Please wait a minute...
Acta Metall Sin  2025, Vol. 61 Issue (9): 1438-1448    DOI: 10.11900/0412.1961.2023.00451
Research paper Current Issue | Archive | Adv Search |
Mesomechanical Modeling and Experimental Study of Effective Elastic Tensors in Additively Manufactured Titanium Alloys
TAN Ruohan1, SONG Yongfeng1,2, CHEN Chao3, LI Dan3, CHENG Shu1, LI Xiongbing1()
1 School of Traffic & Transportation Engineering, Central South University, Changsha 410075, China
2 State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment, Guangdong University of Technology, Guangzhou 510006, China
3 Powder Metallurgy Research Institute, Central South University, Changsha 410083, China
Cite this article: 

TAN Ruohan, SONG Yongfeng, CHEN Chao, LI Dan, CHENG Shu, LI Xiongbing. Mesomechanical Modeling and Experimental Study of Effective Elastic Tensors in Additively Manufactured Titanium Alloys. Acta Metall Sin, 2025, 61(9): 1438-1448.

Download:  HTML  PDF(2522KB) 
Export:  BibTeX | EndNote (RIS)      
Abstract  

Additively manufactured (AM) Ti-6Al-4V alloys are known for their lightweight and superior mechanical properties and are increasingly being favored in the aerospace, energy, and biomedical industries. Among the available AM technologies, selective laser melting (SLM) stands out for its ability to fabricate complex-shaped Ti-6Al-4V efficiently and economically through near-net-shape manufacturing. Despite their advantages, SLM-produced parts often suffer from mechanical anisotropy and contain microdefects such as pores, cracks, and residual stresses, restricting their wider application. Addressing these issues requires a thorough understanding of the effects of texture and porosity on the mechanical properties of AM materials, which is necessary for developing components that comply with strict industry standards. Previous research has predominantly focused on studying the impact of texture or porosity on material properties, overlooking the interplay between these two critical factors. This work introduces an advanced modified Mori-Tanaka (MMT) model that simultaneously considers both texture and porosity in dual-phase AM Ti-6Al-4V alloys. This model enhances the traditional Mori-Tanaka approach by integrating it with the differential method, facilitating a nuanced analysis of how texture and porosity jointly influence the mechanical behavior of polycrystals. For model development, phase transitions and grain orientations are characterized using EBSD, whereas the 3D Gaussian distribution function describes the texture distribution within the polycrystal. Micro/nano computed tomography (CT) plays a pivotal role in determining the volume fraction and morphology of pores, providing crucial data for the model. These parameters were incorporated into the mesomechanical model to analyze the effective elastic stiffness tensor and Young's modulus, quantifying their collective impact on the alloy's mechanical properties. To validate the model, tensile and ultrasonic tests are conducted for two samples with different porosities and textures and compared their outcomes to evaluate the material's mechanical behavior, which exhibits characteristics of transverse isotropy. The comparison highlights the MMT model's superior precision, especially at higher porosity levels, with mean absolute percentage errors (MAPE) between Young's modulus obtained from the MMT model and the tensile test for two samples were 0.87% and 2.51%, respectively. Similarly, the MAPE between the effective elastic stiffness tensor derived from the MMT model and the ultrasonic test were 9.47% and 4.45%, respectively. These findings underscore the model's effectiveness in predicting material properties and its potential as a robust tool for exploring the interactions between microstructural elements and macroscopic mechanical properties of AM polycrystalline materials.

Key words:  effective elastic tensor      additive manufacturing      titanium alloy      anisotropy      modified MT model      porosity      texture     
Received:  14 November 2023     
ZTFLH:  TB301  
Fund: Hunan Provincial Science and Technology Innovation Leading Talent Project(2023RC1015);Natural Science Foundation of Hunan Province(2023JJ60159)
Corresponding Authors:  LI Xiongbing, professor, Tel: 15084761518, E-mail: lixb213@csu.edu.cn

URL: 

https://www.ams.org.cn/EN/10.11900/0412.1961.2023.00451     OR     https://www.ams.org.cn/EN/Y2025/V61/I9/1438

