金属学报  2007, Vol. 43 Issue (4): 393-398

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强流脉冲离子束辐照对316L不锈钢表面改性的实验研究

王旭;张俊善;雷明凯

大连理工大学材料科学与工程学院

EXPERIMENTAL RESEARCH ON THE SURFACE MODIFICATION OF 316L STAINLESS STEEL BY HIGH-INTENSITY PULSED ION BEAMS

Xu Wang;;

大连理工大学材料科学与工程学院

王旭; 张俊善; 雷明凯 . 强流脉冲离子束辐照对316L不锈钢表面改性的实验研究[J]. 金属学报, 2007, 43(4): 393-398 .
, , . EXPERIMENTAL RESEARCH ON THE SURFACE MODIFICATION OF 316L STAINLESS STEEL BY HIGH-INTENSITY PULSED ION BEAMS[J]. Acta Metall Sin, 2007, 43(4): 393-398 .

摘要 参考文献 相关文章 Metrics 全文: PDF(689 KB)   摘要: 利用离子能量为300 keV、束流密度为200 A/cm2、脉冲宽度为75 ns的混合离子束(70%H++30%C+)组成的强流脉冲离子束(HIPIB)对316L不锈钢进行了表面辐照处理, 辐照次数分别为1, 5, 10次. 采用SEM, XRD, TEM和EPMA分析辐照后试样表面形貌、表面层相组成和微观结构及元素分布的变化. 结果表明, HIPIB辐照使试样表面光滑化, 表面层晶粒细化、产生择优取向, 杂质元素选择性烧蚀, 电化学腐蚀性能明显提高. 由于HIPIB辐照引起的大应力和冲击波的影响, 辐照后在深度达100μm表层内显微硬度提高, 表面摩擦系数降低, 表面抗磨损性能显著改善.随着辐照次数的增加, 316L疲劳极限和蠕变断裂寿命延长, 稳态蠕变速率降低. 关键词 ： 强流脉冲离子束,  316L不锈钢,  表面改性     Abstract：The surface of 316L stainless steel was treated by high-intensity pulsed ion beams (HIPIB) with ion energy (70% H+, 30% C+) E = 300 keV, current density J = 200 A/cm2, shot number N = 1, 5, 10, pulse duration τ = 75ns. The surface morphology and the phase structure in the near surface region of original and treated specimens were analyzed with scanning electron microscopy (SEM) and X-ray diffraction (XRD). Electron probe microanalysis (EPMA) was used to study the distribution of elements on the irradiated specimens. It is found that the HIPIB irradiation can smooth the surface of the targets, and the preferred orientation was present in the surface layer of the treated specimens. Otherwise, selective ablation of impurities occurred during the interaction between HIPIB and the targets. The microhardness was increased in a depth range of up to 100 μm due to extremely high stresses and shock waves induced by the bombardment, so as to the friction coefficient of the irradiated surfaces was reduced and the wear resistance of them was improved significantly. Under the cooperation of the smooth surface and the grain refinement with the selective ablation of impurities, the electrochemical corrosion resistance of 316L was enhanced markedly. HIPIB irradiation prolongs the fatigue limit and creep rupture life of 316L, simultaneity reduces the steady creep rate with increasing the shot number. Key words： High-intensity pulsed ion beams (HIPIB)    316L stainless steel    surface modification 收稿日期: 2006-08-23      ZTFLH:  TG142.71   服务 把本文推荐给朋友 加入引用管理器 E-mail Alert RSS 作者相关文章 王旭 张俊善 雷明凯 