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Acta Metall Sin  1994, Vol. 30 Issue (21): 407-412    DOI:
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MORPHOLOGY OF ION-NITRIDED LAYER AND STRUCTURE OF γ'/ε INTERFACES
LI Fengzhao;SUN Dongsheng; AO Qing(Shandong University of Technology; Jinan; Laboratory of Atomic Imaging of Solids;Institute of Metal Research;Chinese Academy of Sciences;Shenyang);DAI Jiyan;LI Douxing (Laboratory of Atomic Imaging of solids;Institute of Metal Research;Chinese Academy of Scicnces; Shenyang)
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LI Fengzhao;SUN Dongsheng; AO Qing(Shandong University of Technology; Jinan; Laboratory of Atomic Imaging of Solids;Institute of Metal Research;Chinese Academy of Sciences;Shenyang);DAI Jiyan;LI Douxing (Laboratory of Atomic Imaging of solids;Institute of Metal Research;Chinese Academy of Scicnces; Shenyang). MORPHOLOGY OF ION-NITRIDED LAYER AND STRUCTURE OF γ'/ε INTERFACES. Acta Metall Sin, 1994, 30(21): 407-412.

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Abstract  The morphologies and the interface structures of ion-nitrided layers, which were obtained by ion nitriding of 35CrMo steel at 550 ℃ for 6 h, were studied with JEM-H800 TEM and JEM 2000 EX II HRTEM. The results show that the structures of theouter layer of ion-nitriding are s (Fe_2-3N)-phase and γ′(Fe_4N)-phase, which are arranged in alternating, ribbon-like strips. There are many various crystal defects, such as vacancies, dislocations,stacking faults,and twins in the internal layer compound——the γ′- phase. The interfaces between ε-phase and γ′ -phase are smooth and straight. Ledges of monoatom layers and multiatom layers were found. The existance of a number of crystal defects is the main reason why ion bombing accelerates the nitriding process.
Key words:  ion-nitrided layer      morphology      interface structure      steel 35 CrMo     
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