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Acta Metall Sin  1994, Vol. 30 Issue (14): 91-96    DOI:
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PREPARATION OF Ni-Al INTERMETALLIC COMPOUNDS BY MECHANICAL ALLOYING
LI Gusong;DING Bingzhe;MIAO Weifang;YE Lilei;GUO Jianting(State Key La boratory of RSA;Institute of Metal Research;The Chinese Academy of Sciences;Shenyang)(Manuscript received 30 June;1993;in revised form 18 August;1993)
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LI Gusong;DING Bingzhe;MIAO Weifang;YE Lilei;GUO Jianting(State Key La boratory of RSA;Institute of Metal Research;The Chinese Academy of Sciences;Shenyang)(Manuscript received 30 June;1993;in revised form 18 August;1993). PREPARATION OF Ni-Al INTERMETALLIC COMPOUNDS BY MECHANICAL ALLOYING. Acta Metall Sin, 1994, 30(14): 91-96.

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Abstract  The powder mixtures of Ni and Al with compositions of Ni50 at.-% Al and Ni-25 at.-% Al as well as Ni_3Al alloy powder were milled in a Spex 8000 Mixer/Mill respectively.After 3 h of milling,Ni-50 at.-%Al mixture transforms into NiAl with grain size of about 5 nm,while after 5 h,Ni-25 at.-%Al mixture transforms into disordered metastable Ni solid solution.As to the Ni_3Al alloy powder,5 h milling makes its structure change from Ll_2-type intermetallic compound with long range order into fcc disordered solid solution;further milling results in the formation of nanocrystalline structure.
Key words:  intermetallic compound      mechanical alloying      nanocrystalline structure      Ni      Al      Ni_3Al      NiAl     
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