Fig.1  Flowchart of modified Mori-Tanaka (MMT) model in additively manufactured (AM) Ti-6Al-4V alloy (w is any initial plane layer, Ceff is effective elastic stiffness tensor, Cijeff is the component of Ceff, γ is Young's modulus. Samples A and B are manufactured with different printing parameters)
Phasec11c12c13c33c44
α170927019252
β138108--51
Table 1  Single crystal elastic constant (c(r)) of Ti-6Al-4V alloy[19]
SamplePhasefp / %qpJ
Aβ0.86133843.94
α87.6113689183.31
Bβ1.66258922.20
α81.3412709801.26
Table 2  EBSD analysis results of AM Ti-6Al-4V samples
Fig.2  Inverse pole figures (IPFs) paralleling to axis Z (a1, b1), IPFs of reconstructed phase β (a2, b2), orientation distribution function (ODF) maps of phase β (a3, b3), and ODF maps of phase α (a4, b4) of AM Ti-6Al-4V sample A (a1-a4) and sample B (b1-b4) (θ—Euler angle)
Fig.3  Probability density distribution map of θ in AM Ti-6Al-4V sample
Fig.4  Pore reconfigurations of AM Ti-6Al-4V sample A (a) and sample B (b)
Fig.5  Probability density distribution maps of pore volume (a) and sphericity (b) in AM Ti-6Al-4V samples (Inset in Fig.5a shows the locally enlarged map)
SampleDirectionPmax / kNγ / GPa
AHorizontal14.52109.46
Vertical13.88125.11
BHorizontal15.56115.56
Vertical16.09126.12
Table 3  Maximum load (Pmax) and γ of AM Ti-6Al-4V samples in different directions
SampleC11effC22effC33effC44effC55effC66eff
A142.7 ± 1.0143.4 ± 0.2137.4 ± 0.444.1 ± 0.744.6 ± 0.443.2 ± 0.4
B169.4 ± 0.7168.6 ± 0.7171.6 ± 0.147.1 ± 2.246.8 ± 2.145.2 ± 1.2
Table 4  Ceff of AM Ti-6Al-4V samples measured by ultrasonic test
Fig.6  C11eff (a), C55eff (b), C13eff (c), and C23eff (d) of AM Ti-6Al-4V samples obtained by MMT model (Insets show the locally enlarged curves. n—iteration number)
Fig.7  C22eff of AM Ti-6Al-4V samples obtained by MMT model and sparse method (SM) (Inset shows the locally enlarged curves)
SampleIndicatorHorizontal γ / GPaVertical γ / GPaMAPE / %EC / %
AV-MMT107.86124.760.8799.51
R-MMT104.16121.663.8098.06
H-MMT106.02123.212.3398.80
V-SM107.41122.611.9399.02
R-SM103.74119.484.8697.53
H-SM105.58121.053.4098.28
Tensile test109.46125.11
BV-MMT115.46132.252.5198.20
R-MMT110.61128.232.9898.42
H-MMT111.55129.002.9398.49
V-SM114.99132.352.7298.19
R-SM110.58127.822.8398.45
H-SM112.80130.102.7798.59
Tensile test115.56126.12
Table 5  γ in different directions of AM Ti-6Al-4V alloy by MMT model, SM, and tensile test, along with its average absolute percentage error (MAPE) and equalization coefficient (EC)
SampleIndicator

