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Acta Metall Sin  1992, Vol. 28 Issue (2): 64-70    DOI:
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BRITTLE-DUCTILE TRANSITION OF ANNEAL-EMBRITTLED Fe_(75)Si_(10)B_(15) METALLIC GLASS
WANG Longbao State Key Laboratory of Rapidly Solidified Non-Equilibrium Alloys; Institute of Metal Research; Academia Sinica; Shenyang;
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WANG Longbao State Key Laboratory of Rapidly Solidified Non-Equilibrium Alloys; Institute of Metal Research; Academia Sinica; Shenyang;. BRITTLE-DUCTILE TRANSITION OF ANNEAL-EMBRITTLED Fe_(75)Si_(10)B_(15) METALLIC GLASS. Acta Metall Sin, 1992, 28(2): 64-70.

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Abstract  Studies were made of the effect of mechanical pulverization on relaxation,crystallization and brittle--ductile transition of the anneal--embrittled Fe_(75)Si_(10)B_(15) metallic glass ribbon. Results show that the Curie temperature, T_c, decreases and the total enthalpy of relaxa-tion increases gradually with variation of pulverized time. DSC traces reveal an extra exothermicpeak, T_(x_1), and a distinct glass transition endothermic peak, T_(g_1), with increasing pulverizedtime, T_c, T_(x_1), and T_(g_1) decrease simultaneously, and the exothermic peak area correspondingto T_(x_1) increases gradually. The surface slip--steps of flaky particles and their corresponding shear are produced by pulverizing the pre--embrittled amorphous glass. The lost ductility of theglass may restore during annealing.
Key words:  mechanical pulverization      Fe_(75)Si_(10)B_(15)      metallic glass      shear band     
Received:  18 February 1992     
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