Microstructure and Mechanical Properties of Ti6Al4V Alloy by Laser Integrated Additive Manufacturing with Alternately Thermal/Mechanical Effects
LU Haifei, LV Jiming, LUO Kaiyu, LU Jinzhong()
School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013, China
Cite this article:
LU Haifei, LV Jiming, LUO Kaiyu, LU Jinzhong. Microstructure and Mechanical Properties of Ti6Al4V Alloy by Laser Integrated Additive Manufacturing with Alternately Thermal/Mechanical Effects. Acta Metall Sin, 2023, 59(1): 125-135.
To meet the requirements of the long fatigue life and high reliability of the key components of the aeroengine as well as solve the challenges of “structure control” and “performance control” based on the fact that plastic deformation can effectively eliminate internal stress and close metallurgical defects generated by the thermal effect, a laser integrated additive manufacturing technology with alternately thermal/mechanical effects is developed. In this study, Ti6Al4V alloy was chosen as the research object. The distributions of residual stress and metallurgical defects and the microstructural evolution of the formed components were systematically studied. The effects of surface laser shock peening (LSP) and interlayer LSP without coating (LSPwC) treatments on mechanical properties were investigated using a tensile test. The results showed that after LSP, tensile residual stress was transformed into compressive residual stress. Additionally, laser shock waves could effectively improve the metallurgical defects in selective laser melting (SLM)-formed components. Moreover, high-density dislocation structures and numerous twins in two directions were produced in coarse α' martensite by laser shock waves, which jointly promoted the grain refinement of α' martensite. The ultimate tensile strength and elongation of Ti6Al4V fabricated by the laser integrated additive manufacturing technology with alternately thermal/mechanical effects reached 1543 MPa and 15.53%, which are 46.5% and 91.5% higher than those of the SLM-formed components, respectively, yielding a good combination of strength and ductility.
Fund: National Natural Science Foundation of China(52175409);National Natural Science Foundation of China(52175323);Jiangsu Provincial Science and Technology Projects in China(BE2021072);Jiangsu Provincial Science and Technology Projects in China(BE2022069-4)
About author: LU Jinzhong, professor, Tel: (0511)88797198, E-mail: jzlu@ujs.edu.cn
Fig.1 Schematics of selective laser melting (SLM) (a), laser shock peening (LSP) (b), the preparation of SLM and SLM-LSP specimens (c), and dimensions of tensile specimen (unit: mm) (d) (CAD—computer-aided design, LSPwC—laser shock peening without coating)
Fig.2 In-depth residual stress distributions of SLM and SLM-LSP specimens
Fig.3 Cross-setional OM images of SLM (a) and SLM-LSP (b) specimens (The dotted lines represent the interfaces between the third layer and second layer)
Fig.4 TEM images in the surface layer of SLM specimen (a) acicular α' martensite (b) magnified image of square region in Fig.4a and the corresponding SAED pattern (inset) (c) mechanical twins (d) dislocation lines
Fig.5 TEM images in the surface layer of SLM-LSP specimen (a) refined α' martensites (b) a large number of parallel mechanical twins and high density dislocation structures (c) magnified image of region Ⅰ in Fig.5b (d) SAED pattern of region Ⅰ in Fig.5b showing {101} twin (T—twin, M—martensite) (e) magnified image of region Ⅱ in Fig.5b (f) SAED pattern of region Ⅱ in Fig.5b showing {102} twin
Fig.6 TEM analyses of dislocations in the surface layer of SLM-LSP specimen (a, b) HRTEM image (a) and corresponding SEAD pattern (b) (c) inverse fast Fourier-transform (IFFT) image of square region in Fig.6a (d) atom arrangement on the () plane (e) atom arrangement on the () plane (f) atom arrangement on the (0001) plane
Fig.7 3D reconstruction graphs revealing 3D pore characteristics (a, c) and statistical results of the size and number of defects (b, d) for SLM specimen (a, b) and SLM-LSP specimen (c, d)
Fig.8 Engneering stress-strain curves of the tensile SLM and SLM-LSP specimens
