Please wait a minute...
Acta Metall Sin  2022, Vol. 58 Issue (11): 1519-1526    DOI: 10.11900/0412.1961.2022.00354
Research paper Current Issue | Archive | Adv Search |
Strong and Tough Heterogeneous TWIP Steel Fabricated by Warm Rolling
HU Chen1,2, PAN Shuai1,3, HUANG Mingxin1,2()
1.Department of Mechanical Engineering, The University of Hong Kong, Hong Kong 999077, China
2.Shenzhen Institute of Research and Innovation, The University of Hong Kong, Shenzhen 518057, China
3.Department of Mechanical and Energy Engineering, Southern University of Science and Technology, Shenzhen 518055, China
Cite this article: 

HU Chen, PAN Shuai, HUANG Mingxin. Strong and Tough Heterogeneous TWIP Steel Fabricated by Warm Rolling. Acta Metall Sin, 2022, 58(11): 1519-1526.

Download:  HTML  PDF(4203KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

Twinning-induced plasticity (TWIP) steel has received significant research attention because of its superior mechanical properties, including uniform elongation, ultimate tensile strength, and fracture toughness. However, it has a relatively low yield stress, which limits its industrial application. Increasing the dislocation density has been proved to be an effective method for enhancing the yield stress. In this work, a simple warm rolling (WR) route was applied at 700oC to manufacture partially recrystallized TWIP steel with a high yield stress (1250 MPa), good total elongation (24%), and exceptional fracture toughness (KJIC of approximately 125 MPa·m1/2). The steel manufactured using WR was characterized using SEM, EBSD, and TEM at different length scales. Compared to the steel microstructure obtained after hot rolling or cold rolling (CR), this WR TWIP steel exhibits a distinct heterogeneous structure. The matrix has numerous dislocations with twinned coarse grains (approximately 75%) and nearly defect-free recrystallized fine grains (approximately 25%), which form during the reheating period of the WR process. The in situ tensile tests of the WR and CR steels show that the deformed coarse grains provide high yield stress with negligible deformation, whereas the recrystallized fine grains can undergo considerable plastic deformation, which results in a good work hardening capacity during tensile deformation. The fracture toughness tests of the compact tension (C(T)) samples indicate that the recrystallized grains in the WR steel can enhance the crack tip blunting and deflect cracks, which enhance the crack-growth resistance. Alternatively, these toughening mechanisms are not observed in the homogeneous CR steel. Therefore, this heterogeneous structure, which is induced by the high temperature WR process, provides the TWIP steel with excellent strength and toughness.

Key words:  TWIP steel      warm rolling      partial recrystallization      fracture toughness      heterogeneous structure      hetero-deformation induced strengthening     
Received:  25 July 2022     
ZTFLH:  TG142.1  
Fund: National Natural Science Foundation of China(52130102);National Key Research and Development Program of China(2019YFA0209900);Research Grants Council of Hong Kong(R7066-18);Guangzhou Municipal Science and Technology Bureau Program(202007020007);Guangdong Basic and Applied Basic Research Foundation of China(2020B1515130007)
About author:  HUANG Mingxin, professor, Tel: (00852)39177906, E-mail: mxhuang@hku.hk

URL: 

https://www.ams.org.cn/EN/10.11900/0412.1961.2022.00354     OR     https://www.ams.org.cn/EN/Y2022/V58/I11/1519

