Please wait a minute...
Acta Metall Sin  2018, Vol. 54 Issue (4): 494-500    DOI: 10.11900/0412.1961.2017.00274
Orginal Article Current Issue | Archive | Adv Search |
Study on Anisotropic Mechanical Properties of Cold Drawn Pearlitic Steel Wire
Peibei JI, Lichu ZHOU, Xuefeng ZHOU, Feng FANG(), Jianqing JIANG
School of Materials Science and Engineering, Southeast University, Nanjing 211189, China
Cite this article: 

Peibei JI, Lichu ZHOU, Xuefeng ZHOU, Feng FANG, Jianqing JIANG. Study on Anisotropic Mechanical Properties of Cold Drawn Pearlitic Steel Wire. Acta Metall Sin, 2018, 54(4): 494-500.

Download:  HTML  PDF(7898KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

Cold drawn pearlitic steel wires with ultra-high strength are widely applied in industrial fields such as bridge cables, automobile tire and springs rope. In recent years, the strengthening mechanism and microstructure evolution have been profoundly studied. In order to investigate the influence of microstructure evolution on mechanical properties, the anisotropic mechanical properties of cold drawn pearlitic steel wires were investigated by tensile test, SEM and TEM. Results indicated that the distinctions of tensile strength between three directions (parallel to the tensile axis, inclined to the tensile axis (45°), vertical to the tensile axis) were amplified with increasing strain. The effect of strain strengthening was observed in parallel and inclined directions while the vertical direction remained strength stability in 1320 MPa. The wire rod was isotropic and the fracture mode was transgranular fracture; After cold drawing, the tensile strength reached peaks in parallel direction and valleys in vertical direction. The fracture mechanism of inclined and vertical directions remained transgranular or intergranular fracture while the fracture mechanism of parallel direction was converted into microvoid accumulation fracture. In TEM, the phenomenon was discovered that due to non-homogeneous distribution in vertical direction, dislocations piled up at the boundaries resulting in stress concentration. On the contrary, the dislocations were uniformly distributed which led to homogeneous transformation in parallel direction.

Key words:  pearlitic steel wire      cold drawing      anisotropy      tensile strength     
Received:  05 July 2017     
ZTFLH:  TG142  
Fund: Supported by National Natural Science Foundation of China (No.51371050), Six Talent Peaks Program of Jiangsu Province (No.2015-XCL-004), Industry-University Strategic Research Fund of Jiangsu Province (No.BY2016076-08) and Key Research Project of Jiangsu Province (No.BE2015097)

URL: 

https://www.ams.org.cn/EN/10.11900/0412.1961.2017.00274     OR     https://www.ams.org.cn/EN/Y2018/V54/I4/494

Fig.1  Schematics of samples which is parallel to the tensile axis (P), 45°-inclined to the tensile axis (I) and vertical to the tensile axis (V)
Fig.2  Tensile strengths of the three directions (P, I and V) at different strains
Fig.3  Engineering stress-strain curves of three directions (P, I and V) at the strains of 0 (a), 0.6 (b) and 1.4 (c)
Fig.4  SEM images of cross-sections in pearlitic steel wire at the strains of 0 (a), 0.2 (b), 0.6 (c) and 1.4 (d)
Fig.5  TEM images of cross-sections in pearlitic steel wire at the strains of 0 (a), 0.6 (b) and 1.4 (c)
Fig.6  SEM images of cross-sections in fracture morphologies at different strains (ε)

(a) ε=0 (sample P) (b) ε=1.4 (sample P) (c) ε=1.4 (sample I) (d) ε=1.4 (sample V)

Fig.7  SEM images of fracture morphologies at ε=1.4

(a) near the fracture of sample P (b) away from the fracture of sample P (c) near the fracture of sample I (d) away from the fracture of sample I (crack propagation path) (e) away from the fracture of sample I (lamellar Fe3C) (f) away from the fracture of sample V

Fig.8  TEM images of cross-sections in fractures at ε=1.4

(a) bright field image of sample P (b) dark field image of sample P (c) bright field image of sample V

