High-Cycle Fatigue Properties and Residual Stress Relaxation Mechanism of Micro-Arc Oxidation 6082-T6 Aluminum Alloy
SU Kaixin1, ZHANG Jiwang1(), ZHANG Yanbin2, YAN Tao3, LI Hang1, JI Dongdong1
1.State Key Laboratory of Traction Power, Southwest Jiaotong University, Chengdu 610031, China 2.School of Mechanical Engineering, Southwest Jiaotong University, Chengdu 610031, China 3.Bj -baodeli Electrical Equipment Co. , Ltd. , Baoji 721000, China
Cite this article:
SU Kaixin, ZHANG Jiwang, ZHANG Yanbin, YAN Tao, LI Hang, JI Dongdong. High-Cycle Fatigue Properties and Residual Stress Relaxation Mechanism of Micro-Arc Oxidation 6082-T6 Aluminum Alloy. Acta Metall Sin, 2022, 58(3): 334-344.
Recently, the fatigue failure of aluminum alloy components of high-speed railway catenary is becoming increasingly serious, which causes a threat to the normal operation of high-speed trains. In this study, the effect of micro-arc oxidation (MAO) coating on the high-cycle fatigue properties of 6082-T6 aluminum alloy for the catenary cantilever of the high-speed railway was studied. First, the rotating bending fatigue tests of untreated (UP) and MAO specimens of 6082-T6 aluminum alloy were performed. Then, the surface morphology and roughness, cross-section morphology, nanoindentation hardness, and elastic modulus gradient distribution, phase composition of MAO coating, and fatigue fracture morphology of the fatigue samples were studied by a confocal laser microscope, nanoindentation, XRD, and SEM. The experimental results showed that after MAO treatment, a large number of micro-cracks and pores were formed on the surface of the samples, and the morphology of the samples severely deteriorated. The XRD results indicated that the closer the coating surface, the stronger was the diffraction peaks of α-Al2O3 and γ-Al2O3. Besides, there was the higher tensile residual stress at the coating-substrate interface, which led to a significant reduction in fatigue properties. The fatigue strength decreased by 26.7% at 2 × 107 cyc. Finally, the formation and relaxation mechanisms of tensile residual stress under cyclic stress were analyzed using mismatch strain theory, and the effects of the coating on the fatigue properties of the substrate under high and low cyclic stresses were discussed further.
Fig.1 Sample shape and dimensions for mechanical property (a) and fatigue property (b) tests (unit: mm)
Fig.2 Schematic of residual stress measurement
Treatment
Elastic modulus
Yield strength
Ultimate tensile
Elongation
Section shrinkage
GPa
MPa
strength / MPa
%
%
UP
69.4 ± 2.2
317.9 ± 9.4
347.4 ± 7.0
8.2 ± 0.1
34.5 ± 0.3
MAO
67.2 ± 0.2
337.7 ± 0.2
350.9 ± 0.6
8.7 ± 0.6
34.8 ± 0.8
Table 1 Mechanical properties of untreated (UP) and micro-arc oxidation (MAO) 6082-T6 Al alloy
Fig.3 Surface morphologies (a, c) and 3D profiles (b, d) of UP (a, b) and MAO (c, d) samples (Inset in Fig.3c shows a higher magnification for MAO surface morphology)
Treatment
Ra
Rz
Rmax
UP
0.07 ± 0.00
0.60 ± 0.10
0.83 ± 0.28
MAO
2.65 ± 0.05
87.22 ± 9.58
93.69 ± 7.30
Table 2 Surface roughnesses of UP and MAO samples
Fig.4 XRD spectra of the MAO coating surface (a) and interior (b)
Fig.5 Cross section morphologies of UP (a) and MAO (b) samples
Fig.6 Coating hardness and elastic modulus distributions
Fig.7 Stress-fatigue life (S-N) curves of UP and MAO samples