Fig.1  Inverse pole figures (IPFs) (a, d), phase maps with twinning boundaries (TBs) (b, e), and grain misorientation maps (c, f) of Hetero-T (a-c) and Homo-T (d-f)
Fig.2  Bright-field (a) and dark-field (b) TEM images, selected area electron diffraction (SAED) pattern (c), and STEM image (d) of recrystallized grains inside Hetero-T; bright-field (e) and dark-field (f) TEM images, and SAED pattern (g) of Homo-T (The matrix (M) and twin (T) diffraction patterns are shown by solid red and dash blue lines, respectively, and the corresponding indexes are shown in red and blue numbers in Figs.2c and g)
Fig.3  Engineering stress-strain curves (a), the loading-unloading-reloading hysteresis loops (b), J-R curves of Homo-T and Hetero-T (c), and tensile fracture surfaces of Hetero-T (d) and Homo-T (e) (J—measured J-integral, R—crack extension resistance, JICJ-integral at crack extension of 0.2 mm, KJIC—plane-strain crack-initiation fracture toughness calculated by JIC, J1mmJ-integral at crack extension of 1 mm, KJ1mm—crack-growth fracture toughness calculated by J1mm, E—elastic modulus, μ—Poisson's ratio)
SampleJIC / (kJ·m-2)KJIC / (MPa·m1/2)J1mm / (kJ·m-2)KJ1mm / (MPa·m1/2)
Hetero-T71.3125.2163.9189.8
Homo-T45.7100.273.4127.0
Table 1  Fracture toughness values of Hetero-T and Homo-T
Fig.4  IPFs (a, e) and KAM figures (b, f) before deforming, KAM figures at strains of 4% (c, g) and 12% (d, h), the full map KAM evolution with strain (i, k), and KAM evolutions of selected areas (white selected areas) with strain (j, l) of the Hetero-T (a-d, i, j) and Homo-T (e-h, k, l)
Fig.5  BSE images of the crack tips (a, c) and crack growth paths (b, d) of Hetero-T (a, b) and Homo-T (c, d)
1 Luo Z C, Liu R D, Wang X, et al. The effect of deformation twins on the quasi-cleavage crack propagation in twinning-induced plasticity steels [J]. Acta Mater., 2018, 150: 59
doi: 10.1016/j.actamat.2018.03.004
2 Tian Y Z, Bai Y, Zhao L J, et al. A novel ultrafine-grained Fe-22Mn-0.6C TWIP steel with superior strength and ductility [J]. Mater. Charact., 2017, 126: 74
doi: 10.1016/j.matchar.2016.12.026
3 Luo Z C, Huang M X. Revisit the role of deformation twins on the work-hardening behaviour of twinning-induced plasticity steels [J]. Scr. Mater., 2018, 142: 28
doi: 10.1016/j.scriptamat.2017.08.017
4 Liang Z Y, Li Y Z, Huang M X. The respective hardening contributions of dislocations and twins to the flow stress of a twinning-induced plasticity steel [J]. Scr. Mater., 2016, 112: 28
doi: 10.1016/j.scriptamat.2015.09.003
5 Zhou P, Liang Z Y, Liu R D, et al. Evolution of dislocations and twins in a strong and ductile nanotwinned steel [J]. Acta Mater., 2016, 111: 96
doi: 10.1016/j.actamat.2016.03.057
6 Li Y Z, Liang Z Y, Huang M X. Strengthening contributions of dislocations and twins in warm-rolled TWIP steels [J]. Int. J. Plast., 2022, 150: 103198
doi: 10.1016/j.ijplas.2021.103198
7 Ritchie R O. The conflicts between strength and toughness [J]. Nat. Mater., 2011, 10: 817
doi: 10.1038/nmat3115 pmid: 22020005
8 Xiong L, You Z S, Lu L. Enhancing fracture toughness of nanotwinned austenitic steel by thermal annealing [J]. Scr. Mater., 2016, 119: 55
doi: 10.1016/j.scriptamat.2016.03.024
9 Liu L, Yu Q, Wang Z, et al. Making ultrastrong steel tough by grain-boundary delamination [J]. Science, 2020, 368: 1347