[1] Zelin M.Microstructure evolution in pearlitic steels during wire drawing[J]. Acta Mater., 2002, 50: 4431
[2] Li Y J, Choi P, Goto S, et al.Evolution of strength and microstructure during annealing of heavily cold-drawn 6.3 GPa hypereutectoid pearlitic steel wire[J]. Acta Mater., 2012, 60: 4005
[3] Read H G, Reynolds Jr W T, Hono K, et al. APFIM and TEM studies of drawn pearlitic wire[J]. Scr. Mater., 1997, 37: 1221
[4] Zhang X D, Godfrey A, Huang X X, et al.Microstructure and strengthening mechanisms in cold-drawn pearlitic steel wire[J]. Acta Mater., 2011, 59: 3422
[5] Embury J D, Fisher R M.The structure and properties of drawn pearlite[J]. Acta Metall., 1966, 14: 147
[6] Buono V T L, Gonzalez B M, Lima T M, et al. Measurement of fine pearlite interlamellar spacing by atomic force microscopy[J]. J. Mater. Sci., 1997, 32: 1005
[7] Zhou L C, Hu X J, Ma C, et al.Effect of pearlitic lamella orientation on deformation of pearlite steel wire during cold drawing[J]. Acta Metall. Sin., 2015, 51: 897(周立初, 胡显军, 马驰等. 珠光体层片取向对冷拔珠光体钢丝形变的影响[J]. 金属学报, 2015, 51: 897)
[8] Fang F, Zhao Y F, Liu P P, et al.Deformation of cementite in cold drawn pearlitic steel wire[J]. Mater. Sci. Eng., 2014, A608: 11
[9] Lamontagne A, Massardier V, Kléber X, et al.Comparative study and quantification of cementite decomposition in heavily drawn pearlitic steel wires[J]. Mater. Sci. Eng., 2015, A644: 105
[10] Li Y J, Choi P, Borchers C, et al.Atom probe tomography characterization of heavily cold drawn pearlitic steel wire[J]. Ultramicroscopy, 2011, 111: 628
[11] Li Y J, Choi P, Borchers C, et al.Atomic-scale mechanisms of deformation-induced cementite decomposition in pearlite[J]. Acta Mater., 2011, 59: 3965
[12] Zhou L C, Fang F, Zhou X F, et al.Cementite nano-crystallization in cold drawn pearlitic wires instigated by low temperature annealing[J]. Scr. Mater., 2016, 120: 5
[13] Li Y J, Raabe D, Herbig M, et al.Segregation stabilizes nanocrystalline bulk steel with near theoretical strength[J]. Phys. Rev. Lett., 2014, 113: 106104
[14] Fang F, Zhou L C, Hu X J, et al.Microstructure and mechanical properties of cold-drawn pearlitic wires affect by inherited texture[J]. Mater. Des., 2015, 79: 60
[15] Zhang X D, Godfrey A, Hansen N, et al.Hierarchical structures in cold-drawn pearlitic steel wire[J]. Acta Mater., 2013, 61: 4898
[16] Zhao T Z, Song H W, Zhang G L, et al.The texture evolution at the center of pearlitic steel wire during drawing and its influence on the mechanical properties[J]. Acta Metall. Sin., 2014, 50: 667(赵天章, 宋鸿武, 张光亮等. 拉拔过程中珠光体钢丝心部的织构演化规律及其对力学性能的影响[J]. 金属学报, 2014, 50: 667)
[17] Zhang X D, Godfrey A, Liu W, et al.Evolutions of microstructure and ferritic micro-orientation and texture in a pearlitic steel wire during cold drawing[J]. Acta Metall. Sin., 2010, 46: 141(张晓丹, Godfrey A, 刘伟等. 珠光体钢丝冷拉拔过程中微观组织及铁素体微区取向与织构演变[J]. 金属学报, 2010, 46: 141)
[18] Kapp M W, Hohenwarter A, Wurster S, et al.Anisotropic deformation characteristics of an ultrafine-and nanolamellar pearlitic steel[J]. Acta Mater., 2016, 106: 239
[19] Kammerhofer C, Hohenwarter A, Scheriau S, et al.Influence of morphology and structural size on the fracture behavior of a nanostructured pearlitic steel[J]. Mater. Sci. Eng., 2013, A585: 190
[20] Hohenwarter A, Taylor A, Stock R, et al.Effect of large shear deformations on the fracture behavior of a fully pearlitic steel[J]. Metall. Mater. Trans., 2011, 42A: 1609
[21] He Y, Xiang S, Shi W, et al.Effect of microstructure evolution on anisotropic fracture behaviors of cold drawing pearlitic steels[J]. Mater. Sci. Eng., 2017, A683: 153
[22] Toribio J, Ayaso F J.Anisotropic fracture behaviour of cold drawn steel: A materials science approach[J]. Mater. Sci. Eng., 2003, A343: 265
[23] Suzuki T, Tomota Y, Isaka M, et al.Strength anisotropy and residual stress in drawn pearlite steel wire[J]. ISIJ Int., 2004, 44: 1426
