Strong and Tough Heterogeneous TWIP Steel Fabricated by Warm Rolling
HU Chen1,2, PAN Shuai1,3, HUANG Mingxin1,2()
1.Department of Mechanical Engineering, The University of Hong Kong, Hong Kong 999077, China 2.Shenzhen Institute of Research and Innovation, The University of Hong Kong, Shenzhen 518057, China 3.Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, China
Cite this article:
HU Chen, PAN Shuai, HUANG Mingxin. Strong and Tough Heterogeneous TWIP Steel Fabricated by Warm Rolling. Acta Metall Sin, 2022, 58(11): 1519-1526.
Twinning-induced plasticity (TWIP) steel has received significant research attention because of its superior mechanical properties, including uniform elongation, ultimate tensile strength, and fracture toughness. However, it has a relatively low yield stress, which limits its industrial application. Increasing the dislocation density has been proved to be an effective method for enhancing the yield stress. In this work, a simple warm rolling (WR) route was applied at 700oC to manufacture partially recrystallized TWIP steel with a high yield stress (1250 MPa), good total elongation (24%), and exceptional fracture toughness (KJIC of approximately 125 MPa·m1/2). The steel manufactured using WR was characterized using SEM, EBSD, and TEM at different length scales. Compared to the steel microstructure obtained after hot rolling or cold rolling (CR), this WR TWIP steel exhibits a distinct heterogeneous structure. The matrix has numerous dislocations with twinned coarse grains (approximately 75%) and nearly defect-free recrystallized fine grains (approximately 25%), which form during the reheating period of the WR process. The in situ tensile tests of the WR and CR steels show that the deformed coarse grains provide high yield stress with negligible deformation, whereas the recrystallized fine grains can undergo considerable plastic deformation, which results in a good work hardening capacity during tensile deformation. The fracture toughness tests of the compact tension (C(T)) samples indicate that the recrystallized grains in the WR steel can enhance the crack tip blunting and deflect cracks, which enhance the crack-growth resistance. Alternatively, these toughening mechanisms are not observed in the homogeneous CR steel. Therefore, this heterogeneous structure, which is induced by the high temperature WR process, provides the TWIP steel with excellent strength and toughness.
Fund: National Natural Science Foundation of China(52130102);National Key Research and Development Program of China(2019YFA0209900);Research Grants Council of Hong Kong(R7066-18);Guangzhou Municipal Science and Technology Bureau Program(202007020007);Guangdong Basic and Applied Basic Research Foundation of China(2020B1515130007)
About author: HUANG Mingxin, professor, Tel: (00852)39177906, E-mail: mxhuang@hku.hk
Fig.1 Inverse pole figures (IPFs) (a, d), phase maps with twinning boundaries (TBs) (b, e), and grain misorientation maps (c, f) of Hetero-T (a-c) and Homo-T (d-f)
Fig.2 Bright-field (a) and dark-field (b) TEM images, selected area electron diffraction (SAED) pattern (c), and STEM image (d) of recrystallized grains inside Hetero-T; bright-field (e) and dark-field (f) TEM images, and SAED pattern (g) of Homo-T (The matrix (M) and twin (T) diffraction patterns are shown by solid red and dash blue lines, respectively, and the corresponding indexes are shown in red and blue numbers in Figs.2c and g)
Fig.3 Engineering stress-strain curves (a), the loading-unloading-reloading hysteresis loops (b), J-R curves of Homo-T and Hetero-T (c), and tensile fracture surfaces of Hetero-T (d) and Homo-T (e) (J—measured J-integral, R—crack extension resistance, JIC—J-integral at crack extension of 0.2 mm, KJIC—plane-strain crack-initiation fracture toughness calculated by JIC, J1mm—J-integral at crack extension of 1 mm, KJ1mm—crack-growth fracture toughness calculated by J1mm, E—elastic modulus, μ—Poisson's ratio)
Sample
JIC / (kJ·m-2)
KJIC / (MPa·m1/2)
J1mm / (kJ·m-2)
KJ1mm / (MPa·m1/2)
Hetero-T
71.3
125.2
163.9
189.8
Homo-T
45.7
100.2
73.4
127.0
Table 1 Fracture toughness values of Hetero-T and Homo-T
Fig.4 IPFs (a, e) and KAM figures (b, f) before deforming, KAM figures at strains of 4% (c, g) and 12% (d, h), the full map KAM evolution with strain (i, k), and KAM evolutions of selected areas (white selected areas) with strain (j, l) of the Hetero-T (a-d, i, j) and Homo-T (e-h, k, l)
Fig.5 BSE images of the crack tips (a, c) and crack growth paths (b, d) of Hetero-T (a, b) and Homo-T (c, d)
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