Acta Metall Sin  1996, Vol. 32 Issue (9): 921-925    DOI:

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SYNTHESIS OF TiN BY MICROWAVE CARBOTHERMAL REDUCTION OF TiO_2

LIU Binghai; OUYANG Shixi (State Key Laboratory for Synthesis and Processing of Advanced Materials; Wuhan University of Technology; Wuhan 430070); ZHANG Yue (University of Science and Technology Beijing; Beijing 100083)

LIU Binghai; OUYANG Shixi (State Key Laboratory for Synthesis and Processing of Advanced Materials; Wuhan University of Technology; Wuhan 430070); ZHANG Yue (University of Science and Technology Beijing; Beijing 100083). SYNTHESIS OF TiN BY MICROWAVE CARBOTHERMAL REDUCTION OF TiO_2. Acta Metall Sin, 1996, 32(9): 921-925.

Abstract References Related Articles Recommended Metrics Download:  PDF(353KB)  Export:  BibTeX | EndNote (RIS)       Abstract  The possibility of manufacture of titanium nitride by microwave carbothermal reduction of titanium oxide was discussed. The mechanism and thermal dynamics of the reaction process was also studied. The resuls showed that the technology has unique advantages compared with the conventional carbothermal reduction method, for example it can not only lower the reaction temperature, shorten the synthesis cycle, but also can refine the powder particles, so the reactivity of the powder is improved. Key words:  TiN      microwave heating      carbothermal reduction      Received:  18 September 1996      Service E-mail this article Add to citation manager E-mail Alert RSS （） Articles by authors URL:  https://www.ams.org.cn/EN/     OR     https://www.ams.org.cn/EN/Y1996/V32/I9/921 1李世普．特种陶瓷工艺学．武汉:武汉工业大学出版社,1990:1412WicksCE,BlockFE．USBurMinesBull,1963:6053WhiteGV,RyanMJ,MackenzieKJD,JohnstonJH．CeramicDevelopment,1988;34-36:6574程吉平．武汉工业大学博士学位论文,1989 [1] ZHENG Liang, ZHANG Qiang, LI Zhou, ZHANG Guoqing. Effects of Oxygen Increasing/Decreasing Processes on Surface Characteristics of Superalloy Powders and Properties of Their Bulk Alloy Counterparts: Powders Storage and Degassing[J]. 金属学报, 2023, 59(9): 1265-1278. [2] DU Jinhui, BI Zhongnan, QU Jinglong. Recent Development of Triple Melt GH4169 Alloy[J]. 金属学报, 2023, 59(9): 1159-1172. [3] LI Jiarong, DONG Jianmin, HAN Mei, LIU Shizhong. Effects of Sand Blasting on Surface Integrity and High Cycle Fatigue Properties of DD6 Single Crystal Superalloy[J]. 金属学报, 2023, 59(9): 1201-1208. [4] CHEN Jia, GUO Min, YANG Min, LIU Lin, ZHANG Jun. Effects of W Concentration on Creep Microstructure and Property of Novel Co-Based Superalloys[J]. 金属学报, 2023, 59(9): 1209-1220. [5] GONG Shengkai, LIU Yuan, GENG Lilun, RU Yi, ZHAO Wenyue, PEI Yanling, LI Shusuo. Advances in the Regulation and Interfacial Behavior of Coatings/Superalloys[J]. 金属学报, 2023, 59(9): 1097-1108. [6] ZHANG Qiliang, WANG Yuchao, LI Guangda, LI Xianjun, HUANG Yi, XU Yunze. Erosion-Corrosion Performance of EH36 Steel Under Sand Impacts of Different Particle Sizes[J]. 金属学报, 2023, 59(7): 893-904. [7] YUAN Jianghuai, WANG Zhenyu, MA Guanshui, ZHOU Guangxue, CHENG Xiaoying, WANG Aiying. Effect of Phase-Structure Evolution on Mechanical Properties of Cr2AlC Coating[J]. 金属学报, 2023, 59(7): 961-968. [8] HOU Juan, DAI Binbin, MIN Shiling, LIU Hui, JIANG Menglei, YANG Fan. Influence of Size Design on Microstructure and Properties of 304L Stainless Steel by Selective Laser Melting[J]. 金属学报, 2023, 59(5): 623-635. [9] FENG Li, WANG Guiping, MA Kai, YANG Weijie, AN Guosheng, LI Wensheng. Microstructure and Properties of AlCo x CrFeNiCu High-Entropy Alloy Coating Synthesized by Cold Spraying Assisted Induction Remelting[J]. 金属学报, 2023, 59(5): 703-712. [10] HUANG Ding, QIAO Yanxin, YANG Lanlan, WANG Jinlong, CHEN Minghui, ZHU Shenglong, WANG Fuhui. Effect of Shot Peening of Substrate Surface on Cyclic Oxidation Behavior of Sputtered Nanocrystalline Coating[J]. 金属学报, 2023, 59(5): 668-678. [11] ZHANG Dongyang, ZHANG Jun, LI Shujun, REN Dechun, MA Yingjie, YANG Rui. Effect of Heat Treatment on Mechanical Properties of Porous Ti55531 Alloy Prepared by Selective Laser Melting[J]. 金属学报, 2023, 59(5): 647-656. [12] WANG Jingyang, SUN Luchao, LUO Yixiu, TIAN Zhilin, REN Xiaomin, ZHANG Jie. Rare Earth Silicate Environmental Barrier Coating Material: High-Entropy Design and Resistance to CMAS Corrosion[J]. 金属学报, 2023, 59(4): 523-536. [13] WANG Di, HE Lili, WANG Dong, WANG Li, ZHANG Siqian, DONG Jiasheng, CHEN Lijia, ZHANG Jian. Influence of Pt-Al Coating on Tensile Properties of DD413 Alloy at High Temperatures[J]. 金属学报, 2023, 59(3): 424-434. [14] XIA Dahai, JI Yuanyuan, MAO Yingchang, DENG Chengman, ZHU Yu, HU Wenbin. Localized Corrosion Mechanism of 2024 Aluminum Alloy in a Simulated Dynamic Seawater/Air Interface[J]. 金属学报, 2023, 59(2): 297-308. [15] LI Dou, XU Changjiang, LI Xuguang, LI Shuangming, ZHONG Hong. Thermoelectric Properties of P-Type CeyFe3CoSb12 Thermoelectric Materials and Coatings Doped with La[J]. 金属学报, 2023, 59(2): 237-247. No Suggested Reading articles found! Viewed Full text Abstract Cited   Shared      Discussed