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THE INTERFACE MICROSTRUCTURE OF A B_4C_p +SiC_w/MB15 MAGNESIUM BASED COMPOSITE |
WU Zhengan; GU Mingyuan; CHEN Yu; ZHANG Gooding (The State Key Laboratory of MMCs; Shanghai Jiaotong University; Shanghai 200030) |
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Cite this article:
WU Zhengan; GU Mingyuan; CHEN Yu; ZHANG Gooding (The State Key Laboratory of MMCs; Shanghai Jiaotong University; Shanghai 200030). THE INTERFACE MICROSTRUCTURE OF A B_4C_p +SiC_w/MB15 MAGNESIUM BASED COMPOSITE. Acta Metall Sin, 1998, 34(4): 443-448.
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Abstract The magnesium alloy (MB15) matrix composites reinforced by the hybrid ofthe boron carbide particle and the silicon carbide whisker were fabricated with vacuum pressure infiltration and hot extrusion techniques. The interface microstructure of the composite has been studied using analytical electron microscope (equipped with EDS, EELS). Experimental results showed that the chemical reaction 4Mg(1)+B2O3(1)=MgB2(s)+3MgO(s) took place during infiltration, and produced magnesium diboride (MgB2) phase and MgO microcrystallites. Due to this interface reaction, liquid magnesium wetted boron carbide particle. Moreover, the surface of boron carbide particle had a serrated periphery, thus a strong interfacial bonding was formed,which resulted in excellent mechanical properties of the composite. Because of the flowabilityof boron chide, the same interfacial reaction also took place at the SiCw/Mg interface region,where the SiC whisker is near a boron carbide particle. When the SiC whisker is far from a boroncarbide particle, the SiCw/Mg interface is straight with β' (MgZn2) precipitates on it.
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Received: 18 April 1998
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