Please wait a minute...
Acta Metall Sin  2015, Vol. 51 Issue (9): 1025-1037    DOI: 10.11900/0412.1961.2015.00127
Current Issue | Archive | Adv Search |
STUDY ON TENSILE BEHAVIOR OF SiCf/TC17 COMPOSITES
Xu ZHANG,Yumin WANG(),Qing YANG,Jiafeng LEI,Rui YANG
Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016
Cite this article: 

Xu ZHANG, Yumin WANG, Qing YANG, Jiafeng LEI, Rui YANG. STUDY ON TENSILE BEHAVIOR OF SiCf/TC17 COMPOSITES. Acta Metall Sin, 2015, 51(9): 1025-1037.

Download:  HTML  PDF(16436KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

Tensile properties and fracture mechanisms of SiCf/TC17 composites at room temperature and 773 K were studied. The results show that fiber elastic deformation and matrix yielding contributed to the shapes of the stress-strain curves of SiCf/TC17 composites, which were the bilinear appearance at 298 K and the slight curvature at 773 K. Major fracture mechanism of SiCf/TC17 composites at room temperature were as follows: multiple fractures of the interfacial reaction layer, single fiber fracture, matrix brittle fracture etc.. Typical fracture mechanism of SiCf/TC17 composites at elevated temperature were as follows: multiple fiber fracture, matrix plastic fracture, interface debonding etc.. Fiber cumulating damage theory was proved to be suitable for estimation of the fracture strength of this composite. The calculations of local loading sharing model while taking three or more fibers failure into account and global loading sharing model were close to the experimental values of room temperature and elevated temperature respectively. In addition, according to fracture mechanisms and strength prediction, tensile fracture process of SiCf/TC17 composites at room and elevated temperature were explained in detail. At room temperature, multiple fractures of the interfacial reaction layer started at first, and then the weak fiber fractured gradually and randomly. After critical fiber cluster has been formed by nearby broken fibers, the crack extended into the matrix from these fibers. With the increase of load, the fibers and the matrix at the tip of crack gradually destroyed. At the same time, the cracks from other critical fiber clusters were also expanding and connecting to each other. When the crack area has reached the critical level, the remaining fiber and matrix quickly fractured. However, at elevated temperature the matrix yielded firstly, and then multiple fracture randomly of the interfacial reaction layer and the weak fiber occurred sequentially. The crack from broken fiber deflected at interface between fiber and matrix, caused interface debonding. With the increasing of broken fiber number, the micro-cavities of matrix emerged gradually in the stress concentration area. When the total crack area accumulated by the broken fibers and micro-cavities of matrix has reached the critical level, the remaining fiber and matrix quickly fractured.

Key words:  titanium matrix composite      SiC fiber      tensile property      fracture mechanism      fracture process     
ZTFLH:     
Fund:  

URL: 

https://www.ams.org.cn/EN/10.11900/0412.1961.2015.00127     OR     https://www.ams.org.cn/EN/Y2015/V51/I9/1025

Fig.1  Schematic of tensile specimen of SiCf/TC17 composites(unit: mm)
Fig.2  Cross-section of the SiCf/TC17 composites rod showing regular distribution of fibers (a) and overview of interface between fiber and matrix (b)
Material Testing temperature Yield strength Fracture strength Failure strain Elastic modulus
K MPa MPa % GPa
SiCf/TC17 298 1150 1717 0.91 196
SiCf/TC17 773 - 1341 0.79 184
TC17 298 959 1059 >2.00 113
TC17 773 613 726 >2.00 77
Table 1  Tensile properties of the SiCf/TC17 composites and TC17 alloy at 298 and 773 K
Fig.3  Stress-strain curves for the SiCf/TC17 composites and the TC17 alloy at 298 and 773 K (Curves for SiCf/TC17 composites were plotted to fracture, curves for TC17 alloy were interrupted at 2% strain, some slight fluctuations in the straight line were marked by dotted square)
Fig.4  Fracture morphologies of the fracture surface of the SiCf/TC17 composites at 298 K

(a) fracture surface divided into 5 regions by height

(b) dimples in the TC17 canning

(c) flat fracture region 3

(d) magnification of the area surrounded by black frame in Fig.4c

(e) irregular fracture region 4

(f) magnification of the area surrounded by black frame in Fig.4e

Fig.5  Fracture morphologies of the fracture surface of the SiCf/TC17 composites at 773 K

(a) panorama of fracture surface

(b) dimples in the TC17 canning

(c) local irregular fracture surface

(d) tunsgen "pull-out"

