EFFECT OF SURFACE NANOCRYSTALLIZATION ON MICROSTRUCTURE AND THERMAL STABILITY OF REDUCED ACTIVATION STEEL

doi:10.3724/SP.J.1037.2012.00742

Acta Metall Sin

2013, Vol. 49

Issue (6): 707-716 DOI: 10.3724/SP.J.1037.2012.00742

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EFFECT OF SURFACE NANOCRYSTALLIZATION ON MICROSTRUCTURE AND THERMAL STABILITY OF REDUCED ACTIVATION STEEL

LIU Wenbo¹⁾, ZHANG Chi¹⁾, YANG Zhigang¹⁾, XIA Zhixin²⁾, GAO Guhui¹⁾, WENG Yuqing³⁾

1) Key Laboratory of Advanced Materials of Ministry of Education, School of Materials Science and Engineering, Tsinghua University, Beijing 100084

2) Suzhou Nuclear Power Research Institute, Suzhou 215004

3) The Chinese Society for Metals, Beijing 100711

Cite this article:

LIU Wenbo, ZHANG Chi, YANG Zhigang, XIA Zhixin, GAO Guhui, WENG Yuqing. EFFECT OF SURFACE NANOCRYSTALLIZATION ON MICROSTRUCTURE AND THERMAL STABILITY OF REDUCED ACTIVATION STEEL. Acta Metall Sin, 2013, 49(6): 707-716.

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Abstract

Nanocrystalline grains in the surface of reduced activation ferrite/martensite(RAFM) steel were produced by means of surface mechanical attrition treatment (SMAT). Analysis results of XRD and TEM showed that grains after SMAT were nanocrystalline. Experiment results after annealing at 550℃ showed that the nanocrystallines were stable. Abnormal grain growth was observed from the TEM images after tempered for 120 min, and the grain sizes became uniform after tempered for 240 min (about 250 nm). The XRD diffraction peaks of carbides became weaker and boarder indicated that carbides in the surface layer became smaller after SMAT, and smaller MC type carbides were found from HRTEM images after SMAT. The lattice parameters of M₂₃C₆ and MC were 1.0631 and 0.4306 nm calculated from the XRD results. The differences of grain sizes obtained by XRD and TEM could be attributed to the different testing mechanism, different measuring depths and the depth-dependent nanocrystalline microstructure, and results obtained by TEM were more accurate to reveal the real grain size.

Key words: surface nanocrystallization thermal stability reduced activation steel, carbide decomposition

Received: 18 December 2012

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	LIU Wenbo
	ZHANG Chi
	YANG Zhigang
	XIA Zhixin
	GAO Guhui
	WENG Yuqing

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https://www.ams.org.cn/EN/10.3724/SP.J.1037.2012.00742 OR https://www.ams.org.cn/EN/Y2013/V49/I6/707

[1] Lu K, Lu L. Acta Metall Sin, 2000; 36: 785

(卢柯, 卢磊. 金属学报, 2000; 36: 785)

[2] Yong X P, Liu G, Lu J, Lu K. Acta Metall Sin, 2002; 38: 157

(雍兴平, 刘刚, 吕坚, 卢柯. 金属学报, 2002; 38: 157)

[3] Valiev R Z, Korznikov A V, Mulyukov R R, Mater Sci Eng, 1993; A168: 141

[4] Lu K, Lu J. Mater Sci Eng, 2004; A375-377: 38

[5] Lu K, Lu J. J Mater Sci Technol, 1999; 15: 193

[6] Wang H L, Wang Z B, Lu K. Acta Mater, 2012; 60: 1762

[7] Tao N R, Wang Z B, Tong W P, Sui M L, Lu J, Lu K. Acta Mater, 2002; 50: 4603

[8] Lu S D, Wang Z B, Lu K. J Mater Sci Technol, 2010; 26: 258

[9] Wang L M, Wang Z B, Lu K. Acta Mater, 2011; 59: 3710

[10] Li W, Xu W Z, Wang X D, Rong Y H. J Alloys Compd, 2009; 474: 546

[11] Ivanisenko Y, Lojkowski W, Valiev R Z, Fecht H J. Acta Mater, 2003; 51: 5555