Fig.8 Fracture morphologies of UP and MAO samples
Fig.9 Relaxation of tensile residual stress under different cyclic stresses of MAO samples
Fig.10 Formation (a) and relaxation (b) of tensile residual stress at the MAO coating-substrate interface
Fig.11 The variation trend of fatigue life of MAO sample compared with UP sample under different cyclic stresses (β—percentage of fatigue life change)
1
Starke E A, Staley J T. Application of modern aluminum alloys to aircraft [J]. Prog. Aeosp. Sci., 1996, 32: 131
2
Heinz A, Haszler A, Keidel C, et al. Recent development in aluminium alloys for aerospace applications [J]. Mater. Sci. Eng., 2000, A280: 102
3
Krishna L R, Somaraju K R C, Sundararajan G. The tribological performance of ultra-hard ceramic composite coatings obtained through microarc oxidation [J]. Surf. Coat. Technol., 2003, 163-164: 484
4
Krishna L R, Purnima A S, Sundararajan G. A comparative study of tribological behavior of microarc oxidation and hard-anodized coatings [J]. Wear, 2006, 261: 1095
5
Lonyuk B, Apachitei I, Duszczyk J. The effect of oxide coatings on fatigue properties of 7475-T6 aluminium alloy [J]. Surf. Coat. Technol., 2007, 201: 8688
6
Wasekar N P, Jyothirmayi A, Sundararajan G. Influence of prior corrosion on the high cycle fatigue behavior of microarc oxidation coated 6061-T6 Aluminum alloy [J]. Int. J. Fatigue, 2011, 33: 1268
7
Nie X, Meletis E I, Jiang J C, et al. Abrasive wear/corrosion properties and TEM analysis of Al2O3 coatings fabricated using plasma electrolysis [J]. Surf. Coat. Technol., 2002, 149: 245
8
Barik R C, Wharton J A, Wood R J K, et al. Corrosion, erosion and erosion-corrosion performance of plasma electrolytic oxidation (PEO) deposited Al2O3 coatings [J]. Surf. Coat. Technol., 2005, 199: 158
9
Wen L, Wang Y M, Zhou Y, et al. Corrosion evaluation of microarc oxidation coatings formed on 2024 aluminium alloy [J]. Corros. Sci., 2010, 52: 2687
10
Gecu R, Yurekturk Y, Tekoglu E, et al. Improving wear resistance of 304 stainless steel reinforced AA7075 aluminum matrix composite by micro-arc oxidation [J]. Surf. Coat. Technol., 2019, 368: 15
11
Kong D J, Liu H, Wang J C. Effects of micro arc oxidation on fatigue limits and fracture morphologies of 7475 high strength aluminum alloy [J]. J. Alloys Compd., 2015, 650: 393
12
Dai W B, Liu Z H, Li C Y, et al. Fatigue life of micro-arc oxidation coated AA2024-T3 and AA7075-T6 alloys [J]. Int. J. Fatigue, 2019, 124: 493
13
Wang Y M, Zhang P F, Guo L X, et al. Effect of microarc oxidation coating on fatigue performance of Ti-Al-Zr alloy [J]. Appl. Surf. Sci., 2009, 255: 8616
14
Khan R H U, Yerokhin A, Li X, et al. Surface characterisation of DC plasma electrolytic oxidation treated 6082 aluminium alloy: Effect of current density and electrolyte concentration [J]. Surf. Coat. Technol., 2010, 205: 1679
15
Leoni A, Apachitei I, Riemslag A C, et al. In vitro fatigue behavior of surface oxidized Ti35Zr10Nb biomedical alloy [J]. Mater. Sci. Eng., 2011, C31: 1779
16
Madhavi Y, Krishna L R, Narasaiah N. Influence of micro arc oxidation coating thickness and prior shot peening on the fatigue behavior of 6061-T6 Al alloy [J]. Int. J. Fatigue, 2019, 126: 297
17
Oliver W C, Pharr G M. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments [J]. J. Mater. Res., 1992, 7: 1564
18