Fig.9 SEM fracture morphologies of SLM (a, a1, a2) and SLM-LSP (b, b1, b2) specimens (B.D.—building direction)
1
Zhao Y Q, Xi Z P, Qu H L. Current situation of titanium alloy materials used for national aviation [J]. J. Aeronaut. Mater., 2003, 23(): 215
Machado A R, Wallbank J. Machining of titanium and its alloys—A review [J]. Proc. Inst. Mech. Eng., 1990, 204B: 53
3
Wang M, Lin X, Huang W. Laser additive manufacture of titanium alloys [J]. Mater. Technol., 2016, 31: 90
4
Liang Z Y, Zhang A F, Liang S D, et al. Research developments of high-performance titanium alloy by laser additive manufacturing technology [J]. Appl. Laser, 2017, 37: 452
Mercelis P, Kruth J P. Residual stresses in selective laser sintering and selective laser melting [J]. Rapid Prototyp. J., 2006, 12: 254
doi: 10.1108/13552540610707013
6
Qiu C L, Panwisawas C, Ward M, et al. On the role of melt flow into the surface structure and porosity development during selective laser melting [J]. Acta Mater., 2015, 96: 72
doi: 10.1016/j.actamat.2015.06.004
7
Wu Z K, Wu S C, Zhang J, et al. Defect induced fatigue behaviors of selective laser melted Ti-6Al-4V via synchrotron radiation X-ray tomography [J]. Acta Metall. Sin., 2019, 55: 811
doi: 10.11900/0412.1961.2018.00408
Lv Y, Lei L Q, Sun L N. Influence of different combined severe shot peening and laser surface melting treatments on the fatigue performance of 20CrMnTi steel gear [J]. Mater. Sci. Eng., 2016, A658: 77
9
Chen A Y, Jia Y Q, Pan D, et al. Reinforcement of laser-welded stainless steels by surface mechanical attrition treatment [J]. Mater. Sci. Eng., 2013, A571: 161
10
Colegrove P A, Coules H E, Fairman J, et al. Microstructure and residual stress improvement in wire and arc additively manufactured parts through high-pressure rolling [J]. J. Mater. Process. Technol., 2013, 213: 1782
doi: 10.1016/j.jmatprotec.2013.04.012
11
Fan Y J, Zhao X H, Liu Y. Research on fatigue behavior of the flash welded joint enhanced by ultrasonic peening treatment [J]. Mater. Des., 2016, 94: 515
doi: 10.1016/j.matdes.2016.01.070
12
Hatamleh O. A comprehensive investigation on the effects of laser and shot peening on fatigue crack growth in friction stir welded AA 2195 joints [J]. Int. J. Fatigue, 2009, 31: 974
doi: 10.1016/j.ijfatigue.2008.03.029
13
Montross C S, Wei T, Lin Y, et al. Laser shock processing and its effects on microstructure and properties of metal alloys: A review [J]. Int. J. Fatigue, 2002, 24: 1021
doi: 10.1016/S0142-1123(02)00022-1
14
Gao Y K. Influence of different surface modification treatments on surface integrity and fatigue performance of TC4 titanium alloy [J]. Acta Metall. Sin., 2016, 52: 915
Dorman M, Toparli M B, Smyth N, et al. Effect of laser shock peening on residual stress and fatigue life of clad 2024 aluminium sheet containing scribe defects [J]. Mater. Sci. Eng., 2012, A548: 142
16
Luo K Y, Jing X, Sheng J, et al. Characterization and analyses on micro-hardness, residual stress and microstructure in laser cladding coating of 316L stainless steel subjected to massive LSP treatment [J]. J. Alloys Compd., 2016, 673: 158
doi: 10.1016/j.jallcom.2016.02.266
17
Kalentics N, Boillat E, Peyre P, et al. Tailoring residual stress profile of selective laser melted parts by laser shock peening [J]. Addit. Manuf., 2017, 16: 90
18
Luo S H, He W F, Chen K, et al. Regain the fatigue strength of laser additive manufactured Ti alloy via laser shock peening [J]. J. Alloys Compd., 2018, 750: 626
doi: 10.1016/j.jallcom.2018.04.029
19
Sun R J, Li L H, Zhu Y, et al. Microstructure, residual stress and tensile properties control of wire-arc additive manufactured 2319 aluminum alloy with laser shock peening [J]. J. Alloys Compd., 2018, 747: 255
doi: 10.1016/j.jallcom.2018.02.353
20
Chi J X, Cai Z Y, Wan Z D, et al. Effects of heat treatment combined with laser shock peening on wire and arc additive manufactured Ti17 titanium alloy: Microstructures, residual stress and mechanical properties [J]. Surf. Coat. Technol., 2020, 396: 125908
doi: 10.1016/j.surfcoat.2020.125908
21
Guo W, Sun R J, Song B W, et al. Laser shock peening of laser additive manufactured Ti6Al4V titanium alloy [J]. Surf. Coat. Technol., 2018, 349: 503
doi: 10.1016/j.surfcoat.2018.06.020
22
