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EFFECT OF PRESTRAIN ON THE SUPERPLASTIC DEFORMATION BEHAVIOR OF LOW-ALLOY HIGH-CARBON STEEL |
ZHANG Han; BAI Bingzhe; FANG Hongsheng |
Key Laboratory for Advanced Materials of Ministry of Education; Department of Materials Science and Engineering; Tsinghua University; Beijing 100084 |
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Cite this article:
ZHANG Han BAI Bingzhe FANG Hongsheng. EFFECT OF PRESTRAIN ON THE SUPERPLASTIC DEFORMATION BEHAVIOR OF LOW-ALLOY HIGH-CARBON STEEL. Acta Metall Sin, 2009, 45(9): 1106-1110.
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Abstract There were some reports on superplasticity of ultra-high carbon steels in the last several decades, mainly referring to the superplasticity of fine-equiaxial double-phase microstructure (fine ferrite + cementite particles). However, in order to get the fine--equiaxial double--phase microstructure, very complicated pre-treatment was needed. An exploration to obtain superplastic microstructure through simple uniaxial compression at pearlite transformation incubation temperature was conducted using Gleeble 1500D in this paper. The microstructural evolution processes of the steel during deformation included (1) pearlite transformation, (2) cementite spheroidization and (3) ferrite recrystallization. The (2) and (3) processes start before the finish of pearlite transformation. Two micro-processes of cementite spheroidization were shown in the experiments. One is that the cementite lamellae were dissolved and broken. This process results in the formation of relatively coarse cementite particles (100-200 nm). Another is that finer cementite particles (10-30 nm) reprecipitated in the ferrite during ferrite recrystallization. Deformation during pearlite incubation period can accelerate pearlite transformation and cementite spheroidization. The above processes lead to form fine double-phase microstructure with sub--micrometer and nanometer cementite particles distributed uniformly in fine ferrite (about 1 μm). Samples with the fine double--phase microstructure show the m value of 0.40 in the strain rate range of 1×10-4-2×10-4 s-1 at 700 ℃. The flow stress under different strain rates reduces with the increase of the prestrain. For example, under the strain rate of 1×10-4 s-1 at 700 ℃, the flow stress of the samples with prestrain of 1.2 is only 70 MPa, much lower than 120 MPa of the samples without prestrain. The dispersed cementite particles can prevent ferrite grains from growing during deformation process at high temperature, as a result, the stability of the fine-equiaxial double-phase microstructure is ensured, which is the microstructural condition realizing superplasticity.
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Received: 04 January 2009
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Fund: Supported by National Basic Research Program of China (No.2004CB619105) |
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