doi: 10.1126/science.aba9413 pmid: 32381592
10 Gludovatz B, Hohenwarter A, Catoor D, et al. A fracture-resistant high-entropy alloy for cryogenic applications [J]. Science, 2014, 345: 1153
doi: 10.1126/science.1254581 pmid: 25190791
11 Gludovatz B, Hohenwarter A, Thurston K V S, et al. Exceptional damage-tolerance of a medium-entropy alloy CrCoNi at cryogenic temperatures [J]. Nat. Commun., 2016, 7: 10602
doi: 10.1038/ncomms10602 pmid: 26830651
12 Baik S I, Ahn T Y, Hong W P, et al. In situ observations of transgranular crack propagation in high-manganese steel [J]. Scr. Mater., 2015, 100: 32
doi: 10.1016/j.scriptamat.2014.12.005
13 Zhang J L, Raabe D, Tasan C C. Designing duplex, ultrafine-grained Fe-Mn-Al-C steels by tuning phase transformation and recrystallization kinetics [J]. Acta Mater., 2017, 141: 374
doi: 10.1016/j.actamat.2017.09.026
14 Wu X L, Yang M X, Yuan F P, et al. Heterogeneous lamella structure unites ultrafine-grain strength with coarse-grain ductility [J]. Proc. Natl. Acad. Sci. USA, 2015, 112: 14501
doi: 10.1073/pnas.1517193112
15 Yang M X, Yan D S, Yuan F P, et al. Dynamically reinforced heterogeneous grain structure prolongs ductility in a medium-entropy alloy with gigapascal yield strength [J]. Proc. Natl. Acad. Sci. USA, 2018, 115: 7224
doi: 10.1073/pnas.1807817115
16 Guo F J, Wang Y F, Wang M S, et al. Hetero-deformation induced strengthening and toughening of pure iron with inverse and multi-gradient structures [J]. Mater. Sci. Eng., 2020, A782: 139256
17 Liu X L, Xue Q Q, Wang W, et al. Back-stress-induced strengthening and strain hardening in dual-phase steel [J]. Materialia, 2019, 7: 100376
doi: 10.1016/j.mtla.2019.100376
18 Wu X L, Zhu Y T. Heterogeneous materials: A new class of materials with unprecedented mechanical properties [J]. Mater. Res. Lett., 2017, 5: 527
doi: 10.1080/21663831.2017.1343208
19 Yang M X, Pan Y, Yuan F P, et al. Back stress strengthening and strain hardening in gradient structure [J]. Mater. Res. Lett., 2016, 4: 145
doi: 10.1080/21663831.2016.1153004
20 Xiong L, You Z S, Qu S D, et al. Fracture behavior of heterogeneous nanostructured 316L austenitic stainless steel with nanotwin bundles [J]. Acta Mater., 2018, 150: 130
doi: 10.1016/j.actamat.2018.02.065
21 Garcia-mateo C, Caballero F G. Ultra-high-strength bainitic steels [J]. ISIJ Int., 2005, 45: 1736
doi: 10.2355/isijinternational.45.1736
22 Pawel J E, Alexander D J, Grossbeck M L, et al. Fracture toughness of candidate materials for ITER first wall, blanket, and shield structures [J]. J. Nucl. Mater., 1994, 212-215: 442
doi: 10.1016/0022-3115(94)90101-5
23 Linaza M A, Romero J L, Rodríguez-Ibabe J M, et al. Improvement of fracture toughness of forging steels microalloyed with titanium by accelerated cooling after hot working [J]. Scr. Metall. Mater., 1993, 29: 1217
doi: 10.1016/0956-716X(93)90112-6
24 He Y, Yang K, Qu W S, et al. Strengthening and toughening of a 2800-MPa grade maraging steel [J]. Mater. Lett., 2002, 56: 763
doi: 10.1016/S0167-577X(02)00610-9
25 Bayram A, Uǧuz A, Ula M. Effects of microstructure and notches on the mechanical properties of dual-phase steels [J]. Mater. Charact., 1999, 43: 259
doi: 10.1016/S1044-5803(99)00044-3
