镍基单晶高温合金<strong>DD432</strong>的持久性能各向异性

doi:10.11900/0412.1961.2022.00108

金属学报

2023, Vol. 59

Issue (12): 1559-1567 DOI: 10.11900/0412.1961.2022.00108

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镍基单晶高温合金DD432的持久性能各向异性

张子轩¹^,², 于金江¹(

), 刘金来¹

¹中国科学院金属研究所师昌绪先进材料创新中心沈阳 110016
²中国科学技术大学材料科学与工程学院沈阳 110016

Anisotropy of Stress Rupture Property of Ni Base Single Crystal Superalloy DD432

ZHANG Zixuan¹^,², YU Jinjiang¹(

), LIU Jinlai¹

¹Shi -changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
²School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China

引用本文:

张子轩, 于金江, 刘金来. 镍基单晶高温合金DD432的持久性能各向异性[J]. 金属学报, 2023, 59(12): 1559-1567.
Zixuan ZHANG, Jinjiang YU, Jinlai LIU. Anisotropy of Stress Rupture Property of Ni Base Single Crystal Superalloy DD432[J]. Acta Metall Sin, 2023, 59(12): 1559-1567.

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摘要:

分别制备了偏离<001>、<011>及<111>取向的镍基单晶高温合金DD432样品，测定其在760℃、810 MPa和1000℃、280 MPa条件下的持久性能。结果表明，在760℃、810 MPa条件下3个取向的样品组织未发生明显筏化，具有明显的持久寿命各向异性，其中<111>取向样品的持久寿命最长，随着取向偏离角度的增加，持久寿命逐渐降低；<001>取向样品的持久寿命较低，且随着取向偏离角度的增大而增长；而<011>取向样品的持久性能最低，随着取向偏离角度的增加持久性能也有所提升。在1000℃、280 MPa条件下3个取向样品的组织都明显筏化，且筏化组织差异明显，持久性能各向异性有所下降但仍然存在，<111>取向样品的持久性能较<001>取向样品略好，<011>取向样品的持久性能虽然有所提升但依然最差。随着取向偏离角度的变化持久寿命仍然存在差异，但没有表现出明显的线性规律。

关键词 ：镍基单晶高温合金, 持久性能, 各向异性

Abstract：

Ni base superalloys have been extensively used in advanced aeroengine. With the development of modern aviation industry, high demands are being placed on the comprehensive performance of Ni base superalloys at high temperatures. To meet this demand, numerous refractory alloy elements are added to Ni base superalloys. However, in this way, the temperature bearing capacity of the alloy is enhanced, while the microstructure stability is reduced. Therefore, some scholars proposed to develop single crystal blades with various orientations through the anisotropy of a single crystal alloy. The stress rupture anisotropies of a Ni base single crystal superalloy DD432 under 760^oC, 810 MPa and 1000^oC, 280 MPa have been investigated in this study. The stress rupture properties of Ni base single crystal superalloy DD432 that deviated from <001>, <011>, and <111> with certain degrees were measured. It is discovered that rafting does not occur in specimens with three orientations, and the stress rupture life anisotropy of specimens is visible at 760^oC and 810 MPa. Furthermore, the stress rupture life of specimens with <111> orientation is the best, and as the orientation deviation degree increases, the stress rupture life gradually decreases. The stress rupture property of specimens with <001> orientation is lower than that of specimens with <111> orientation, and the stress rupture life increases with increasing orientation deviation degree. The creep resistance of specimens with <011> orientation is the lowest, and the stress rupture property is also enhanced as the orientation deviation degree increases. Rafting occurred in all the specimens with three orientations under the conditions of 1000^oC and 280 MPa, and the stress rupture property anisotropy of specimens decreased, but still existed. The stress rupture property of specimens with <111> orientation was slightly better than that of specimens with <001> orientation, and the stress rupture property of specimens with <011> orientation was still the worst, although it improved. A difference still exists in the stress rupture life as the degree of orientation deviation changes. However, there is no visible linear tendency.

