Please wait a minute...
Acta Metall Sin  2014, Vol. 50 Issue (12): 1413-1420    DOI: 10.11900/0412.1961.2014.00306
Current Issue | Archive | Adv Search |
EFFECT OF INDUCTION TEMPERING ON CARBIDE PRECIPITATION BEHAVIOR AND TOUGHNESS OF A 1000 MPa GRADE HIGH STRENGTH LOW ALLOY STEEL
FANG Yupei, XIE Zhenjia, SHANG Chengjia()
School of Materials Science and Engineering, University Science and Technology Beijing, Beijing 100083
Cite this article: 

FANG Yupei, XIE Zhenjia, SHANG Chengjia. EFFECT OF INDUCTION TEMPERING ON CARBIDE PRECIPITATION BEHAVIOR AND TOUGHNESS OF A 1000 MPa GRADE HIGH STRENGTH LOW ALLOY STEEL. Acta Metall Sin, 2014, 50(12): 1413-1420.

Download:  HTML  PDF(11158KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

By comparing induction tempering with conventional tempering, the effect of induction reheating tempering on carbide precipitation behavior and toughness of a 1000 MPa grade high strength low alloy steel was investigated. Microstructures of the steel in different heat treatment stages were characterized using SEM and TEM (with EDS), mechanical properties inclusive of Vickers hardness and toughness were tested. The results showed that microstructure of quenched samples consisted of lath martensite and lower bainite, needle like carbides were observed in lower bainitic lath. With tempering temperature increasing from 400 ℃ to 550 ℃, the shape of carbides located within the bainitic lath gradually changed from needle like to short rod like type. Carbides were fine and well distributed using induction tempering. When the tempering temperature was 550 ℃, the long axis length of short rod like carbides located within the bainitic lath by conventional reheating tempering was 200 nm, whereas the long axis length of short rod like carbides located within the bainitic lath by induction reheating tempering was about 60 nm. When tempering by conventional reheating, carbides mainly precipitated along martensite lath boundaries, while carbides were more dispersed in the matrix lath by induction reheating, the size of these dispersed carbides was less than 100 nm when tempering temperature was 550 ℃. As a result, a superior of mechanical properties with 344 HV and Charpy impact energy of 133 J at -20 ℃ was obtained with induction reheating tempering at 550 ℃.

Key words:  high strength low alloy steel      induction tempering      toughness      nano-sized carbide     
ZTFLH:  TG113  
Fund: Supported by National Basic Research Program of China (No.2010CB630801)

URL: 

https://www.ams.org.cn/EN/10.11900/0412.1961.2014.00306     OR     https://www.ams.org.cn/EN/Y2014/V50/I12/1413