Chi J X, Cai Z Y, Zhang H P, et al. Combining manufacturing of titanium alloy through direct energy deposition and laser shock peening processes [J]. Mater. Des., 2021, 203: 109626
doi: 10.1016/j.matdes.2021.109626
23
Lan L, Jin X Y, Gao S, et al. Microstructural evolution and stress state related to mechanical properties of electron beam melted Ti-6Al-4V alloy modified by laser shock peening [J]. J. Mater. Sci. Technol., 2020, 50: 153
doi: 10.1016/j.jmst.2019.11.039
24
Jin X Y, Lan L, Gao S, et al. Effects of laser shock peening on microstructure and fatigue behavior of Ti-6Al-4V alloy fabricated via electron beam melting [J]. Mater. Sci. Eng., 2020, A780: 139199
25
Peyre P, Carboni C, Forget P, et al. Influence of thermal and mechanical surface modifications induced by laser shock processing on the initiation of corrosion pits in 316L stainless steel [J]. J. Mater. Sci., 2007, 42: 6866
doi: 10.1007/s10853-007-1502-4
26
Kalentics N, Boillat E, Peyre P, et al. 3D laser shock peening—A new method for the 3D control of residual stresses in selective laser melting [J]. Mater. Des., 2017, 130: 350
doi: 10.1016/j.matdes.2017.05.083
27
Kalentics N, Sohrabi N, Tabasi H G, et al. Healing cracks in selective laser melting by 3D laser shock peening [J]. Addit. Manuf., 2019, 30: 100881
28
Kalentics N, de Seijas M O V, Griffiths S, et al. 3D Laser shock peening—A new method for improving fatigue properties of selective laser melted parts [J]. Addit. Manuf., 2020, 33: 101112
29
Bartlett J L, Li X D. An overview of residual stresses in metal powder bed fusion [J]. Addit. Manuf., 2019, 27: 131
doi: 10.1016/j.addma.2019.02.020
30
Lu J Z, Wu L J, Sun G F, et al. Microstructural response and grain refinement mechanism of commercially pure titanium subjected to multiple laser shock peening impacts [J]. Acta Mater., 2017, 127: 252
doi: 10.1016/j.actamat.2017.01.050
31
Cloots M, Uggowitzer P J, Wegener K. Investigations on the microstructure and crack formation of IN738LC samples processed by selective laser melting using Gaussian and doughnut profiles [J]. Mater. Des., 2016, 89: 770
doi: 10.1016/j.matdes.2015.10.027
32
Liu X Q, Tan C W, Zhang J, et al. Influence of microstructure and strain rate on adiabatic shearing behavior in Ti-6Al-4V alloys [J]. Mater. Sci. Eng., 2009, A501: 30
33
Leuders S, Thöne M, Riemer A, et al. On the mechanical behaviour of titanium alloy TiAl6V4 manufactured by selective laser melting: Fatigue resistance and crack growth performance [J]. Int. J. Fatigue, 2013, 48: 300
doi: 10.1016/j.ijfatigue.2012.11.011
34
Sanaty-Zadeh A. Comparison between current models for the strength of particulate-reinforced metal matrix nanocomposites with emphasis on consideration of Hall-Petch effect [J]. Mater. Sci. Eng., 2012, A531: 112
35
Lu K, Lu L, Suresh S. Strengthening materials by engineering coherent internal boundaries at the nanoscale [J]. Science, 2009, 324: 349
doi: 10.1126/science.1159610
pmid: 19372422
36
Wang C L, Yu D P, Niu Z Q, et al. The role of pyramidal <c + a> dislocations in the grain refinement mechanism in Ti-6Al-4V alloy processed by severe plastic deformation [J]. Acta Mater., 2020, 200: 101
doi: 10.1016/j.actamat.2020.08.076
37
Liu W H, Wu Y, He J Y, et al. Grain growth and the Hall-Petch relationship in a high-entropy FeCrNiCoMn alloy [J]. Scr. Mater., 2013, 68: 526
doi: 10.1016/j.scriptamat.2012.12.002
38
Tian X N, Zhu Y M, Lim C V S, et al. Isotropic and improved tensile properties of Ti-6Al-4V achieved by in-situ rolling in direct energy deposition [J]. Addit. Manuf., 2021, 46: 102151
39
Vandenbroucke B, Kruth J P. Selective laser melting of biocompatible metals for rapid manufacturing of medical parts [J]. Rapid Prototyp. J., 2007, 13: 196
doi: 10.1108/13552540710776142
40
Lv J M, Luo K Y, Lu H F, et al. Achieving high strength and ductility in selective laser melting Ti-6Al-4V alloy by laser shock peening [J]. J. Alloys Compd., 2022, 899: 163335
doi: 10.1016/j.jallcom.2021.163335
41
Lu H F, Wu L J, Wei H L, et al. Microstructural evolution and tensile property enhancement of remanufactured Ti6Al4V using hybrid manufacturing of laser directed energy deposition with laser shock peening [J]. Addit. Manuf., 2022, 55: 102877