Key words： Ni base single crystal superalloy stress rupture property anisotropy

收稿日期: 2022-03-11

ZTFLH:

TG113.25

基金资助:国家自然科学基金项目(51971214)

通讯作者: 于金江，jjyu@imr.ac.cn，主要从事镍基高温合金性能研究

作者简介: 张子轩，男，1994年生，硕士生

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图1 <001>、<011>和<111> 3个取向镍基单晶高温合金横截面铸态组织的OM像

图2 760℃、810 MPa条件下持久寿命随取向偏离角度变化统计图

图3 1000℃、280 MPa条件下持久寿命随取向偏离角度变化统计图

表1 760℃、810 MPa条件下3种取向样品拉伸蠕变的延伸率

表2 1000℃、280 MPa条件下3种取向样品拉伸蠕变的延伸率

图4 <001>、<011>和<111>取向样品的蠕变曲线

图5 1000℃、280 MPa持久样品在铸造孔洞处的裂纹扩展

图6 3种取向样品在不同条件下蠕变断裂后显微组织的SEM像

图7 <001>取向1000℃、280 MPa持久样品微裂纹形貌的SEM像

图8 <011>和<111>取向样品在不同条件下蠕变断裂位错组态的TEM像

1	Jiang K H, Chen J W, Jing F L, et al. Thermomechanical fatigue on the nickel based single crystal superalloy DD6 with film cooling hole[J]. J. Aerosp. Power, 2019, 34: 980
1	蒋康河, 陈竞炜, 荆甫雷等. 镍基单晶高温合金DD6气膜孔热机械疲劳试验[J]. 航空动力学报, 2019, 34: 980
2	Gell M, Duhl D N, Giamei A F. The development of single crystal superalloy turbine blades[A]. Superalloys[C]. Champion, PA: TMS, 1980: 205
3	Sun X F, Jin T, Zhou Y Z, et al. Research progress of nickel-base single crystal superalloys[J]. Mater. China, 2012, 31(12): 1
3	孙晓峰, 金涛, 周亦胄等. 镍基单晶高温合金研究进展[J]. 中国材料进展, 2012, 31(12): 1
4	Gui Z L. Research status of anisotropy of Russian single crystal superalloys[J]. Aeronaut. Manufact. Eng., 1997, (1): 20
4	桂忠楼. 俄罗斯单晶高温合金各向异性的研究现状[J]. 航空制造工程, 1997, (1): 20
5	Rae C M F, Reed R C. Primary creep in single crystal superalloys: Origins, mechanisms and effects[J]. Acta Mater., 2007, 55: 1067 doi: 10.1016/j.actamat.2006.09.026
6	Matan N, Cox D C, Carter P, et al. Creep of CMSX-4 superalloy single crystals: Effects of misorientation and temperature[J]. Acta Mater., 1999, 47: 1549 doi: 10.1016/S1359-6454(99)00029-4
7	Bai L. Creep behavior and constitutive modeling of single crystal nickel-base superalloys[D]. Beijing: Beihang University, 2010
7	白露. 镍基单晶合金高温蠕变行为及其本构理论研究[D]. 北京: 北京航空航天大学, 2010
8	Yu J, Li J R, Han M, et al. Anisotropy of stress rupture properties of DD6 single crystal superalloy at 980^oC/250 MPa near orientation [001][J]. J. Mater. Eng., 2012, (4): 1
8	喻健, 李嘉荣, 韩梅等. 近[001]取向DD6单晶高温合金980℃/250 MPa持久性能各向异性研究[J]. 材料工程, 2012, (4): 1
9	Hu B, Li S S, Pei Y L, et al. Influence of small misorientation from <111> on creep properties of a Ni-based single crystal superalloy[J]. Acta Metall. Sin., 2019, 55: 1204
9	胡斌, 李树索, 裴延玲等. <111>取向小角偏离对一种镍基单晶高温合金蠕变性能的影响[J]. 金属学报, 2019, 55: 1204
10	Xu J H, Li L F, Liu X G, et al. Thermal-stress coupling effect on microstructure evolution of a fourth-generation nickel-based single-crystal superalloy at 1100^oC[J]. Acta Metall. Sin., 2021, 57: 205
10	徐静辉, 李龙飞, 刘心刚等. 热力耦合对一种第四代镍基单晶高温合金1100℃蠕变组织演变的影响[J]. 金属学报, 2021, 57: 205
11	Han G M. Investigation of anisotropic stress rupture, creep and thermo-mechanical fatigue properties of SRR99 alloy[D]. Shenyang: Institute of Metal Research, Chinese Academy of Sciences, 2010
11	韩国明. SRR99合金持久蠕变各向异性行为及热机械疲劳性能的研究article-title>[D]. 沈阳: 中国科学院金属研究所, 2010