44.8K 链接本文: https://www.ams.org.cn/CN/      或      https://www.ams.org.cn/CN/Y2007/V43/I4/393 [1]Davis H A,Remnev G E,Stinnett R W,Yatsui K.Mater Res Bull,1996;21:58 [2]Rej D J,Davis H A,Nastasi M,Olson J C,Peterson E J, Reiswig R D,Walter K C.Stinnett R W,Remnev G E, Strutsn V K.Nuclear Instrum Method,1997;127/128B: 987 [3]Shulov V A,Nochovnaya N A,Remnev G E.Mater Sci Eng,1998;A243:290 [4]Akamatsu H,Tanihara Y,Ikeda T,Iwasaki H,Azuma K, Yatsuzuka M.IEEE Trans Plasma Sci,2002;30:1800 [5]Zhang H T,Wang T M,Wang C.Han B X,Yan S,Zhao W J,Han Y F.Nucl Instrum Methods,2002;197B:83 [6]Le X Y,Zhao W J,Yan S,Han B X,Xiang W.Surf Coat Technol,2002;158-159:14 [7]Zhu X P,Lei M K,Ma T C.Nuclear Instrum Method, 2003;211B:69 [8]Korotaev A D,Tyumentsev A N,Pinzhin Y P,Remnev G E.Surf Coat Technol,2004;185:38 [9]Korotaev A D,Ovchinnikov S V,Pochivalov Y I,Tyu- mentsev A N,Shchipakin D A,Tretjak M V,Isakov I F, Remnev G E.Surf Coat Technol,1998;105:84 [10]Zhang H T,Wang T M,Wang C,Wang W J,Han B X, Yan S,Zhao W J,Han Y F.Rare Met Mater Eng,2003; 32:216 (张洪涛,王天民,王聪,王文军,韩宝玺,颜莎,赵渭江,韩雅芳．稀有金属材料与工程,2003;32:216) [11]Mei X X,Ma T C,Wang X M,Xu W P,Song M L.Acta Metall Sin,2003;39:926 (梅显秀,马腾才,王秀敏,徐卫平,宋美丽．金属学报,2003; 39:926) [1] 高晗, 刘力, 周笑宇, 周心怡, 蔡汶君, 周泓伶. Ti6Al4V表面微纳结构的制备及生物活性[J]. 金属学报, 2023, 59(11): 1466-1474. [2] 崔振铎, 朱家民, 姜辉, 吴水林, 朱胜利. Ti及钛合金表面改性在生物医用领域的研究进展[J]. 金属学报, 2022, 58(7): 837-856. [3] 余晨帆, 赵聪聪, 张哲峰, 刘伟. 选区激光熔化316L不锈钢的拉伸性能[J]. 金属学报, 2020, 56(5): 683-692. [4] 李丹, 李杨, 陈荣生, 倪红卫. 不锈钢网上水热制备NiCo2O4/MoS2纳米复合结构及其在电解水制氢中的应用[J]. 金属学报, 2018, 54(8): 1179-1186. [5] 刘廷光, 夏爽, 白琴, 周邦新. 316L不锈钢的三维晶粒与晶界形貌特征及尺寸分布[J]. 金属学报, 2018, 54(6): 868-876. [6] 刘廷光, 夏爽, 白琴, 周邦新, 陆永浩. 孪晶界在316L不锈钢三维晶界网络中的分布特征[J]. 金属学报, 2018, 54(10): 1377-1386. [7] 郭舒,韩恩厚,王海涛,张志明,王俭秋. 核电站316L不锈钢弯头应力腐蚀行为的寿命预测[J]. 金属学报, 2017, 53(4): 455-464. [8] 张二林, 王晓燕, 憨勇. 医用多孔Ti及钛合金的国内研究现状[J]. 金属学报, 2017, 53(12): 1555-1567. [9] 林潇, 葛隽, 吴水林, 刘宝华, 杨惠林, 杨磊. 兼具成骨和抗感染性能的医用金属材料研究进展[J]. 金属学报, 2017, 53(10): 1284-1302. [10] 于振涛, 余森, 程军, 麻西群. 新型医用钛合金材料的研发和应用现状[J]. 金属学报, 2017, 53(10): 1238-1264. [11] 马广璐, 崔新宇, 沈艳芳, NuriaCINCA, JosepM.GUILEMANY, 熊天英. 基体材料力学性能对316L不锈钢颗粒沉积行为的影响*[J]. 金属学报, 2016, 52(12): 1610-1618. [12] 罗新民, 王翔, 陈康敏, 鲁金忠, 王兰, 张永康. 激光冲击诱导的航空铝合金表层高熵结构及其抗蚀性[J]. 金属学报, 2015, 51(1): 57-66. [13] 刘侠和, 吴欣强, 韩恩厚. 温度对国产核级316L不锈钢在加Zn水中电化学腐蚀性能的影响*[J]. 金属学报, 2014, 50(1): 64-70. [14] 张利涛,王俭秋. 国产锻造态核级管材316L不锈钢在高温高压水中的应力腐蚀裂纹扩展行为[J]. 金属学报, 2013, 49(8): 911-916. [15] 罗新民,陈康敏,张静文,鲁金忠,任旭东,罗开玉,张永康. 纯Al和铝合金激光冲击表面改性的位错机制[J]. 金属学报, 2013, 49(6): 667-674. Viewed Full text Abstract Cited   Shared      Discussed