Please wait a minute...
Acta Metall Sin  2010, Vol. 46 Issue (9): 1075-1080    DOI: 10.3724/SP.J.1037.2010.00185
论文 Current Issue | Archive | Adv Search |
MICROSTRUCTURAL EVOLUTION OF DIRECTIONALLY SOLIDIFIED Ni-BASED SUPERALLOY DZ125 UNDER PLANAR GROWTH
MIN Zhixian, SHEN Jun, WANG Lingshui, FENG Zhourong, LIU Lin, FU Hengzhi
State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072
Cite this article: 

MIN Zhixian SHEN Jun WANG Lingshui FENG Zhourong LIU Lin FU Hengzhi. MICROSTRUCTURAL EVOLUTION OF DIRECTIONALLY SOLIDIFIED Ni-BASED SUPERALLOY DZ125 UNDER PLANAR GROWTH. Acta Metall Sin, 2010, 46(9): 1075-1080.

Download:  PDF(709KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

By using liquid metal cooling method, the Ni-based superalloy DZ125 was directionally solidified under planar interface growth condition of drawing rate of 1.5 μm/s. The microstructures at different solidified fractions were examined by OM and SEM. The results showed that the solid/liquid interface is planar and the microstructure evolution undergoes three stages: the γ phase was formed as solidified fraction (fs) was not more than 0.26, and the fine HfC phase sparsely distributed in γ matrix; the coupled γ/MC growth appeared as fs ranged from 0.26 to 0.86, and the morphology of MC was fibrous or plate-like shapes; the γ/γ´ eutectic was obtained as fs was more than and equaled 0.86 0.86, in which the octahedral MC was precipitated simultaneously. EPMA was used to determine the solute distribution along the longitudinal direction of the sample. The contents of Al, Ti, Ta and Mo increased with fs increasing, while the contents of W, Cr and Co decreased. The analysis showed that the microstructure transformation is attributed to macro-scale non-uniform solute distribution which resulted from solute redistribution during directional solidification.

Key words:  Ni-based superalloy      directional solidification      microstructure      solute distribution     
Received:  21 April 2010     
Fund: 

Supported by National Natural Science Foundation of China (No.50827102), National Basic Research Program of China (No.2010CB631202) and the Research Fund of State Key Laboratory of Solidification Processing (NWPU) (No.28-TP-2009)

URL: 

https://www.ams.org.cn/EN/10.3724/SP.J.1037.2010.00185     OR     https://www.ams.org.cn/EN/Y2010/V46/I9/1075

[1] Fu H Z. J Aeronaut Mater, 1998; 18(4): 52
(傅恒志. 航空材料学报, 1998; 18(4): 52)
[2] McLean M. Directionally Solidified Materials for High Temperature Service. UK: The Metals Society, 1983: 11
[3] Liu L, Huang T W, Zhang J, Fu H Z. Mater Lett, 2007; 61: 227
[4] Versnyder F I, Shank M E. Mater Sci Eng, 1970; A6: 213
[5] Tien J K, Gamble R P. Mater Sci Eng, 1971; A8: 152
[6] Bae J S, Lee J H, Kim S S, Jo C Y. Scr Mater, 2001; 45: 50
[7] Sellamuthu R, Giamei A F. Metall Mater Trans, 1986; 16A: 419
[8] Seo S M, Lee J H, Yoo Y S, Jo C Y, Miyahara H, Ogi K. In: Reed R C, Green K A, Caron P, Gabb T P, Fahrmann M G, Huron E S, Woodard S A. eds, Superalloys 2008, Warrendale, PA: TMS, 2008: 2773
[9] Stefanescu D M. Science and Engineering of Casting Solidification. New York: Kluwer Academic/Plenum Publishers, 2002: 33
[10] Trivedi R, Minyahara H, Mazumder P, Simsek E, Tewari S N. J Cryst Growth, 2001; 222: 365
[11] Tiller W A. Trans TMS–AIME, 1959; 215: 555
[12] Liu L, Sommer F, Fu H Z. Scr Metall Mater, 1994; 30: 584
[13] ZhangWG. PhD Thesis, Northwestern Polytechnical University, Xi’an, 2009
(张卫国. 西北工业大学博士论文, 西安, 2009)
[14] Li R J. Ceramic–Metal Composites. Beijing: Metallurgical Industry Press, 2004: 39
(李荣久. 陶瓷-金属复合材料, 北京: 冶金工业出版社, 2004: 39)
[15] Bhambri A K, Kattamis T Z, Morral J E. Metall Mater Trans, 1986; 6B: 523
[16] Chen J, Lee J H, Jo C Y, Choe S J, Lee Y T. Mater Sci Eng, 1998; A247: 113