12	Liu J L. Tensile property and stress rupture property and microstructure evolution of a nickel base single crystal superalloy[D]. Shenyang: Institute of Metal Research, Chinese Academy of Sciences, 2002
12	刘金来. 一种镍基单晶高温合金的拉伸、持久性能及组织演化[D]. 沈阳: 中国科学院金属研究所, 2002
13	Knowles D M, Chen Q Z. Superlattice stacking fault formation and twinning during creep in γ/γ' single crystal superalloy CMSX-4[J]. Mater. Sci. Eng., 2003, A340: 88
14	Sui T X, Shi D Q, Wang X P, et al. Analysis on the stress rupture properties' anisotropy of single crystal superalloy[J]. J. Aerosp. Power, 2021, 36: 1286
14	隋天校, 石多奇, 王相平等. 单晶高温合金持久性能各向异性分析[J]. 航空动力学报, 2021, 36: 1286
15	Rae C M F, Matan N, Reed R C. The role of stacking fault shear in the primary creep of [001]-oriented single crystal superalloys at 750^oC and 750 MPa[J]. Mater. Sci. Eng., 2001, A300: 125
16	Rae C M F, Matan N, Cox D C, et al. On the primary creep of CMSX-4 superalloy single crystals[J]. Metall. Mater. Trans., 2000, 31A: 2219
17	Peng Z, Glatzel U, Link T, et al. Change of phase morpholigies during creep of CMSX-4 at 1253 K[J]. Scr. Mater., 1996, 34: 221 doi: 10.1016/1359-6462(95)00510-2
18	Caron P, Ohta Y, Nakagawa Y G, et al. Creep deformation anisotropy in single crystal superalloys[A]. Superalloys[C]. Warrendale, PA: TMS, 1988: 215
19	Sass V, Feller-Kniepmeier M. Orientation dependence of dislocation structures and deformation mechanisms in creep deformed CMSX-4 single crystals[J]. Mater. Sci. Eng., 1998, A245: 19
20	Feller-Kniepmeier M, Kuttner T. [011] creep in a single crystal nickel base superalloy at 1033 K[J]. Acta Metall. Mater., 1994, 42: 3167 doi: 10.1016/0956-7151(94)90415-4
21	Kakehi K. Influence of secondary precipitates and crystallographic orientation on the strength of single crystals of a Ni-based superalloy[J]. Metall. Mater. Trans., 1999, 30A: 1249
22	Liu J L, Jin T, Sun X F, et al. Anisotropy of stress rupture properties of a Ni base single crystal superalloy at two temperatures[J]. Mater. Sci. Eng., 2008, A479: 277
23	Mackay R A, Maier R D. The influence of orientation on the stress rupture properties of nickel-base superalloy single crystals[J]. Metall. Trans., 1982, 13A: 1747
24	Wang X G, Liu J L, Jin T, et al. Creep deformation related to dislocations cutting the γ' phase of a Ni-base single crystal superalloy[J]. Mater. Sci. Eng., 2015, A626: 406
25	Yan H J, Tian S G, Zhu X J, et al. Stacking fault energies of single crystal nickel-based superalloy and its influence on creep mechanism[J]. J. Mater. Eng., 2018, 46(10): 87
25	闫化锦, 田素贵, 朱新杰等. 单晶镍基合金的层错能及其对蠕变机制的影响[J]. 材料工程, 2018, 46(10): 87 doi: 10.11868/j.issn.1001-4381.2016.000711
26	Link T, Epishin A, Fedelich B. Inhomogeneity of misfit stresses in nickel-base superalloys: Effect on propagation of matrix dislocation loops[J]. Philos. Mag., 2009, 89: 1141 doi: 10.1080/14786430902877810
27	Field R D, Pollock T M, Murphy W H. The development of γ/γ' interfacial dislocation networks during creep in Ni-base superalloys[A]. Superalloys 1988[C]. Champaign: The Minerals, Metals & Materials Society (TMS), 1992: 557

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