(e) longitudinal matrix cracks

(f) interface debonding and matrix damage in a ductile way

Fig.6  Typical morphologies of longitudinal section related to the flat fracture regions in fracture surface of the SiCf/TC17 composites at room temperature

(a) partial macromorphology of longitudinal section

(b) multiple fracture of reaction layer near damaged fiber

(c) matrix cracking from the damaged reaction layer following fiber fracture

(d) flat fracture surface of matrix

Fig.7  Typical morphologies of longitudinal section related to the irregular fracture region in fracture surface of the SiCf/TC17 composites at room temperature

(a) partial macromorphology of longitudinal section

(b) multiple fracture of tungsten core and matrix plastic deformation near the damaged fiber

(c) multiple fracture of reaction layer near damaged fiber

(d) irregular fracture surface and micro-cavities of matrix

Fig.8  Typical morphologies of longitudinal section of fracture surface of the SiCf/TC17 composites at 773 K

(a) partial macromorphology of longitudinal section

(b) a damaged fiber with many fracture mechanisms

(c) multiple fracture of reaction layer and C-coating layer near damaged fiber

(d) irregular fracture surface and micro-cavities of matrix

Fig.9  Fiber fracture of the SiCf/TC17 composites in tensile testing at elevated temperature

(a) formation of pancake structure

(b) formation of tungsten core pull-out

Testing temperature K scomp / MPa
Experiment GLS LLS, i=1 LLS, i=2 LLS, i=3 LLS, i=4
298 1717 2048 1361 1608 1701 1746
773 1341 1381 599 1071 1136 1167
Table 2  Experimental and model prediction results of fracture strength for the SiCf/TC17 composites
[1] Christoph L, Frank K, Joachim H, Wolfgang A K. Aerosp Sci Technol, 2003; 7: 201
[2] Nicolas C, Frédéric F, Serge K. Aerosp Sci Technol, 2003; 7: 307
[3] Naseem K, Yang Y Q, Luo X, Huang B, Feng G H. Mater Sci Eng, 2011; A528: 4507
[4] Thomas M P, Winstone M R. Compos Sci Technol, 1999; 59: 297
[5] Gundel D B, Wawner F E. Compos Sci Technol, 1997; 57: 471
[6] Fukushima A, Fujiwara C, Kagawa Y, Masuda C. Mater Sci Eng, 2000; A276: 243
[7] Weber C H, Chen X, Connell S J, Zok F W. Acta Metall Mater, 1994; 42: 3443
[8] Gálvez F, González C, Poza P, Llorca J. Scr Mater, 2001; 44: 2667
[9] Kagawa Y, Fujita T, Okura A. Acta Metall Mater, 1994; 42: 3019
[10] Peters P W M, Hemptenmacher J. Composites, 2002; 33A: 1373
[11] Truon A, Ccota J, Mainí P, Trias D, Mayugo J A. Compos Sci Technol, 2005; 65: 2039
[12] Baik K H, Grant P S. Scr Mater, 2001; 4: 607
[13] Yang Y Q, Zhu Y, Ma Z J, Chen Y. Scr Mater, 2004; 5: 385
[14] González C, Llorca J. Acta Mater, 2001; 49: 3505
[15] Zhang X. PhD Dissertation, Institute of Metal Research, Chinese Academy of Sciences, Shenyang, 2012 (张 旭. 中国科学院金属研究所博士学位论文, 沈阳, 2012)
[16] Garc??a-Leiva M C, Oca?a I, Mart??n-Meizoso A, Mart??nez-Esnaola J M, Marqués V, Heredero F. Eng Fract Mech, 2003; 70: 2137
[17] Cheng T T, Jones I P, Shatwell R A, Doorbar P. Mater Sci Eng, 1999; A260: 139
[18] Hill R A. J Mech Phys Solids, 1965; 13: 213
[19] Curtin W A. J Am Ceram Soc, 1991; 74: 283
[20] Curtin W A. Composites, 1993; 24: 98
[21] Li J K, Yang Y Q, Yuan M N, Luo X, Li L L. Trans Nonferrous Met Soc China, 2008; 18: 523
