MECHANICALLY--DRIVEN AMORPHIZATION IN A (Ti, Zr, Hf)--(Cu, Ni, Ag)--Al MULTICOMPONENT ALLOY SYSTEM

Acta Metall Sin

2004, Vol. 40

Issue (4): 421-428 DOI:

Research Articles

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MECHANICALLY--DRIVEN AMORPHIZATION IN A (Ti, Zr, Hf)--(Cu, Ni, Ag)--Al MULTICOMPONENT ALLOY SYSTEM

HANG Laichang; SHEN Zhiqi; XU Jian

Shenyang National Laboratory for Materials Science; Institute of Metal Research; The Chinese Academy of Sciences; Shenyang 110016

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HANG Laichang; SHEN Zhiqi; XU Jian. MECHANICALLY--DRIVEN AMORPHIZATION IN A (Ti, Zr, Hf)--(Cu, Ni, Ag)--Al MULTICOMPONENT ALLOY SYSTEM. Acta Metall Sin, 2004, 40(4): 421-428 .

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Abstract The glass formation under high--energy ball milling was investigated for a (Ti0.33Zr0.33Hf0.33)50(Ni0.33Cu0.33Ag0.33)40Al10 high--order alloy system. For comparison, the glassy ribbon with the same composition was prepared using melt--spinning (MS) method as well. Structural features of the samples were characterized using X--ray diffraction, ransmission electron microscopy and differential scanning calorimetry. Mechanical alloying (MA) results in a formation of glassy alloy similar to that obtained by MS. But, the glass formation is incomplete and a small amount of unreated crystallites smaller than 30 nm in size still remains in the final product. Like the melt--spun glass, the ball--milled glassy alloy also exhibits a distinct glass transition and a wide supercooled liquid region of about 80 K. Crystallization of the glassy alloy is a two--step p rocess, regardless of the synthesis routes. After the primary crystallization is completed, the remaining amorphous phase shows a detectable glass transition and a large supercooled liquid region of about 100 K.

Key words: mechanical alloying amorphous alloy supercooled liquid region

Received: 13 May 2003

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