Fig.1  Low (a) and locally high (b, c) magnified SEM images of the experimental steel after quenching
Fig.2  SEM images within the bainitic lath of the specimens tempered with conventional tempering (a, c, e) and induction tempering (b, d, f) at 400 ℃ (a, b), 480 ℃ (c, d) and 550 ℃ (e, f)
Fig.3  SEM images on the matensite lath boundary of the specimens tempered with conventional tempering (a, c, e) and induction tempering (b, d, f) at 400 ℃ (a, b), 480 ℃ (c, d) and 550 ℃ (e, f)
Fig.4  TEM images of the as-quenched specimens (a, b) and tempered at 550 ℃ with induction tempering (c, d) and conventional tempering (e, f)
Fig.5  Relationship between hardness (a), -20 ℃ impact energy AKV (b) and tempering temperature of the specimens tempered with conventional tempering and induction tempering
Fig.6  Axis ratio of the carbide precipitates within the lath in different tempering temperature with conventional tempering and induction tempering
Fig.7  TEM images of the replica-specimens as-quenched (a) and tempered at 550 ℃ with induction tempering (b) and EDS of the carbide marked by circle in Fig.7b (c)
Fig.8  SEM images of fracture surface in the specimens tempered at 550 ℃ with induction tempering (a) and conventional tempering (b)
[1] Akihide N, Takayuki I, Tadashi O. JFE Tech Rep, 2008; 6: 13
[2] Li X C, Xie Z J, Wang X L, Wang X M, Shang C J. Acta Metall Sin, 2013; 49: 167
(李秀程, 谢振家, 王学林, 王学敏, 尚成嘉. 金属学报, 2013; 49: 167)
[3] Barani A A, Li F, Romano P, Ponge D, Raabe D. Mater Sci Eng, 2007; A43: 138
[4] Hahn G T. Metall Trans, 1984; 15A: 947
[5] Furuhara T, Kobayashi K, Maki T. ISIJ Int, 2004; 44: 1937
[6] Xie Z J, Fang Y P, Han G, Guo H, Misra R D K, Shang C J. Mater Sci Eng, 2014; A618: 112
[7] Nam W J, Lee C S, Ban D Y. Mater Sci Eng, 2000; A289: 8
[8] Won J N, Dae S K, Soon T A. J Mater Sci Lett, 2003; 38: 3611
[9] Park J S, Lee Y K. Scr Mater, 2007; 57: 109
[10] Revilla C, Uranga P, Lopez B, Rodriguez-Ibabe J M. In: Bai D Q ed., Proc Materials Science and Technology Conference, Cleveland: Steel Product Metallurgy and Applications, 2012: 1069
[11] Lee J B, Kang N, Park J T, Ahn S T, Park Y D, Choi D, Kim K R, Cho K M. Mater Chem Phys, 2011; 129: 365
[12] Soon T A, Dae S K, Won J N. J Mater Process Technol, 2005; 160: 54
[13] Kawasaki K, Chiba T, Yamazaki T. Tetsu Hagané, 1988; 74: 334
(川嵜一博, 千葉貴世, 山崎隆雄. 鉄と鋼, 1988; 74: 334)
[14] Yusa S, Hara T, Tsuzaki K, Takahashi T. Mater Sci Eng, 1999; A273: 462
[15] Ahn S T, Cho K M, Lee S L, Kor J. Inst Met Mater, 2002; 40: 252
[16] Reviall C, López B, Rodriguez-Ibabe J M. Mater Des, 2014; 62: 296
[17] Yong Q L. Secondary Phases in Steel. Beijing: Metallurgical Industry Press, 2006: 226
(雍岐龙. 钢铁材料中的第二相. 北京: 冶金工业出版社, 2006: 226)
[18] Yang S W, Shang C J, He X L. Int J Miner Met Mater, 2001; 8: 119
[19] Yong Q L, Chen M X, Pei H Z, Pan L, Zhou X L, Yang T W, Zhong W, Hao J Y. J Iron Steel Res, 2006; 18(3): 30
(雍岐龙, 陈明昕, 裴和中, 潘 俐, 周晓玲, 杨天武, 钟 卫, 郝建英. 钢铁研究学报, 2006; 18(3): 30)
[20] Xu Y B, Yu Y M, Wu D, Wang G D. Chin J Mater Res, 2006; 20: 104
(许云波, 于永梅, 吴 迪, 王国栋. 材料研究学报, 2006; 20: 104)
[21] Liu Q D, Chu Y L, Wang Z M, Liu W Q, Zhou B X. Acta Metall Sin, 2008; 44: 1281
(刘庆冬, 褚于良, 王泽民, 刘文庆, 周邦新. 金属学报, 2008; 44:1281)
[22] Liu Q D, Liu W Q, Wang Z M, Zhou B X. Acta Metall Sin, 2009; 45: 1281
(刘庆冬, 刘文庆, 王泽民, 周邦新. 金属学报, 2009; 45: 1281)
[23] Nam W J, Kim D S. J Mater Sci, 2003; 38: 3611
[24] Hayakawa M, Matsuoka S, Tsuzaki K, Hanada H, Sugisaki M. Scr Mater, 2002; 47: 655