C11eff

GPa

C22eff

GPa

C33eff

GPa

C44eff

GPa

C55eff

GPa

C66eff

GPa

MAPE

%

EC

%

AV-MMT152.60163.09157.3648.4240.5044.069.4794.35
Ultrasonic143.68143.23136.9244.1144.9843.18
BV-MMT165.65175.67170.3451.2543.3146.974.4598.49
Ultrasonic169.43169.60171.6047.0946.7945.21
Table 6  C11eff, C22eff, C33eff, C44eff, C55eff, and C66eff of AM Ti-6Al-4V alloy by MMT method and ultrasonic test, along with its MAPE and EC
[1] Tshephe T S, Akinwamide S O, Olevsky E, et al. Additive manufacturing of titanium-based alloys—A review of methods, properties, challenges, and prospects [J]. Heliyon, 2022, 8(3): e09041
[2] Li S J, Hou W T, Hao Y L, et al. Research progress on the mechanical properties of the biomedical titanium alloy porous structures fabricated by 3D printing technique [J]. Acta Metall. Sin., 2023, 59: 478
doi: 10.11900/0412.1961.2022.00566
李述军, 侯文韬, 郝玉琳 等. 3D打印医用钛合金多孔材料力学性能研究进展 [J]. 金属学报, 2023, 59: 478
doi: 10.11900/0412.1961.2022.00566
[3] Song B, Zhang J L, Zhang Y J, et al. Research progress of materials design for metal laser additive manufacturing [J]. Acta Metall. Sin., 2023, 59: 15
宋 波, 张金良, 章媛洁 等. 金属激光增材制造材料设计研究进展 [J]. 金属学报, 2023, 59: 15
[4] Vilaro T, Colin C, Bartout J D. As-fabricated and heat-treated microstructures of the Ti-6Al-4V alloy processed by selective laser melting [J]. Metall. Mater. Trans., 2011, 42A: 3190
[5] Liu W C, Huang J, Liu J W, et al. Experimental and crystal plasticity modelling study on the crack initiation in micro-texture regions of Ti-6Al-4V during high cycle fatigue tests [J]. Int. J. Fatigue, 2021, 148: 106203
[6] Ren Y M, Lin X, Huang W D. Research progress of microstructure and fatigue behavior in additive manufacturing Ti-6Al-4V alloy [J]. Rare Met. Mater. Eng., 2017, 46: 3160
任永明, 林 鑫, 黄卫东. 增材制造Ti-6Al-4V合金组织及疲劳性能研究进展 [J]. 稀有金属材料与工程, 2017, 46: 3160
[7] Cheng M, Lu Z G, Wu J, et al. Effect of thermal induced porosity on high-cycle fatigue and very high-cycle fatigue behaviors of hot isostatic-pressed Ti-6Al-4V powder components [J]. J. Mater. Sci. Technol., 2022, 98: 177
doi: 10.1016/j.jmst.2021.04.066
[8] Zhao T F, Zhang L, Huang M J. Effective elasticity tensors of fiber-reinforced composite materials with 2D or 3D fiber distribution coefficients [J]. Acta Mech., 2019, 230: 4175
[9] Man C S, Zhao D. Remarks on texture coefficients of polycrystals with improper crystallite symmetry [J]. J. Elast., 2020, 138: 111
[10] Sha G F. Explicit backscattering coefficient for ultrasonic wave propagating in hexagonal polycrystals with fiber texture [J]. J. Nondestr. Eval., 2018, 37: 51
[11] Li J, Rokhlin S I. Elastic wave scattering in random anisotropic solids [J]. Int. J. Solids Struct., 2016, 78-79: 110
[12] Park I, Moon J, Bae S, et al. Application of micro-CT to Mori-Tanaka method for non-randomly oriented pores in air-entrained cement pastes [J]. Constr. Build. Mater., 2020, 255: 119342
[13] Giraud A, Huynh Q V, Hoxha D, et al. Effective poroelastic properties of transversely isotropic rock-like composites with arbitrarily oriented ellipsoidal inclusions [J]. Mech. Mater., 2007, 39: 1006
[14] Yan H B. Determination of the effective modulus of the syntactic foam containing hollow spheres by differential scheme and Mori-Tanaka method [J]. J. Beijing Univ. Aeronaut. Astronaut., 2000, 26: 688
严寒冰. 用微分法及Mori-Tanaka法求解复合泡沫塑料的有效模量 [J]. 北京航空航天大学学报, 2000, 26: 688
[15] Gui J C, Ma T S, Chen P, et al. Anisotropic damage to hard brittle shale with stress and hydration coupling [J]. Energies, 2018, 11: 926
[16] Zhang Q G, Fan X Y, Chen P, et al. Geomechanical behaviors of shale after water absorption considering the combined effect of anisotropy and hydration [J]. Eng. Geol., 2020, 269: 105547
[17] Asef M R, Farrokhrouz M. A semi-empirical relation between static and dynamic elastic modulus [J]. J. Petrol. Sci. Eng., 2017, 157: 359
