连续SiC纤维增强钛基复合材料研究进展<sup>*</sup>

doi:10.11900/0412.1961.2016.00347

金属学报

2016, Vol. 52

Issue (10): 1153-1170 DOI: 10.11900/0412.1961.2016.00347

论文

本期目录 | 过刊浏览

连续SiC纤维增强钛基复合材料研究进展^*

王玉敏,张国兴,张旭,杨青,杨丽娜,杨锐(

)

中国科学院金属研究所, 沈阳 110016

ADVANCES IN SiC FIBER REINFORCED TITANIUM MATRIX COMPOSITES

Yumin WANG,Guoxing ZHANG,Xu ZHANG,Qing YANG,Lina YANG,Rui YANG

Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

引用本文:

王玉敏, 张国兴, 张旭, 杨青, 杨丽娜, 杨锐. 连续SiC纤维增强钛基复合材料研究进展^*[J]. 金属学报, 2016, 52(10): 1153-1170.
Yumin WANG, Guoxing ZHANG, Xu ZHANG, Qing YANG, Lina YANG, Rui YANG. ADVANCES IN SiC FIBER REINFORCED TITANIUM MATRIX COMPOSITES[J]. Acta Metall Sin, 2016, 52(10): 1153-1170.

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摘要:

简述了近年来国内外SiC纤维增强钛基复合材料的发展进程和应用进展情况, 从纤维批量化生产、复合材料界面、主要力学性能、无损检测和结构件研制与考核5个方面对该类材料的研究进展进行了回顾. 在纤维批量化生产和复合材料结构件研制方面, 重点介绍了中国科学院金属研究所的研究工作, 并对该类复合材料未来的发展趋势进行了展望.

关键词 ：钛基复合材料, SiC纤维, 界面反应, 无损检测, 整体叶环

Abstract：

SiC fibers can be used to reinforce a range of titanium base materials including alloys of the (α+β) type, metastable β type and near α type, as well intermetallic based γ-TiAl and orthorhombic Ti₂AlNb. Along the fiber directions the obtained composites possess exceptional strength and stiffness, creating a large room and great flexibility for the design of higher performance components to be used in both aero engine and aircraft. The composites can be used by itself such as in sheet and bar form, or as a reinforcing module embedded in titanium alloy components, e.g., as a ring at the rim of a compressor disk. In this paper, recent progress in the development and application of SiC fiber reinforced titanium matrix composites was reviewed, emphasizing the work conducted at the Institute of Metal Research, Chinese Academy of Sciences. Five aspects of research were covered, the first is fiber manufacture and batch production, in which the influence of the chemical vapor deposition parameters on the quality of the W-core SiC fiber was discussed, and the relationship between the tungsten-SiC interface reaction and the high temperature stability of the fiber was described. The second part covers the composite interface, in which a detailed discussion was given to both the chemical and physical compatibility, followed by the design of different reaction layers between the SiC fiber and different titanium based matrixs. The mechanical property section presents tensile data of a range of composites developed in the authors' group and compares to literature reports where available, together with a comprehensive discussion of failure due to fatigue and creep. The fourth part deals with nondestructive testing, presenting new results of inspection on real size composite components using a combination of several techniques including X-ray, industrial CT and ultrasonic scanning. The limitations of each method were shown and the technical challenges were identified. The last part describes the development of structural parts and their verification testing. Titanium matrix composite sheets with [0/90] laminate prepared by both the foil-fiber-foil and matrix coated fiber methods were highlighted, followed by a description of the development of full size bladed ring and excess revolution testing. Future directions of research on SiC fiber reinforced titanium matrix composites were also discussed.

Key words： titanium matrix composites SiC fiber interfacial reaction non-destructive testing bladed ring

收稿日期: 2016-08-01

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https://www.ams.org.cn/CN/10.11900/0412.1961.2016.00347 或 https://www.ams.org.cn/CN/Y2016/V52/I10/1153

图1 直流加热法和射频加热法SiC纤维生产示意图

图2 中国科学院金属研究所设计和建立的SiC纤维批量化生产装置(11套)

图3 中国科学院金属研究所生产的SiC纤维及其横截面形貌

图4 SiC纤维抗拉强度与W芯/SiC界面反应层厚度之间的关系(插图为Gambone与Gundel[17]有关Trimarc 1?纤维实验数据的总结)[16]

图5 不同温度拉伸后典型断口及W芯/SiC反应层区域的形貌[16]

表1 Ti-SiC热力学体系可能发生的化学反应

图6 G峰位置与SiC纤维拉力的关系[49]

表2 国内外研制的几种钛基复合材料(TMCs)的典型室温拉伸性能[83-96]

图7 纤维裂纹的钝化和偏转[15]

图8 整体叶环超声C扫描检测图谱(中间部分为复合材料, 不连续处为纤维集中断裂)

图9 热压态板材超声显微镜成像和室温拉伸断口XRT技术成像

图10 不同工艺制备的[0/90]层合板的横截面纤维排布

图11 中国科学院金属研究所制备的不同规格和形状的板材照片

图12 热等静压致密化过程有限元计算结果与实验结果对比

图13 国内首件全尺寸复合材料整体叶环

图14 复合材料整体叶环超转实验件

图15 复合材料叶环强度实验件及破转后照片

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