[24] Zhang X D, Hansen N, Godfrey A, et al.Dislocation-based plasticity and strengthening mechanisms in sub-20 nm lamellar structures in pearlitic steel wire[J]. Acta Mater., 2016, 114: 176
[25] Ju H L, Li B H, Wu Z F, et al.Perpendicular magnetic anisotropy in Co/Ni multilayers studied by anomalous Hall effect[J]. Acta Phys. Sin., 2015, 64: 097501(俱海浪, 李宝河, 吴志芳等. Co/Ni多层膜垂直磁各向异性的研究[J]. 物理学报, 2015, 64: 097501)
[26] Chen Z Y, Cai H N, Wang F C, et al.Investigation on anisotropy of dynamic compressive mechanical properties of cold-rolled Cu sheet[J]. Acta Metall. Sin., 2009, 45: 143(陈志永, 才鸿年, 王富耻等. 冷轧Cu板动态压缩力学性能各向异性的研究[J]. 金属学报, 2009, 45: 143)
[27] Xu Y B, Liu M Z.An in situ study of crack nucleation and propagation in pearlite during deformation[J]. Acta Metall. Sin., 1982, 18: 58(徐永波, 刘民治. 珠光体组织的形变、裂纹形核与扩展微观过程的动态研究[J]. 金属学报, 1982, 18: 58)
[1] ZHANG Zixuan, YU Jinjiang, LIU Jinlai. Anisotropy of Stress Rupture Property of Ni Base Single Crystal Superalloy DD432[J]. 金属学报, 2023, 59(12): 1559-1567.
[2] GE Jinguo, LU Zhao, HE Siliang, SUN Yan, YIN Shuo. Anisotropy in Microstructures and Mechanical Properties of 2Cr13 Alloy Produced by Wire Arc Additive Manufacturing[J]. 金属学报, 2023, 59(1): 157-168.
[3] GAO Yubi, DING Yutian, LI Haifeng, DONG Hongbiao, ZHANG Ruiyao, LI Jun, LUO Quanshun. Effect of Deformation Rate on the Elastic-Plastic Deformation Behavior of GH3625 Alloy[J]. 金属学报, 2022, 58(5): 695-708.
[4] LU Lei, ZHAO Huaizhi. Progress in Strengthening and Toughening Mechanisms of Heterogeneous Nanostructured Metals[J]. 金属学报, 2022, 58(11): 1360-1370.
[5] WANG Di, HUANG Jinhui, TAN Chaolin, YANG Yongqiang. Review on Effects of Cyclic Thermal Input on Microstructure and Property of Materials in Laser Additive Manufacturing[J]. 金属学报, 2022, 58(10): 1221-1235.
[6] BI Sheng, LI Zechen, SUN Haixia, SONG Baoyong, LIU Zhenyu, XIAO Bolv, MA Zongyi. Microstructure and Mechanical Properties of Carbon Nanotubes-Reinforced 7055Al Composites Fabricated by High-Energy Ball Milling and Powder Metallurgy Processing[J]. 金属学报, 2021, 57(1): 71-81.
[7] ZHANG Lin, GUO Xiao, GAO Jianwen, DENG Anyuan, WANG Engang. Effect of Electromagnetic Stirring on Microstructure and Mechanical Properties of TiB2 Particle-Reinforced Steel[J]. 金属学报, 2020, 56(9): 1239-1246.
[8] LIU Jinlai, YE Lihua, ZHOU Yizhou, LI Jinguo, SUN Xiaofeng. Anisotropy of Elasticity of a Ni Base Single Crystal Superalloy[J]. 金属学报, 2020, 56(6): 855-862.
[9] HU Bin,LI Shusuo,PEI Yanling,GONG Shengkai,XU Huibin. Influence of Small Misorientation from <111> on Creep Properties of a Ni-Based Single Crystal Superalloy[J]. 金属学报, 2019, 55(9): 1204-1210.
[10] Hanchen FENG,Xuegang MIN,Dasheng WEI,Lichu ZHOU,Shiyun CUI,Feng FANG. Effect of Low Temperature Annealing on Microstructure and Mechanical Properties of Ultra-Heavy Cold-DrawnPearlitic Steel Wires[J]. 金属学报, 2019, 55(5): 585-592.
[11] WANG Li,HE Yufeng,SHEN Jian,ZHENG Wei,LOU Langhong,ZHANG Jian. Effect of Secondary Orientation on Oxidation Anisotropy Around the Holes of Single Crystal Superalloy During Thermal Fatigue Tests[J]. 金属学报, 2019, 55(11): 1417-1426.
[12] HE Xianmei, TONG Liuniu, GAO Cheng, WANG Yichao. Effect of Nd Content on the Structure and Magnetic Properties of Si(111)/Cr/Nd-Co/Cr Thin Films Prepared by Magnetron Sputtering[J]. 金属学报, 2019, 55(10): 1349-1358.
[13] Ran TAO, Yutao ZHAO, Gang CHEN, Xizhou KAI. Microstructure and Properties of In-Situ ZrB2 np/AA6111 Composites Synthesized Under an Electromagnetic Field[J]. 金属学报, 2019, 55(1): 160-170.
[14] Xiaoqin MA, Qingfeng ZHAN, Jincai LI, Qingfang LIU, Baomin WANG, Runwei LI. Influence of Oblique Sputtering on Stripe Magnetic Domain Structure and Magnetic Anisotropy of CoFeB Thin Films[J]. 金属学报, 2018, 54(9): 1281-1288.
[15] Mingliang HUANG, Hongyu SUN. Interaction Between β-Sn Grain Orientation and Electromigration Behavior in Flip-Chip Lead-Free Solder Bumps[J]. 金属学报, 2018, 54(7): 1077-1086.
No Suggested Reading articles found!