[1] ZHANG Jian, WANG Li, XIE Guang, WANG Dong, SHEN Jian, LU Yuzhang, HUANG Yaqi, LI Yawei. Recent Progress in Research and Development of Nickel-Based Single Crystal Superalloys[J]. 金属学报, 2023, 59(9): 1109-1124.
[2] MA Dexin, ZHAO Yunxing, XU Weitai, WANG Fu. Effect of Gravity on Directionally Solidified Structure of Superalloys[J]. 金属学报, 2023, 59(9): 1279-1290.
[3] ZHENG Liang, ZHANG Qiang, LI Zhou, ZHANG Guoqing. Effects of Oxygen Increasing/Decreasing Processes on Surface Characteristics of Superalloy Powders and Properties of Their Bulk Alloy Counterparts: Powders Storage and Degassing[J]. 金属学报, 2023, 59(9): 1265-1278.
[4] WANG Lei, LIU Mengya, LIU Yang, SONG Xiu, MENG Fanqiang. Research Progress on Surface Impact Strengthening Mechanisms and Application of Nickel-Based Superalloys[J]. 金属学报, 2023, 59(9): 1173-1189.
[5] GONG Shengkai, LIU Yuan, GENG Lilun, RU Yi, ZHAO Wenyue, PEI Yanling, LI Shusuo. Advances in the Regulation and Interfacial Behavior of Coatings/Superalloys[J]. 金属学报, 2023, 59(9): 1097-1108.
[6] ZHANG Leilei, CHEN Jingyang, TANG Xin, XIAO Chengbo, ZHANG Mingjun, YANG Qing. Evolution of Microstructures and Mechanical Properties of K439B Superalloy During Long-Term Aging at 800oC[J]. 金属学报, 2023, 59(9): 1253-1264.
[7] LU Nannan, GUO Yimo, YANG Shulin, LIANG Jingjing, ZHOU Yizhou, SUN Xiaofeng, LI Jinguo. Formation Mechanisms of Hot Cracks in Laser Additive Repairing Single Crystal Superalloys[J]. 金属学报, 2023, 59(9): 1243-1252.
[8] LI Jingren, XIE Dongsheng, ZHANG Dongdong, XIE Hongbo, PAN Hucheng, REN Yuping, QIN Gaowu. Microstructure Evolution Mechanism of New Low-Alloyed High-Strength Mg-0.2Ce-0.2Ca Alloy During Extrusion[J]. 金属学报, 2023, 59(8): 1087-1096.
[9] MU Yahang, ZHANG Xue, CHEN Ziming, SUN Xiaofeng, LIANG Jingjing, LI Jinguo, ZHOU Yizhou. Modeling of Crack Susceptibility of Ni-Based Superalloy for Additive Manufacturing via Thermodynamic Calculation and Machine Learning[J]. 金属学报, 2023, 59(8): 1075-1086.
[10] CHEN Liqing, LI Xing, ZHAO Yang, WANG Shuai, FENG Yang. Overview of Research and Development of High-Manganese Damping Steel with Integrated Structure and Function[J]. 金属学报, 2023, 59(8): 1015-1026.
[11] LIU Xingjun, WEI Zhenbang, LU Yong, HAN Jiajia, SHI Rongpei, WANG Cuiping. Progress on the Diffusion Kinetics of Novel Co-based and Nb-Si-based Superalloys[J]. 金属学报, 2023, 59(8): 969-985.
[12] SUN Rongrong, YAO Meiyi, WANG Haoyu, ZHANG Wenhuai, HU Lijuan, QIU Yunlong, LIN Xiaodong, XIE Yaoping, YANG Jian, DONG Jianxin, CHENG Guoguang. High-Temperature Steam Oxidation Behavior of Fe22Cr5Al3Mo-xY Alloy Under Simulated LOCA Condition[J]. 金属学报, 2023, 59(7): 915-925.
[13] ZHANG Lu, YU Zhiwei, ZHANG Leicheng, JIANG Rong, SONG Yingdong. Thermo-Mechanical Fatigue Cycle Damage Mechanism and Numerical Simulation of GH4169 Superalloy[J]. 金属学报, 2023, 59(7): 871-883.
[14] FENG Aihan, CHEN Qiang, WANG Jian, WANG Hao, QU Shoujiang, CHEN Daolun. Thermal Stability of Microstructures in Low-Density Ti2AlNb-Based Alloy Hot Rolled Plate[J]. 金属学报, 2023, 59(6): 777-786.
[15] WU Dongjiang, LIU Dehua, ZHANG Ziao, ZHANG Yilun, NIU Fangyong, MA Guangyi. Microstructure and Mechanical Properties of 2024 Aluminum Alloy Prepared by Wire Arc Additive Manufacturing[J]. 金属学报, 2023, 59(6): 767-776.
No Suggested Reading articles found!