OPTIMIZING CONTROL OF PRECIPITATES IN T91 FERRITIC HEAT－RESISTAN STEEL

doi:10.3724/SP.J.1037.2013.00178

Acta Metall Sin

2013, Vol. 49

Issue (9): 1075-1080 DOI: 10.3724/SP.J.1037.2013.00178

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OPTIMIZING CONTROL OF PRECIPITATES IN T91 FERRITIC HEAT－RESISTAN STEEL

ZHANG Ruihui¹⁾, ZHANG Chi¹⁾, XIA Zhixin²⁾, YANG Zhigang¹⁾

1) Key Laboratory of Advanced Materials of Ministry of Education, School of Materials Science and Engineering,Tsinghua University, Beijing 100084
2) Suzhou Nuclear Power Research Institute, Suzhou 215004

Cite this article:

ZHANG Ruihui, ZHANG Chi, XIA Zhixin, YANG Zhigang. OPTIMIZING CONTROL OF PRECIPITATES IN T91 FERRITIC HEAT－RESISTAN STEEL. Acta Metall Sin, 2013, 49(9): 1075-1080.

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Abstract

T91 steel is one representative of (9%－12%)Cr (mass fraction) ferritic heat－resistant steel, in which MX carbonitrides and M₂₃C₆ carbides are two major strengthened precipitates for long－term creep under high temperature. This work attempted to control the precipitation of MX carbonitrides and M₂₃C₆ carbides by applying new heat treatment procedures. With the assist of Thermal－Calc software calculation, two new heat treatment procedures have been designed for T91 steel based on its traditional normalized－tempered treatment, in which an isothermal treatment at 850℃ was introduced between normalized treatment and tempered treatment. The mean size of M₂₃C₆ carbides decreased from 350 nm to 250 nm and the number density of MX carbonitrides increased due to the new heat treatment procedures. The calculated results of Thermal－Calc software showed that the nucleation rate of M₂₃C₆ carbides at 750℃ increased with the decrease of carbon content in the matrix, which might be the major reason why the mean size of M₂₃C₆ carbides decreased.

Key words: T91 steel precipitate M₂₃C₆ nucleation rate

Received: 09 April 2013

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https://www.ams.org.cn/EN/10.3724/SP.J.1037.2013.00178 OR https://www.ams.org.cn/EN/Y2013/V49/I9/1075

[1] Sklenicka V, Kucha rv a K, Svoboda M, Kloc L,Bursik J, Kroupa A. Mater Charact, 2003; 51: 35

[2] Ha V H, Jung W S. Mater Sci Eng, 2012; A558: 103

[3] Wang Y, Mayer K H, Scholz A, Berger C, Chilukuru H, Durst K, Blum W.Mater Sci Eng, 2009; A511: 180

[4] Prat O, Garcia J, Rojas D, Carrasco C, Kaysser－Pyzalla A R. Mater Sci Eng,2010; A527: 5976

[5] Knezevic V, Balun J, Sauthoff G, Inden G, Schneider A. Mater Sci Eng, 2008; A477: 334

[6] Tsuchida Y, Okamoto K, Tokunaga Y. ISIJ Int, 1995; 35: 309

[7] Klueh R L, Hashimoto N, Maziasz P J. J Nucl Mater, 2007; 367－370: 48

[8] Tamura M, Kumagai T, Sakai K, Shinozuka K, Esaka H. J Nucl Mater, 2011; 417: 29

[9] Abe F, Taneike M, Sawada K. Int J Pressure Vessels Piping, 2007; 84(1－2): 3

[10] Abe F, Horiuchi T, Taneike M, Sawada K. Mater Sci Eng, 2004; A378: 299

[11] Gutierrez N Z, Cicco H D, Marrero J, Danon C A, Luppo M I. Mater Sci Eng, 2011; A528: 4019

[12] Masuyama F. ISIJ Int, 2001; 41: 612

[13] Hollner S, Fournier B, Le Pendu J, Cozzika T, Tournie I,Brachet J C, Pineau A. J Nucl Mater, 2010; 405: 101

[14] Taneike M, Abe F, Sawada K. Nature, 2003; 424: 294

[15] Cipolla L, Danielsen H K, Venditti D, Nunzio P E D, Hald J, Somers M A J. Acta Mater, 2010; 58: 669

[16] Sawada K, Kushima H, Tabuchi M, Kimura K. Mater Sci Eng, 2011; A528: 5511

[17] Zhu F X, Liu C, Wang P, Gao D F, Gao C, Zhu C Q, Ni G Z. Steel Pipe, 1999; 28(1): 8

(朱伏先, 刘川, 王平, 高德福, 高潮, 祝春清, 倪国政. 钢管, 1999; 28(1): 8)

[18] Pan J S, Tong J M, Tian M B. Fundamentals of Materials Science. Beijing:Tsinghua University Press, 2009: 526

(潘金生, 仝健民, 田民波. 材料科学基础. 北京: 清华大学出版社, 2009: 526)

[19] Foley D C, Hartwig K T, Maloy S A, Hosemann P, Zhang X. J Nucl Mater, 2009; 389: 221

[20] Sivaprasad P V, Mannan S L, Prasad Y V R K. Mater Sci Technol, 2004; 20: 1545

[21] Tamura M, Sakasegawa H, Kohyama A, Esaka H, Shinozuka K. J Nucl Mater, 2003; 321: 288

[22] Yamada K, Igarashi M, Muneki S, Abe F. ISIJ Int, 2002; 42: 779

[23] Schneider A, Inden G. Acta Mater, 2005; 53: 519

[24] Tsukada Y, Shiraki A, Murata Y, Takaya S, Koyama T, Morinaga M. J Nucl Mater, 2010;401: 154

[25] Rojas D, Garcia J, Prat O, Carrasco C, Sauthoff G, Kaysser－Pyzalla A R.Mater Sci Eng, 2010; A527: 3864

[26] Yong Q L. The Second Phase in Iron and Steels. Beijing: Metallurgical Industry Press, 2006: 284

(雍岐龙. 钢铁材料中的第二相. 北京: 冶金工业出版社, 2006: 284)

[27] Prat O, Garcia J, Rojas D, Carrasco C, Inden G. Acta Mater, 2010; 58: 6142

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