26 Cao Z H, Zhang B N, Huang M X. Comparing hydrogen embrittlement behaviors of two press hardening steels: 2 GPa vs. 1.5 GPa grade [J]. J. Mater. Sci. Technol., 2022, 124: 109
doi: 10.1016/j.jmst.2022.02.020
27 Wu R M, Li W, Zhou S, et al. Effect of retained austenite on the fracture toughness of quenching and partitioning (Q&P)-treated sheet steels [J]. Metall. Mater. Trans., 2014, 45A: 1892
[1] SI Yongli, XUE Jintao, WANG Xingfu, LIANG Juhua, SHI Zimu, HAN Fusheng. Effect of Cr Addition on the Corrosion Behavior of Twinning-Induced Plasticity Steel[J]. 金属学报, 2023, 59(7): 905-914.
[2] GU Ruicheng, ZHANG Jian, ZHANG Mingyang, LIU Yanyan, WANG Shaogang, JIAO Da, LIU Zengqian, ZHANG Zhefeng. Fabrication of Mg-Based Composites Reinforced by SiC Whisker Scaffolds with Three-Dimensional Interpenetrating-Phase Architecture and Their Mechanical Properties[J]. 金属学报, 2022, 58(7): 857-867.
[3] PENG Jun, JIN Xinyan, ZHONG Yong, WANG Li. Influence of Substrate Surface Structure on the Galvanizability of Fe-16Mn-0.7C-1.5Al TWIP Steel Sheet[J]. 金属学报, 2022, 58(12): 1600-1610.
[4] LIN Yan, SI Cheng, XU Jingyu, LIU Ze, ZHANG Cheng, LIU Lin. Heterogeneous Structure and Mechanical Properties of Strong and Tough Al Alloys Prepared by Selective Laser Melting[J]. 金属学报, 2022, 58(11): 1509-1518.
[5] CHEN Ruirun, CHEN Dezhi, WANG Qi, WANG Shu, ZHOU Zhecheng, DING Hongsheng, FU Hengzhi. Research Progress on Nb-Si Base Ultrahigh Temperature Alloys and Directional Solidification Technology[J]. 金属学报, 2021, 57(9): 1141-1154.
[6] LI Gen, LAN Peng, ZHANG Jiaquan. Solidification Structure Refinement in TWIP Steel by Ce Inoculation[J]. 金属学报, 2020, 56(5): 704-714.
[7] LI Yizhuang,HUANG Mingxin. A Method to Calculate the Dislocation Density of a TWIP Steel Based on Neutron Diffraction and Synchrotron X-Ray Diffraction[J]. 金属学报, 2020, 56(4): 487-493.
[8] LI Jinxu,WANG Wei,ZHOU Yao,LIU Shenguang,FU Hao,WANG Zheng,KAN Bo. A Review of Research Status of Hydrogen Embrittlement for Automotive Advanced High-Strength Steels[J]. 金属学报, 2020, 56(4): 444-458.
[9] Futao DONG,Fei XUE,Yaqiang TIAN,Liansheng CHEN,Linxiu DU,Xianghua LIU. Effect of Annealing Temperature on Microstructure, Properties and Hydrogen Embrittlement of TWIP Steel[J]. 金属学报, 2019, 55(6): 792-800.
[10] Dongdong LI, Lihe QIAN, Shuai LIU, Jiangying MENG, Fucheng ZHANG. Effect of Manganese Content on Tensile Deformation Behavior of Fe-Mn-C TWIP Steels[J]. 金属学报, 2018, 54(12): 1777-1784.
[11] Yizhe LI, Baoming GONG, Xiuguo LIU, Dongpo WANG, Caiyan DENG. Out-of-Plane Constraint Effect on the Fracture Toughness of Single Edge Notch Tension Specimens[J]. 金属学报, 2018, 54(12): 1785-1791.
[12] Xiangli FENG,Lei WANG,Yang LIU. STUDY ON MICROSTRUCTURE AND DYNAMIC FRACTURE BEHAVIOR OF Q460 STEEL WELDING JOINTS[J]. 金属学报, 2016, 52(7): 787-796.
[13] Xiaoyun YUAN, Liqing CHEN. EFFECT OF GRAIN AND GRAIN BOUNDARY FEATURESON ANTI-CORROSION ABILITY OF A HIGH MANGANESE AUSTENITIC TWIP STEEL[J]. 金属学报, 2016, 52(10): 1345-1352.
[14] Xiaoyun YUAN, Liqing CHEN. HOT DEFORMATION AT ELEVATED TEMPERATURE AND RECRYSTALLIZATION BEHAVIOR OF A HIGH MANGANESE AUSTENITIC TWIP STEEL[J]. 金属学报, 2015, 51(6): 651-658.
[15] SUN Chaoyang, GUO Xiangru, HUANG Jie, GUO Ning, WANG Shanwei, YANG Jing. MODELLING OF PLASTIC DEFORMATION ON COUPLING TWINNING OF SINGLE CRYSTAL TWIP STEEL[J]. 金属学报, 2015, 51(3): 357-363.
No Suggested Reading articles found!