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HIGH RESOLUTION ELECTRON MICROSCOPIC STUDY OF IMMISCIBLE Cu-Fe SYSTEM DURING MECHANICAL ALLOYING |
WU Yukun;HUANG Jianyu;HE Anqiang;HU Kuiyi;MENG Xiangmin Laboratory of Atomic Imaging of Solids; Institute of Metal Research; Academia Sinica; Shenyang |
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Cite this article:
WU Yukun;HUANG Jianyu;HE Anqiang;HU Kuiyi;MENG Xiangmin Laboratory of Atomic Imaging of Solids; Institute of Metal Research; Academia Sinica; Shenyang. HIGH RESOLUTION ELECTRON MICROSCOPIC STUDY OF IMMISCIBLE Cu-Fe SYSTEM DURING MECHANICAL ALLOYING. Acta Metall Sin, 1993, 29(12): 39-46.
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Abstract Supersaturated solid solutions have been obtained by mechanical alloying inCu-Fe system which are immiscible at room temperature. The fcc phase range has been ex-tended to x>35 at.-% Cu. High resolution electron microscope images show that thereexist N-W orientation relationship,i.e. < 001 > α//<110>γ and < 110 > α// < 111 > γbetween bcc phase and fcc phase after 3h milling. It is quite possible that inverse martensitictransformation has occurred during mechanical alloying and the extension of fcc phase rangeclosely relates to this transformation. The fracture and refinement of particles, and cold-weld-ing images were also observed by using a high resolution electron microscope. After 60h me-chanical alloying, homogenous nanocrystals with particle size about 10 nm formed.
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1 Schwarz R B, Koch C C. Appl Phys Lett, 1989; 49: 146 2 Eckert J, Schultz L, Urban K. Appl Phys Lett, 1988; 55: 117 3 Hellstern E, Fech H J, Fu Z, Johnson W L. J Appl Phys, 1989; 65. 305 4 Eckert J, Holzer J C, Krill C E, Ⅲ, Johnson W L. J Mater Res, 1992; 7: 1751 5 Schultz l. Mater Sci Eng 1989; 97: 15. 6 Massalski T B. Binary Alloys Phase Diagram, 2nd ed, Metals Park, Ohio. ASM INTERNATIONAL, 1990 7 Uenishi k, Kobayashi K F, Nasu S, Hatano H, Ishibara K N, Singu P H. Z Metalk, 1992; 83. 132 8 杨元政,马学鸣,董远达.金属学报,1992;28:A399 9 Eckert J, Holzer J C, Krill C E, Ⅲ, Johnson W L. J Mater Res. 1992; 7: 1980 10 齐民,朱敏,刘文革,刘伟,杨大智.材料科学进展.1993;7:31 11 Yavari A R, Desre P J, Benameur T. Phys Rev Lett, 1992, 68: 2235 12 黄建宇,吴玉琨,胡魁毅,孟祥敏.金属学报,1993;29:60 13 Huang J Y, He A Q, Wu Y K. J Appl Phys (Submitted) 14 Schwarz R B. Petrich C K, Saw C K, J Non-Cryst Solids, 1986; 76: 281 15 Hellstern E, Schultz L. Appl Phys Lett, 1988; 48: 124 16 Klement W, Jr. Trans AIME, 1986; 233. 1180 17 Guinier A. X-ray Diffraction. Freeman, Sanfrancisco, CA, 1963; 124 |
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