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A TEM STUDY OF SPINODAL DECOMPOSITION IN Fe-1 .83C MARTENSITE |
REN Xiaobing; WANG Xiaotian (Xi'an Jiaotong University) SHIMIZU Ken'ichi(Kanazawa institute of Technology; Japan) TADAKI Tsugio (Osaka University;Japan)(Manuscript received 27 October; 1993; in revised form 4 January; 1994) |
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Cite this article:
REN Xiaobing; WANG Xiaotian (Xi'an Jiaotong University) SHIMIZU Ken'ichi(Kanazawa institute of Technology; Japan) TADAKI Tsugio (Osaka University;Japan)(Manuscript received 27 October; 1993; in revised form 4 January; 1994). A TEM STUDY OF SPINODAL DECOMPOSITION IN Fe-1 .83C MARTENSITE. Acta Metall Sin, 1994, 30(7): 289-295.
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Abstract Diffuse scattering and microstructure of Fe-1.83C(%) martensite aged at room temperature was studied by TEM. The intensity distribution of diffuse scattering in reciprocal space was determined by double-tilt technique. The results show that the shape of martensite diffraction spot becomes a diffuse spike after aging, and its 3-dimensional profile appears to be two head-on 4-sided regular pyramids. Fourier analysis of the diffuse scattering suggests that martensite undergoes a spinodal decomposition during aging,the tweed-like modulated structure is composed of a dominant wave with wavelength of about 1 nm and non-dominant waves with longer wavelengths. For the first time it is found that the modulated structure of Fe-C martensite does not grow even after aged for several months.The reason is considered to be due to the strong elastic interactions among carbon-enriched and depleted regions.Correspondent: REN Hiaobing, Presently with Department of Physics, Nanjing, University, Nanjing 21008)
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Received: 18 July 1994
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