[22] Chandra N, Ghonem H. Composites, 2001; 32A: 575
[23] Chandra N, Ananth C R. Compos Sci Technol, 1995; 54: 87
[24] Kalton A F, Howard S J, Janczak-rusch J, Clyne T W. Acta Mater, 1998; 46: 3175
[25] Jeng S M, Yang J M, Yang C J. Mater Sci Eng, 1991; A138: 169
[1] WANG Di, HE Lili, WANG Dong, WANG Li, ZHANG Siqian, DONG Jiasheng, CHEN Lijia, ZHANG Jian. Influence of Pt-Al Coating on Tensile Properties of DD413 Alloy at High Temperatures[J]. 金属学报, 2023, 59(3): 424-434.
[2] SUN Tengteng, WANG Hongze, WU Yi, WANG Mingliang, WANG Haowei. Effect ofIn Situ 2%TiB2 Particles on Microstructure and Mechanical Properties of 2024Al Additive Manufacturing Alloy[J]. 金属学报, 2023, 59(1): 169-179.
[3] CHEN Run, WANG Shuai, AN Qi, ZHANG Rui, LIU Wenqi, HUANG Lujun, GENG Lin. Effect of Hot Extrusion and Heat Treatment on the Microstructure and Tensile Properties of Network Structured TiBw/TC18 Composites[J]. 金属学报, 2022, 58(11): 1478-1488.
[4] WANG Chao, ZHANG Xu, WANG Yumin, YANG Qing, YANG Lina, ZHANG Guoxing, WU Ying, KONG Xu, YANG Rui. Mechanisms of Interfacial Reaction and Matrix Phase Transition in SiCf /Ti65 Composites[J]. 金属学报, 2020, 56(9): 1275-1285.
[5] WU Yupeng, ZHANG Bo, LI Jingming, ZHANG Shuangnan, WU Ying, WANG Yumin, CAI Guixi. Ultrasonic Detection for Fiber Broken in Aero-Engine Integral Bladed Ring[J]. 金属学报, 2020, 56(8): 1175-1184.
[6] LIU Xianfeng, LIU Dong, LIU Renci, CUI Yuyou, YANG Rui. Microstructure and Tensile Properties of Ti-43.5Al-4Nb-1Mo-0.1B Alloy Processed by Hot Canned Extrusion[J]. 金属学报, 2020, 56(7): 979-987.
[7] LI Yuancai, JIANG Wugui, ZHOU Yu. Effect of Nanopores on Tensile Properties of Single Crystal/Polycrystalline Nickel Composites[J]. 金属学报, 2020, 56(5): 776-784.
[8] YU Chenfan, ZHAO Congcong, ZHANG Zhefeng, LIU Wei. Tensile Properties of Selective Laser Melted 316L Stainless Steel[J]. 金属学报, 2020, 56(5): 683-692.
[9] WANG Xi,LIU Renci,CAO Ruxin,JIA Qing,CUI Yuyou,YANG Rui. Effect of Cooling Rate on Boride and Room Temperature Tensile Properties of β-Solidifying γ-TiAl Alloys[J]. 金属学报, 2020, 56(2): 203-211.
[10] ZHU Jian, ZHANG Zhihao, XIE Jianxin. Plastic Deformation Behavior and Fracture Mechanism of Rare Earth H13 Steel Based on In Situ TEM Tensile Study[J]. 金属学报, 2020, 56(12): 1592-1604.
[11] Zheng LIU,Jianrong LIU,Zibo ZHAO,Lei WANG,Qingjiang WANG,Rui YANG. Microstructure and Tensile Property of TC4 Alloy Produced via Electron Beam Rapid Manufacturing[J]. 金属学报, 2019, 55(6): 692-700.
[12] Dechun REN, Huhu SU, Huibo ZHANG, Jian WANG, Wei JIN, Rui YANG. Effect of Cold Rotary-Swaging Deformation on Microstructure and Tensile Properties of TB9 Titanium Alloy[J]. 金属学报, 2019, 55(4): 480-488.
[13] Shenghu CHEN, Lijian RONG. Microstructure Evolution During Solution Treatment and Its Effects on the Properties of Ni-Fe-Cr Alloy[J]. 金属学报, 2018, 54(3): 385-392.
[14] Jialin LIU, Yumin WANG, Guoxing ZHANG, Xu ZHANG, Lina YANG, Qing YANG, Rui YANG. Research on Single SiC Fiber Reinforced TC17 CompositesUnder Transverse Tension[J]. 金属学报, 2018, 54(12): 1809-1817.
[15] Dongdong LI, Lihe QIAN, Shuai LIU, Jiangying MENG, Fucheng ZHANG. Effect of Manganese Content on Tensile Deformation Behavior of Fe-Mn-C TWIP Steels[J]. 金属学报, 2018, 54(12): 1777-1784.
No Suggested Reading articles found!