Lin J, Ma N S, Lei Y P, et al. Measurement of residual stress in arc welded lap joints by cosα X-ray diffraction method [J]. J. Mater. Process. Technol., 2017, 243: 387
19
Dai W B, Li C Y, He D, et al. Influence of duty cycle on fatigue life of AA2024 with thin coating fabricated by micro-arc oxidation [J]. Surf. Coat. Technol., 2019, 360: 347
20
Li J, Sun Q, Zhang Z P, et al. Theoretical estimation to the cyclic yield strength and fatigue limit for alloy steels [J]. Mech. Res. Commun., 2009, 36: 316
21
Bäumel A, Seeger T. Materials Data for Cyclic Loading [M]. Amsterdam: Elsevier, 1990: 1
22
Wasekar N P, Ravi N, Babu P S, et al. High-cycle fatigue behavior of microarc oxidation coatings deposited on a 6061-T6 Al alloy [J]. Metall. Mater. Trans., 2010, 41A: 255
23
Gu W C, Lv G H, Chen H, et al. Characterisation of ceramic coatings produced by plasma electrolytic oxidation of aluminum alloy [J]. Mater. Sci. Eng., 2007, A447: 158
24
Krishna L R, Gupta P S V N B, Sundararajan G. The influence of phase gradient within the micro arc oxidation (MAO) coatings on mechanical and tribological behaviors [J]. Surf. Coat. Technol., 2015, 269: 54
25
Xue W B, Deng Z W, Chen R Y, et al. Distribution of hardness and elastic modulus near the interface between aluminum alloy substrate and microarc oxidation coating [J]. Acta Metall. Sin., 1999, 35: 638
Malyshev V. Mikrolichtbogen-oxidation: EIN neuartiges verfahren zur verfestigung von aluminiumoberflächen [J]. Metalloberflaeche, 1995, 49: 606
27
Dai W B, Li C Y, He D, et al. Mechanism of residual stress and surface roughness of substrate on fatigue behavior of micro-arc oxidation coated AA7075-T6 alloy [J]. Surf. Coat. Technol., 2019, 380: 125014
28
Su K X, Zhang J W, Li H, et al. Analysis on the fatigue properties of shot-peened Al-Si-Mg alloy and its fatigue life prediction [J]. J. Mater. Eng. Perform., 2020, 29: 5114
29
Schijve J. Fatigue of Structures and Materials [M]. New York: Springer Science & Business Media, 2001: 1
30
Hadzima B, Nový F, Trško L, et al. Shot peening as a pre-treatment to anodic oxidation coating process of AW 6082 aluminum for fatigue life improvement [J]. Int. J. Adv. Manuf. Technol., 2017, 93: 3315
31
Krishna L R, Madhavi Y, Sahithi T, et al. Influence of prior shot peening variables on the fatigue life of micro arc oxidation coated 6061-T6 Al alloy [J]. Int. J. Fatigue, 2018, 106: 165
32
Freund L B, Suresh S. Thin Film Materials: Stress, Defect Formation and Surface Evolution [M]. Cambridge: Cambridge University Press, 2004: 1
33
Dai W B, Hao J, Li C Y, et al. Residual stress relaxation and duty cycle on high cycle fatigue life of micro-arc oxidation coated AA7075-T6 alloy [J]. Int. J. Fatigue, 2020, 130: 105283
34
Kim J C, Cheong S K, Noguchi H. Residual stress relaxation and low- and high-cycle fatigue behavior of shot-peened medium-carbon steel [J]. Int. J. Fatigue, 2013, 56: 114
35
Zhong W, Ding Y L, Song Y S, et al. Relaxation effect of welding residual stress in deck-to-rib joints [J]. J. Zhejiang Univ. (Eng. Sci.), 2020, 54: 83
Zhang J W, Lu L T, Shiozawa K, et al. Analysis on fatigue property of microshot peened railway axle steel [J]. Mater. Sci. Eng., 2011, A528: 1615
37
Ishihara S, Saka S, Nan Z Y, et al. Prediction of corrosion fatigue lives of aluminium alloy on the basis of corrosion pit growth law [J]. Fatigue Fract. Eng. Mater. Struct., 2006, 29: 472