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金属学报    DOI: 10.11900/0412.1961.2025.00032
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热压缩Mg-Gd-Y-Nd合金分裂织构形成及再结晶行为

李岩峰1,2  李振亮1,2  张海艳1,2  丁 国1,2  张建飞1,2

1 内蒙古科技大学 材料科学与工程学院 包头 014010

2 内蒙古自治区新金属材料重点实验室 包头 014010

Recrystallization Behavior and Split Texture Evolution of Hot Compressed Mg–Gd–Y–Nd Alloy

LI Yanfeng1,2, LI Zhenliang1,2, ZHANG Haiyan1,2, DING Guo1,2, ZHANG Jianfei1,2

1 School of Materials Science and Engineering, Inner Mongolia University of Science and Technology, Baotou 014010, China

2 Inner Mongolia Key Laboratory of New Metal Material, Baotou 014010, China

引用本文:

李岩峰 李振亮 张海艳 丁国 张建飞. 热压缩Mg-Gd-Y-Nd合金分裂织构形成及再结晶行为[J]. 金属学报, DOI: 10.11900/0412.1961.2025.00032.

全文: PDF(4110 KB)  
摘要: 
高合金化稀土镁合金微观组织演化与塑性变形之间具有动态敏感性,本工作通过快速凝固技术制备Mg-4.7Y-2.1Nd-0.6Gd-0.5Zr合金,利用EBSD和Wulff网分析多道次和单道次压缩后合金微观组织演变,探究应变梯度工艺对分裂织构与动态再结晶(DRX)机制的作用规律。研究表明,2°取向差晶粒减少、“软取向”晶粒增加、发生柱面<a>滑移的晶粒转向增多是导致多道次热压缩后形成横向(TD)分裂织构的主要原因。单道次热压缩过程中,由于协调晶粒沿c轴方向变形需将大量晶粒转到易于激活锥面<c + a>滑移取向,因此形成压缩方向(ED)分裂织构。TD分裂织构有利于提高镁合金TD强度和非TD (即ED和法向方向(ND))塑性,而ED分裂织构则有利于提高ED强度和非ED (即ND和TD)塑性。多道次热压缩交替发生连续/非连续DRX,其几何必需位错密度(4.59 × 1013 m-2)高于单道次(4.20 × 1013 m-2),再结晶晶粒面积分数为16%且混晶结构被弱化。单道次热压缩以非连续DRX为主,其再结晶晶粒面积分数为14%,大尺寸微米级亚结构被保留导致形成混晶结构。
关键词 稀土镁合金热压缩变形EBSD动态再结晶分裂织构    
Abstract

Alloying design and grain refinement strategies have emerged as promising synergistic approaches to overcoming the persistent strength–ductility trade-off that occurs during Mg alloy processing. However, the regulatory effect of plastic deformation on microstructural evolution requires further systematic investigation to synergistically optimize mechanical performance. In this study, multi-pass and single-pass hot compression tests were performed on MgGdYNd alloys that had been rapidly solidified, and the key parameters for alloy design in big data research—dynamic recrystallization (DRX), geometrically necessary dislocation (GND) density, and texture—were analyzed using EBSD and Wulff net. The results show that a split texture in the transverse direction (TD) (in the Wulff net coordinate system, the peak distribution is in the ranges of 20° ≤ φ ≤ 40° and 50° ≤ θ ≤ 70°, where θ represents the radius, φ denotes the latitude) was formed during the multi-pass hot compression. The primary factors that affect the formation of TD split texture are the reduction in the number of grains having a 2° correlated misorientation angle, the increase in the fraction of soft-oriented grains, and the reorientation of grains into positions that are favorable for activating the prismatic <a> slip. In contrast, the results showed that a split texture in the extruding direction (ED) (in the Wulff net coordinate system, the peak distribution is in the ranges of 60° ≤ φ ≤ 70° and θ ≈ 80°) was formed during single-pass hot compression. The primary factor that affected the formation of the ED split texture was the need for a significant number of grains to reorient to positions that were favorable for activating the pyramidal <c + a> slip to coordinate the deformation of the c-axis during single-pass hot compression. The splitting texture of magnesium alloys enhances both strength and plasticity. The TD split texture involves orienting the c-axis of the grains toward the TD. When a load is applied in the TD direction, the deformation is primarily coordinated by the activation of the pyramidal <c + a> slip (with a high critical resolved shear stress (CRSS)), which is beneficial for enhancing strength. When a load is applied in the non-TD directions (i.e., the ED and normal direction (ND)), the deformation is coordinated by the prismatic <a> slip and basal <a> slip (with a lower CRSS than the pyramidal <c + a> slip), which is beneficial for enhancing plasticity. With an ED split texture, the c-axis of the grains are oriented toward the ED. When a load is applied in the ED direction, the deformation is primarily coordinated by the activation of the pyramidal <c + a> slip, which is beneficial for enhancing strength. When a load is applied in the non-ED directions (i.e., the TD and ND directions), the deformation is coordinated by the prismatic <a> slip and basal <a> slip, which is beneficial for enhancing plasticity. The recrystallized grain fraction during multi-pass hot compression was 16% and was accompanied by a higher GND density (4.59 × 10¹³ m⁻²) than during single-pass hot compression (4.20 × 10¹³ m⁻²), as well as a significant weakening of the mixed crystal structure. This outcome was primarily attributed to the alternating occurrences of continuous dynamic recrystallization (CDRX) and discontinuous dynamic recrystallization (DDRX) during multi-pass hot compression. In contrast, during single-pass hot compression, the recrystallized grain fraction was 14% and larger micron-sized substructures were retained (which led to the formation of the mixed crystal structure). This outcome was primarily attributed to the dominance of DDRX during single-pass hot compression.

Key wordsrare-earth magnesium alloy    hot compression deformation    electron back scatter diffraction    dynamic recrystallization    split texture
收稿日期: 2025-01-26     
ZTFLH:  TG146.2  
基金资助:Ca/Nd复合高合金化镁合金塑性变形过程中织构影响规律研究;稀土高合金化/亚结构演变构筑高性能镁合金的增强增塑机理研究
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