[18] Tan R H, Song Y F, Li X B, et al. Effective elastic stiffness tensor and ultrasonic velocities for 3D printed polycrystals with pores and texture [J]. Res. Nondestr. Eval., 2022, 33: 196
[19] Warwick J L W, Coakley J, Raghunathan S L, et al. Effect of texture on load partitioning in Ti-6Al-4V [J]. Acta Mater., 2012, 60: 4117
[20] Cho J H, Rollett A D, Oh K H. Determination of volume fractions of texture components with standard distributions in Euler space [J]. Metall. Mater. Trans., 2004A, 35: 1075
[21] Gong S, Li Z, Zhao Y Y. An extended Mori-Tanaka model for the elastic moduli of porous materials of finite size [J]. Acta Mater., 2011, 59: 6820
[22] Simonelli M, Tse Y Y, Tuck C. Effect of the build orientation on the mechanical properties and fracture modes of SLM Ti-6Al-4V [J]. Mater. Sci. Eng., 2014, A616: 1
[23] Bozzolo N, Gerspach F, Sawina G, et al. Accuracy of orientation distribution function determination based on EBSD data—A case study of a recrystallized low alloyed Zr sheet [J]. J. Microsc., 2007, 227: 275
[24] Simonelli M, Tse Y Y, Tuck C. On the texture formation of selective laser melted Ti-6Al-4V [J]. Metall. Mater. Trans., 2014, 45A: 2863
[25] Huang S S, Ma Y J, Zhang S L, et al. Influence of alloying elements partitioning behaviors on the microstructure and mechanical properties in α + β titanium alloy [J]. Acta Metall. Sin., 2019, 55: 741
黄森森, 马英杰, 张仕林 等. α + β两相钛合金元素再分配行为及其对显微组织和力学性能的影响 [J]. 金属学报, 2019, 55: 741
doi: 10.11900/0412.1961.2018.00460
[26] Kasperovich G, Haubrich J, Gussone J, et al. Correlation between porosity and processing parameters in TiAl6V4 produced by selective laser melting [J]. Mater. Des., 2016, 105: 160
[27] Ge J G, Yan X C, Lei Y P, et al. A detailed analysis on the microstructure and compressive properties of selective laser melted Ti6Al4V lattice structures [J]. Mater. Des., 2021, 198: 109292
[28] Liu Z, Liu J R, Zhao Z B, et al. Microstructure and tensile property of TC4 alloy produced via electron beam rapid manufacturing [J]. Acta Metall. Sin., 2019, 55: 692
doi: 10.11900/0412.1961.2019.00007
刘 征, 刘建荣, 赵子博 等. 电子束快速成形制备TC4合金的组织和拉伸性能分析 [J]. 金属学报, 2019, 55: 692
[29] Banerjee D, Williams J C. Perspectives on titanium science and technology [J]. Acta Mater., 2013, 61: 844
[30] Yuan M D, Dai A B, Ma J T, et al. Nondestructive measurement of anisotropic elastic constants of selective laser melted 316L based on a tri-mode ultrasonic method [J]. Meas. Sci. Technol., 2023, 34: 045101
[31] Dai A B, Yuan M D, Wu J W, et al. Nondestructive characterization of elastic constants for 316L parts by selective laser melting based on dual-mode ultrasonic transducer [J]. Chin. J. Sci. Instrum., 2021, 42(6): 95
戴安帮, 袁懋诞, 吴俊伟 等. 基于双模式超声换能器的选择性激光熔化316L制件弹性常数无损表征研究 [J]. 仪器仪表学报, 2021, 42(6): 95
[32] Prioul R, Bakulin A, Bakulin V. Nonlinear rock physics model for estimation of 3D subsurface stress in anisotropic formations: Theory and laboratory verification [J]. Geophysics, 2004, 69: 415
[33] Mishra N, Das K. A Mori-Tanaka based micromechanical model for predicting the effective electroelastic properties of orthotropic piezoelectric composites with spherical inclusions [J]. SN Appl. Sci., 2020, 2: 1206
[34] Wu J. Thermal expansion coefficient prediction of asphalt mixture with the Eshelby equivalent inclusion theory [J]. Appl. Mech. Mater., 2014, 584-586: 1071
[35] Zhang Y, Han L. Foundation of Mesomechanics [M]. Beijing: Science Press, 2014: 91
张 研, 韩 林. 细观力学基础 [M]. 北京: 科学出版社, 2014: 91
[36] Yang J J, Yu H C, Wang Z M, et al. Effect of crystallographic orientation on mechanical anisotropy of selective laser melted Ti-6Al-4V alloy [J]. Mater. Charact., 2017, 127: 137
[37] Yang L, Zhao F, Jiang L, et al. Development of composition and heat treatment process of 2000 MPa grade spring steels assisted by machine learning [J]. Acta Metall. Sin., 2023, 59: 1499
