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金属学报  2026, Vol. 62 Issue (6): 1043-1058    DOI: 10.11900/0412.1961.2025.00350
  研究论文 本期目录 | 过刊浏览 |
热处理对FGH96高温合金惯性摩擦焊接头微观组织演变及力学性能的影响
王彬1, 赵鹏2, 刘家伟1, 张春波3, 秦志伟1, 董红刚1, 李鹏1()
1 大连理工大学 材料科学与工程学院 大连 116024
2 中国航发动力股份有限公司 西安 710021
3 中国机械总院集团哈尔滨焊接研究所有限公司 哈尔滨 150028
Effect of Heat Treatment on Microstructural Evolution and Mechanical Properties of Inertial Friction Welded Joints for FGH96 Superalloy
WANG Bin1, ZHAO Peng2, LIU Jiawei1, ZHANG Chunbo3, QIN Zhiwei1, DONG Honggang1, LI Peng1()
1 School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024, China
2 AECC Aviation Power Co. Ltd., Xi'an 710021, China
3 CAM Harbin Welding Institute Limited Company, Harbin 150028, China
引用本文:

王彬, 赵鹏, 刘家伟, 张春波, 秦志伟, 董红刚, 李鹏. 热处理对FGH96高温合金惯性摩擦焊接头微观组织演变及力学性能的影响[J]. 金属学报, 2026, 62(6): 1043-1058.
Bin WANG, Peng ZHAO, Jiawei LIU, Chunbo ZHANG, Zhiwei QIN, Honggang DONG, Peng LI. Effect of Heat Treatment on Microstructural Evolution and Mechanical Properties of Inertial Friction Welded Joints for FGH96 Superalloy[J]. Acta Metall Sin, 2026, 62(6): 1043-1058.

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摘要: 

针对惯性摩擦焊接头焊核区(WZ)强化相溶解和轴向/径向微观组织不均匀等固有工艺瓶颈,本工作提出一种基于FGH96高温合金惯性摩擦焊接头的焊后热处理精细化调控策略,系统研究了固溶时效和双级时效处理对接头微观组织演变及力学性能的影响规律。结果表明,随着固溶温度升高,接头晶粒尺寸和再结晶程度增加,γ′强化相的析出和长大更为显著,碳化物分布趋于均匀,WZ晶界锯齿化加剧。当固溶温度达到1140 ℃时,晶粒发生异常长大,γ′强化相粗化且分布不均。随固溶温度升高,固溶时效处理后接头冲击韧性提升,抗拉强度则呈现先增后降的趋势。当固溶温度为1080 ℃时,晶粒和γ′强化相尺寸适中且分布均匀,再结晶和晶界锯齿化程度较高,碳化物均匀弥散分布,接头沿轴/径向的微观组织不均匀性明显改善。接头在室温和750 ℃时的抗拉强度分别为1455和1042 MPa,室温冲击韧性为41 J/cm2,实现了接头强度与韧性的良好协同。双级时效处理促进焊缝区三次γ′强化相均匀析出,使接头在室温和750 ℃时的抗拉强度分别达到1574和1279 MPa,基本达到母材强度。同时,接头硬度显著提升并超过母材,但冲击韧性较焊态接头略有下降。

关键词 焊后热处理惯性摩擦焊接γ′强化相微观组织力学性能    
Abstract

Aero engines serve as a critical indicator of national comprehensive strength and technological advancement. However, their performance enhancement poses considerable challenges to the manufacturing technologies of hot-end components. Hot-end structures undergo inertial friction welding, which effectively avoids the defects associated with fusion welding and has been widely adopted for high-quality joining of these structures. This study addresses the inherent process limitations of inertial friction welded joints, including strengthening phase dissolution within the welding zone (WZ), along with axial and radial microstructural heterogeneity, and proposes a customized post-weld heat treatment (PWHT) strategy for inertial friction welded joints of FGH96 superalloys. A systematic investigation was conducted on the effects of solution aging and double aging on microstructural evolution and mechanical properties. The results indicated that increasing the solution temperature leads to grain coarsening and enhanced recrystallization, accompanied by pronounced precipitation and growth of the γ′ strengthening phase, a more uniform carbide distribution, and intensified grain boundary serration within the WZ compared to joints at low solution temperature. At a solution temperature of 1140 oC, abnormal grain growth occurred, along with coarsening and inhomogeneous distribution of the γ′ strengthening phase. After solution aging, the impact toughness of the joints improved with increasing solution temperature, whereas the tensile strength initially increased and then decreased. At the solution temperature of 1080 oC, the grain size and γ′ strengthening phase were moderate and uniformly distributed, the degree of recrystallization and grain boundary serration were relatively high, carbides were uniformly dispersed, and microstructural inhomogeneity was notably improved. Under this condition, the ultimate tensile strengths of the joints at room temperature and 750 °C were 1455 and 1042 MPa, respectively; and the impact toughness reached 41 J/cm2, demonstrating an optimal strength-toughness synergy. Double aging promoted the uniform precipitation of tertiary γ′ strengthening phase in the WZ, resulting in tensile strengths of 1574 and 1279 MPa at room temperature and 750 oC, respectively, approaching base metal levels. Meanwhile, the hardness was considerably enhanced beyond the base metal, although the impact toughness was slightly reduced compared with the as-welded joints.

Key wordspost-weld heat treatment    inertial friction welding    γ′ strengthening phase    microstructure    mechanical property
收稿日期: 2025-10-31     
ZTFLH:  TG132.3  
基金资助:国家自然科学基金项目(52375313);国家自然科学基金项目(51605075)
通讯作者: 李 鹏,lipeng2016@dlut.edu.cn,主要从事固相焊接理论与技术研究
Corresponding author: LI Peng, professor, Tel: (0411)84706283, E-mail: lipeng2016@dlut.edu.cn
作者简介: 王 彬,男,1999年生,博士
图1  微观组织形貌、热处理工艺流程、焊接设备照片以及组织观察和力学测试试样取样位置
图2  焊态及不同焊后热处理态接头中沿轴向晶粒分布的反极图(IPF)
图3  焊态及不同焊后热处理态接头的平均晶粒尺寸分布
图4  焊态及不同焊后热处理态接头沿轴向的晶粒分布图
图5  焊态及不同焊后热处理态接头沿轴向的晶粒占比
图6  焊态及不同焊后热处理态接头焊核区(WZ)和母材(BM)区强化相分布的SEM像
图7  焊态及不同焊后热处理态接头WZ和母材区晶界和碳化物的SEM像
图8  焊态接头不同区域微观组织的IPF
图9  焊态接头沿径向的特殊晶界分析
图10  1080 ℃ SA接头微观组织的IPF
图11  1080 ℃ SA接头平均晶粒尺寸分布
图12  焊态及焊后热处理态接头的显微硬度
图13  焊后热处理态接头的力学性能
图14  焊后热处理态接头照片和断口形貌的SEM像
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