α-dendrites became fragmentation under the forced melt flow which was induced by electromagnetic force can also lead to the grain refinement during the early growth stage of primary phase.

Key words:  Al-Si alloy      low voltage alternating current pulse      grain refinement      macrostructure      microstructure     
Received:  21 June 2016     
Fund: Supported by Fundamental Research Funds for the Central Universities (Nos.GEKY1008 and 3102015ZY078), Natural Science Foundation of Shaanxi Province (No.2015JQ5125), and Fundamental Research Funds of Northwestern Polytechnical University (No.JC201272)

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https://www.ams.org.cn/EN/10.11900/0412.1961.2016.00247     OR     https://www.ams.org.cn/EN/Y2017/V53/I2/192

Fig.1  Schematic of the designed molds (I—inside of wire mesh tube, II—outside of wire mesh tube)
(a) without wire mesh tube
(b) with wire mesh tube of 15 mm diameter
(c) with wire mesh tube of 8 mm diameter
Fig.2  Schematic of solidification stages of Al-7%Si alloy treated with low voltage alternating current pulse (LACP) (a—the whole solidification process: 720~550 ℃, b—the stage of molten metal: 720~620 ℃, c—nucleation stage of α-Al: 620~609 ℃, d—nucleation stage and early stages of crystal growth of α-Al: 620~600 ℃, e—late stages of crystal growth of α-Al: 600~550 ℃)
Fig.3  OM image of solidification macrostructure of Al-7%Si alloy without LACP
Fig.4  OM images of solidification macrostructures of Al-7%Si alloy with LACP of 230 A/cm2 at different solidification stages
(a) 720~550 ℃ (b) 720~620 ℃ (c) 620~609 ℃ (d) 620~600 ℃ (e) 600~550 ℃
Fig.5  Relationship between the mean grain size of equiaxed grain of Al-7%Si alloy and the different solidification stages with LACP of 230 A/cm2
Fig.6  OM images of solidification macrostructures of Al-7%Si alloy under LACP with wire mesh tube diameters of 15 mm (a) and 8 mm (b)
Fig.7  Electromagnetic force applied to the unit volume element melt with LACP
Fig.8  OM images of solidification microstructures of Al-7%Si alloy with wire mesh tube of diameters of 8 mm before and after LACP
(a) 0 A/cm2 (b) inside of wire mesh tube, 230 A/cm2 (c) outside of wire mesh tube, 230 A/cm2
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