[12] Nam W J, Bae C M, Oh S J, Kwon S J. Scr Mater, 2000; 42: 457

[13] Lanfuillaume J, Kapelski G, Baudelet B. Acta Mater, 1997; 45: 1201

[14] Gavriljuk V G. Mater Sci Eng, 2003; A345: 81

[15] Zhou L, Liu G, Ma X L, Lu K. Acta Mater, 2008; 56: 78

[16] Lojkowski W, Djahanbakhsh M, Burkle G, Gierlotka S, Zielinski W, Fecht H J. Mater Sci Eng, 2001; A303: 197

[17] Jo T S, Lim J H, Kim Y D. J Nucl Mater, 2010; 406: 360

[18] Huang Q Y, Yu J N, Wan F R, Li J G, Wu Y C. Chin J Nucl Eng, 2004; 24: 56

(黄群英, 郁金南, 万发荣, 李建刚, 吴宜灿. 核科学与工程, 2004; 24: 56)

[19] Jones R H, Heinisch H L, McCarthy K A. J Nucl Mater, 1999; 271--272: 518

[20] Xia Z X, Zhang C, Yang Z G. Acta Metall Sin, 2011; 47: 713

(夏志新, 张弛, 杨志刚. 金属学报, 2011; 47: 713)

[21] Bai X M, Voter A F, Hoagland R G, Nastasi M, Uberuaga B P. Science, 2010; 327: 1631

[22] Ackland G. Science, 2010; 327: 1587

[23] Klug H P, Alexander L E. X-ray Diffraction Procedures for Polycrystalline and Amorphous Materials. New York: Wiley, 1974: 662

[24] Feng G, Shi L J, Lu J, Lu K. Acta Metall Sin, 2000; 36: 300

(冯淦, 石连捷, 吕坚, 卢柯. 金属学报, 2000; 36: 300)

[25] Schiotz J, Tolla F D, Jacobsen K W. Nature, 1998; 391: 561

[26] Jeon J B, Lee B J, Chang Y W. Scr Mater, 2011; 64: 494

[27] Huang F, Tao N R, Lu K. J Mater Sci Technol, 2011; 27: 1

[28] Gavriljuk V. Scr Mater, 2002; 46: 175

[29] Ohsaki S, Hono H, Hidaka H, Takaki S. Scr Mater, 2005; 52: 271

[30] Sauvage X, Quelennec X, Malandain J J, Pareige P. Scr Mater, 2006; 54: 1099

[31] Liu W B, Zhang C, Xia Z X, Yang Z G, Wang P H, Chen J M.Mater Sci Eng, 2013; A568: 176

[32] Erdos E. Analysis of High Temperature Materials. London and New York: Applied Science Publishers, 1983: 204

[33] Franck F J, Tambuyser P, Zubani I. J Mater Sci, 1982; 17: 3057

[34] Song X Y, Zhang J X, Li L M, Yang K Y, Liu G Q. Acta Mater, 2006; 54: 5541

[35] Salati A, Panjepour M, Aryanpour G. J Phys Chem Solids, 2011; 72: 104

[36] Waniewska A S, Greneche J M. Phys Rev, 1997; 56B: 8491

[37] Meng Q, Zhou N, Rong Y, Chen S, Hsu T Y (Xu Z Y). Acta Mater, 2002; 50: 4563

[39] Pan J S, Tong J M, Tian M B. Fundamentals of Materials Science. Beijing: Tsinghua University Press,2004: 579

(潘金生, 仝健民, 田民波. 材料科学基础. 北京: 清华大学出版社, 2004: 579)

[38] Krill C E, Helfen L, Michels D, Natter H, Fitch A, Phys Rev Lett, 2001; 86: 842

[40] Ungar T, Tichy G, Gubicza J, Hellmig R J. Powder Diffr, 2005; 20: 366

[41] Ungar T, Gubicza J, Ribarik G, Borbely A. J Appl Crystallogr, 2001; 34: 298

[42] Zhu Y T, Huang J Y, Gubicza J, Ungar T, Wang Y M, Ma E, Valiev R Z. J Mater Res,2003; 18: 1908

[43] Malow T R, Koch C C. Acta Mater, 1997; 45: 2177

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