First Exploration of Hot Isostatic Pressing High-Throughput Synthesis on Fe-Co-Ni Combinatorial Alloy

doi:10.11900/0412.1961.2021.00070

Acta Metall Sin

2021, Vol. 57

Issue (12): 1627-1636 DOI: 10.11900/0412.1961.2021.00070

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First Exploration of Hot Isostatic Pressing High-Throughput Synthesis on Fe-Co-Ni Combinatorial Alloy

ZHAO Lei¹^,², WANG Hui¹^,², YANG Lixia¹^,², CHEN Xuebin³, LANG Runqiu³, HE Linfeng⁴, CHEN Dongfeng⁴, WANG Haizhou¹^,²(

)

^1.Beijing Advanced Innovation Center for Materials Genome Engineering, Central Iron & Steel Research Institute, Beijing 100081, China
^2.Beijing Key Laboratory of Metal Materials Characterization, The NCS Testing Technology Co. , Ltd. , Beijing 100081, China
^3.National Center for Materials Service Safety, University of Science and Technology Beijing, Beijing 100083, China
^4.Department of Nuclear Physics, China Institute of Atomic Energy, Beijing 102413, China

Cite this article:

ZHAO Lei, WANG Hui, YANG Lixia, CHEN Xuebin, LANG Runqiu, HE Linfeng, CHEN Dongfeng, WANG Haizhou. First Exploration of Hot Isostatic Pressing High-Throughput Synthesis on Fe-Co-Ni Combinatorial Alloy. Acta Metall Sin, 2021, 57(12): 1627-1636.

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Abstract

Material genome engineering (MGE) is an advanced research concept that integrates high-throughput computing, high-throughput experiment (synthesis and characterization), and a special database. The purpose of MGE is to adopt an efficient and economical method to accelerate the correlation between the composition, microstructure, and performance. However, low composition, small size, characterization difficulty, and high cost limit its application in the high-throughput synthesis of a bulk metal. A new high-throughput synthesis based on hot isostatic pressing (HIP), which uses a honeycomb structure sleeve made of pure Ni and Ti foils, was proposed. A combinatorial-bulk-alloy with 19 gradient components was HIPed by filling different mixtures of pure Fe, Co, and Ni powders into each cell of the honeycomb sleeve. The high-throughput characterization of the composition and microstructure showed that the composition of each cell was homogeneous and in accordance with the design, the mixed powders diffused to the alloy phases, and the bulk alloy had good density and without macroscopic defects. The mechanism of alloying and its effect on the mechanical behavior was discussed by investigating the microhardness of Fe-Co-Ni combinatorial alloy. Fe- and Ni-based alloys were solid solution and second phase strengthened, whereas Co-based alloy was two-phase solid solution strengthened. The strengthening effect of Ni was better than that of Co for Fe-based alloy. The strengthening effect of Fe was better than that of Co for Ni-based alloy. The strengthening effect of Ni was better than that of Fe for Co-based alloy.

Key words: hot isostatic pressing honeycomb structure sleeve high-throughput synthesis combinatorial alloy Fe-Co-Ni

Received: 07 February 2021

ZTFLH:

TG142.71

Fund: National Key Research and Development Program of China(2017YFB0701900)

About author: WANG Haizhou, professor, Tel: (010) 62181950, E-mail: wanghaizhou@ncschina.com

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	Articles by authors
	Lei ZHAO
	Hui WANG
	Lixia YANG
	Xuebin CHEN
	Runqiu LANG
	Linfeng HE
	Dongfeng CHEN
	Haizhou WANG

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https://www.ams.org.cn/EN/10.11900/0412.1961.2021.00070 OR https://www.ams.org.cn/EN/Y2021/V57/I12/1627

Fig.1 Hot isostatic pressing (HIP) high-throughput synthesis process

Table 1 Composition details of 19 Fe-Co-Ni alloys system

Fig.2 Composition distributions and intensities of Fe (a), Co (b), and Ni (c) in the combinatorial alloys

Fig.3 Two dimensional projections of combinatorial alloys via neutron imaging (a) and the gray value curve of neutron images with different compositions (b)

Fig.4 OM (a-i) and SEM (j-l) images of the combinatorial alloy

Fig.5 XRD spectra of the combinatorial alloys

Fig.6 Hardnesses of the combinatorial alloys

Fig.7 Contour map of relationship between composition and hardness in 19 combinatorial alloys

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