[25] Bowen P, Druce S G, Knott J F. Acta Metall, 1987; 35: 1735
[26] Chen Z Z, Ma Y L, Xing S Q, Feng D C, Li H Q. J Inn Mong Univ Sci Technol, 2010; 29: 123
(陈正宗, 麻永林, 邢淑清, 冯佃臣, 李慧琴. 内蒙古科技大学学报, 2010; 29: 123)
[1] WANG Bin, NIU Mengchao, WANG Wei, JIANG Tao, LUAN Junhua, YANG Ke. Microstructure and Strength-Toughness of a Cu-Contained Maraging Stainless Steel[J]. 金属学报, 2023, 59(5): 636-646.
[2] GU Ruicheng, ZHANG Jian, ZHANG Mingyang, LIU Yanyan, WANG Shaogang, JIAO Da, LIU Zengqian, ZHANG Zhefeng. Fabrication of Mg-Based Composites Reinforced by SiC Whisker Scaffolds with Three-Dimensional Interpenetrating-Phase Architecture and Their Mechanical Properties[J]. 金属学报, 2022, 58(7): 857-867.
[3] FENG Kai, GUO Yanbing, FENG Yulei, YAO Chengwu, ZHU Yanyan, ZHANG Qunli, LI Zhuguo. Microstructure Controlling and Properties of Laser Cladded High Strength and High Toughness Fe-Based Coatings[J]. 金属学报, 2022, 58(4): 513-528.
[4] LI Wei, JIA Xingqi, JIN Xuejun. Research Progress of Microstructure Control and Strengthening Mechanism of QPT Process Advanced Steel with High Strength and Toughness[J]. 金属学报, 2022, 58(4): 444-456.
[5] ZHOU Cheng, ZHAO Tan, YE Qibin, TIAN Yong, WANG Zhaodong, GAO Xiuhua. Effects of Tempering Temperature on Microstructure and Low-Temperature Toughness of 1000 MPa Grade NiCrMoV Low Carbon Alloyed Steel[J]. 金属学报, 2022, 58(12): 1557-1569.
[6] ZHU Dongming, HE Jiangli, SHI Genhao, WANG Qingfeng. Effect of Welding Heat Input on Microstructure and Impact Toughness of the Simulated CGHAZ in Q500qE Steel[J]. 金属学报, 2022, 58(12): 1581-1588.
[7] HU Chen, PAN Shuai, HUANG Mingxin. Strong and Tough Heterogeneous TWIP Steel Fabricated by Warm Rolling[J]. 金属学报, 2022, 58(11): 1519-1526.
[8] CHEN Ruirun, CHEN Dezhi, WANG Qi, WANG Shu, ZHOU Zhecheng, DING Hongsheng, FU Hengzhi. Research Progress on Nb-Si Base Ultrahigh Temperature Alloys and Directional Solidification Technology[J]. 金属学报, 2021, 57(9): 1141-1154.
[9] JIANG Zhonghua, DU Junyi, WANG Pei, ZHENG Jianneng, LI Dianzhong, LI Yiyi. Mechanism of Improving the Impact Toughness of SA508-3 Steel Used for Nuclear Power by Pre-Transformation of M-A Islands[J]. 金属学报, 2021, 57(7): 891-902.
[10] YANG Rui, MA Yingjie, LEI Jiafeng, HU Qingmiao, HUANG Sensen. Toughening High Strength Titanium Alloys Through Fine Tuning Phase Composition and Refining Microstructure[J]. 金属学报, 2021, 57(11): 1455-1470.
[11] LUO Haiwen,SHEN Guohui. Progress and Perspective of Ultra-High Strength Steels Having High Toughness[J]. 金属学报, 2020, 56(4): 494-512.
[12] WAN Xiangliang, HU Feng, CHENG Lin, HUANG Gang, ZHANG Guohong, WU Kaiming. Influence of Two-Step Bainite Transformation on Toughness in Medium-Carbon Micro/Nano-Structured Steel[J]. 金属学报, 2019, 55(12): 1503-1511.
[13] SHAO Yi , LI Yanmo , LIU Chenxi , YAN Zesheng , LIU Yongchang . Annealing Process Optimization of High Frequency Longitudinal Resistance Welded Low-CarbonFerritic Stainless Steel Pipe[J]. 金属学报, 2019, 55(11): 1367-1378.
[14] Mingyue WEN, Wenchao DONG, Huiyong PANG, Shanping LU. Microstructure and Impact Toughness of Welding Heat-Affected Zones of a Fe-Cr-Ni-Mo High Strength Steel[J]. 金属学报, 2018, 54(4): 501-511.
[15] Yizhe LI, Baoming GONG, Xiuguo LIU, Dongpo WANG, Caiyan DENG. Out-of-Plane Constraint Effect on the Fracture Toughness of Single Edge Notch Tension Specimens[J]. 金属学报, 2018, 54(12): 1785-1791.
No Suggested Reading articles found!