金属学报  2011, Vol. 47 Issue (12): 1561-1566    DOI: 10.3724/SP.J.1037.2011.00401

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多向压缩变形及退火制备超细晶铜合金

杨续跃,张之岭,王军,秦佳,陈志永

中南大学材料科学与工程学院, 有色金属材料科学与工程教育部重点实验室, 长沙 410083

PREPARATION OF ULTRAFINE–GRAINED COPPER ALLOY PROCESSED BY ANNEALING TREATMENT AFTER MULTI–DIRECTIONAL COMPRESSION

YANG Xuyue, ZHANG Zhiling, WANG Jun, QIN Jia, CHEN Zhiyong

Key Laboratory of Nonferrous Metal Materials Science and Engineering, Ministry of Education, School of Materials Science and Engineering, Central South University, Changsha 410083

杨续跃 张之岭 王军 秦佳 陈志永. 多向压缩变形及退火制备超细晶铜合金[J]. 金属学报, 2011, 47(12): 1561-1566.
, , , . PREPARATION OF ULTRAFINE–GRAINED COPPER ALLOY PROCESSED BY ANNEALING TREATMENT AFTER MULTI–DIRECTIONAL COMPRESSION[J]. Acta Metall Sin, 2011, 47(12): 1561-1566.

摘要 参考文献 相关文章 Metrics 全文: PDF(1016 KB)   摘要: 通过OM, TEM和SEM/EBSD研究了QBe1.7铜合金室温多向压缩变形及973 K退火后的微观组织及其取向演化规律. 结果表明: 室温变形时,其真应力-累积真应变(σ-Σε)曲线因动态回复而呈类似稳态流变特征, 随变形道次的增加组织内部产生了大量的亚晶,但均匀弥散分布的细小析出物的存在严重抑制了动态再结晶的进行,累积变形至Σε=4.8时仍未出现细晶; 而在中等变形程度下(Σε=2.4)通过退火处理可获得平均晶粒尺寸仅0.8 μm左右的超细晶组织. 超细晶主要是由变形所产生的中低角度晶界迅速转变为包含大量孪晶界的高角晶界演化而成. 根据晶粒尺寸变化可把退火过程分为回复、晶粒急剧细化和晶粒正常长大3个阶段. 关键词 ： 铜合金,  多向压缩,  退火处理,  超细晶,  再结晶     Abstract：Ultrafine grained (UFG) metallic materials arouse a great interest due to their great mechanical properties. Through the way of severe plastic deformation (SPD), including equal channel angular pressing (ECAP) and high–pressure torsion (HPT), the UFG materials obtained can be of obvious improvement in strength but of decrease in their thermal stability and ductility. In this article, the authors manage to obtain an UFG QBe1.7 copper alloy with great comprehensive properties by annealing the samples after being multi–directional compressioned (MDCed) at room temperature. The multiple tests were carried out using rectangular samples with consequent changing of loading direction in 90? through three of mutually perpendicular axes from pass–to–pass. The deformed and subsequent annealed microstructures were investigated by OM, TEM and SEM/EBSD metallographic observations. The integrated flow curves plotted over a number of compression passes increase to a maximum at moderate strains of 1 to 2 followed by steady–state–like flow at high cumulative strains. Fine grains were not observed even at a higher cumulative stain of Σε=4.8, although there were many sub–grains when the samples were deformed to Σε=2.4. This indicates that the dynamic recrystallization or recovery was completely inhibited by fine precipitates. Static recrystallization (SRX) of the MDCed structure at 973 K was also investigated. With the increment of cumulative strains, the effect of grain refinement became more obvious, but the thermal stability was getting worse. At a medium strain of Σε=2.4, the minimal grain size of 0.8 μm can be developed with an excellent combination property. The formation of ultrafine grain is characterized by large–angle boundaries developed from low to medium boundaries. The change of the average grain size with annealing time can be divided into three stages: a recovery period for grain refinement, rapid grain refinement and normal grain growth. Key words： copper alloy    multi–directional compression    annealing    ultrafine grain    recrystallization 收稿日期: 2011-06-28      基金资助: 国家自然科学基金项目51174234和中央高校基本科研业务费中南大学前瞻重点项目2010QZDD014资助 作者简介: 杨续跃, 男, 1959年生, 教授 服务 把本文推荐给朋友 加入引用管理器 E-mail Alert RSS 作者相关文章 杨续跃 张之岭 王军 陈志永 44.8K 链接本文: https://www.ams.org.cn/CN/10.3724/SP.J.1037.2011.00401      或      https://www.ams.org.cn/CN/Y2011/V47/I12/1561 [1] Armstrong R W. Metall Mater Trans, 1970; 1: 1169 [2] Hansen N. Scr Mater, 2004; 51: 801 [3] Mishra A, Kad B K, Gregori F, Meyers M A. 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