doi: 10.11900/0412.1961.2022.00047
杨 累, 赵 帆, 姜 磊 等. 机器学习辅助2000 MPa级弹簧钢成分和热处理工艺开发 [J]. 金属学报, 2023, 59: 1499
[38] Zhang S Y, Lin X, Chen J, et al. Influence of processing parameter on the microstructure and forming characterizations of Ti-6Al-4V titanium alloy after laser rapid forming processing [J]. Rare Met. Mater. Eng., 2007, 36: 1839
张霜银, 林 鑫, 陈 静 等. 工艺参数对激光快速成形TC4钛合金组织及成形质量的影响 [J]. 稀有金属材料与工程, 2007, 36: 1839
[1] XU Xiaoyan, FANG Chao, QIU Jianke, ZHANG Mengmeng, SHI Donggang, MA Yingjie, LEI Jiafeng, YANG Rui. Influence of Peak Stress on Room Temperature Dwell Effect in Ti6242 Compressor Disc Forging[J]. 金属学报, 2025, 61(8): 1141-1152.
[2] FAN Ronglei, CHEN Minghe, WU Dipeng, WU Yong. Prediction of Damage and Hot Forming Limit of TA32 Titanium Alloy Based on Crystal Plasticity Model[J]. 金属学报, 2025, 61(8): 1293-1304.
[3] ZHANG Mingchuan, XU Qinsi, LIU Yi, CAI Yusheng, MU Yiqiang, REN Dechun, JI Haibin, LEI Jiafeng. Effect of Hot-Pressing Temperature on the Microstructure and Properties of the Diffusion-Bonded Region of TC4 Alloy[J]. 金属学报, 2025, 61(8): 1183-1192.
[4] YANG Fan, PEI Shichao, LUO Xinrui, CHEN Yuxiang, LI Ningyu, CHANG Yongqin. Microstructure Evolution and Mechanical Properties of 6061 Aluminum Alloy Fabricated by Friction Stir Additive Manufacturing[J]. 金属学报, 2025, 61(8): 1129-1140.
[5] WU Zewei, YAN Junxiong, HU Li, HAN Xiuzhu. Abnormal Rolling Behavior and Deformation Mechanisms of Bimodal Non-Basal Texture AZ31 Magnesium Alloy Sheet at Medium Temperature[J]. 金属学报, 2025, 61(8): 1165-1173.
[6] SHANG Hongchun, TIAN Zhongwang, NIU Lanjie, FAN Chenyang, ZHANG Zhewei, LOU Yanshan. Yield Evolution Behavior Characterization and Crystal Plasticity Simulation for 5182-O Aluminum Alloy[J]. 金属学报, 2025, 61(8): 1276-1292.
[7] YOU Yunxiang, TAN Li, GAO Jingjing, ZHOU Tao, ZHOU Zhiming. Controlling the Texture of Mg-Al-Zn-Mn-Ca Magnesium Alloy by Hot Rolling-Shearing-Bending Process and Annealing[J]. 金属学报, 2025, 61(6): 866-874.
[8] ZHOU Xiaowei, Guo Yun, JING Xueyan, WANG Yuxin. Biologically Inspired Xanthium-Like Spherical Texture in Superhydrophobic Ni-Co-Zn Coatings and Their Anti-Icing Performances[J]. 金属学报, 2025, 61(5): 783-796.
[9] ZHAO Zhuoya, MENG Lingjian, LIN Peng, CAO Xiaoqing. Microstructure Evolution and Texture Formation Mechanism of α Phase During Continuous Through-Transus Thermal Compression of TC4 Titanium Alloy[J]. 金属学报, 2025, 61(5): 717-730.
[10] HUANG Ke, LI Xinzhi, FANG Xuewei, LU Bingheng. State-of-the-Art Progress and Outlook in Wire Arc Additive Manufacturing of Magnesium Alloys[J]. 金属学报, 2025, 61(3): 397-419.
[11] HAN Qifei, DI Xinglong, GUO Yueling, YE Shuijun, ZHENG Yuanxuan, LIU Changmeng. Microstructure and Mechanical Properties of Mg/Mg Bimetals Fabricated by Wire Arc Additive Manufacturing[J]. 金属学报, 2025, 61(2): 211-225.
[12] QI Min, WANG Qian, MA Yingjie, CAO Hemeng, HUANG Sensen, LEI Jiafeng, YANG Riu. Growth Behavior of Grain Boundary α Phase and Its Effect on the Microtexture During βα Phase Transformation in Ti6246 Titanium Alloys[J]. 金属学报, 2025, 61(2): 265-277.
[13] DAI Jincai, MIN Xiaohua, XIN Shewei, LIU Fengjin. Effect of Interstitial Element O on Cryogenic Mechanical Properties in β-Type Ti-15Mo Alloy[J]. 金属学报, 2025, 61(2): 243-252.
[14] YU Yunhe, XIE Yong, CHEN Peng, DONG Haokai, HOU Jixin, XIA Zhixin. Interfacial Compatibility for Laser Melting Deposition of CoCrNiCu Medium-Entropy Alloy on 316L Austenitic Stainless Steel Surface[J]. 金属学报, 2024, 60(9): 1213-1228.
[15] ZHOU Mu, WANG Qian, WANG Yanxu, ZHAI Zirong, HE Lunhua, LI Bing, MA Yingjie, LEI Jiafeng, YANG Rui. Effect of Prewelding Pretreatment on Welding Residual Stress of Titanium Alloy Thick Plate[J]. 金属学报, 2024, 60(8): 1064-1078.
No Suggested Reading articles found!