Three-Dimensional Characteristics and Morphological Evolution of Micro/Meso Pores inG20Mn5N Steel Castings
Huadong YAN,Hui JIN()
Jiangsu Key Laboratory of Engineering Mechanics, Department of Civil Engineering, Southeast University, Nanjing 211189, China
Cite this article:
Huadong YAN,Hui JIN. Three-Dimensional Characteristics and Morphological Evolution of Micro/Meso Pores inG20Mn5N Steel Castings. Acta Metall Sin, 2019, 55(3): 341-348.
Cast steel is an important metal material that is widely used in civil engineering due to its strength and ductility. However, a variety of casting defects such as micro/meso pores are usually present in the as-cast components and can lead to the degradation of mechanical properties. In this work, the initial micro/meso pores in the G20Mn5N low-alloy cast steel were investigated based on high resolution 3D X-ray tomography technology. Based on their formation mechanism and characteristics, pores were classified into gas, gas-shrinkage and shrinkage pores, and the parameters such as the number, size and sphericity of three types of pores have been counted and analyzed. Then the evolutionary behavior of micro/meso pores in G20Mn5N low-alloy cast steel specimens under monotonic tensile loading has also been studied. The results showed that the volume of gas pore was small and its sphericity coefficients were high. Compared with the gas pore, the shrinkage pore had large volume and more complex shape in space. The volume and sphericity coefficients of gas-shrinkage pore were between the gas pore and the shrinkage. Damage evolution to metallic materials can be divided into void nucleation, growth and coalescence. The void nucleation and growth law were investigated by statistical analysis, which showed that the evolution of the void density could be modeled by an empirical function, and the evolution of void average radius was not only related to void growth but also affected by void nucleation.
Fund: National Key Research and Development Program of China(2017YFC0805100);National Natural Science Foundation of China(51578137);Open Research Fund Program of Jiangsu Key Laboratory of Engineering Mechanics;Priority Academic Program Development of the Jiangsu Higher Education Institutions
Fig.1 Shape and dimension of notched specimen (unit: mm)
Fig.2 Average load-displacement curve of notched specimens and loading or unloading paths
Fig.3 Pores inspected with 3D X-ray tomography technology in the specimen gauge section(a) specimen 4 (b) specimen 5 (c) specimen 6 (d) specimen 7
Specimen
Pore type
Number
Voxel
Surface area / mm2
Sphericity
No.
Max.
Min.
Mean
Max.
Min.
Mean
Max.
Min.
Mean
4
Gas pore
98
159
20
50.66
0.08
0.02
0.03
0.70
0.51
0.56
Gas-shrinkage pore
84
678
24
89.74
0.23
0.02
0.05
0.50
0.41
0.47
Shrinkage pore
8
7315
212
1676.25
2.12
0.14
0.55
0.38
0.24
0.34
5
Gas pore
86
540
20
59.62
0.15
0.04
0.04
0.64
0.51
0.55
Gas-shrinkage pore
88
454
20
76.41
0.19
0.02
0.05
0.50
0.40
0.47
Shrinkage pore
10
779
38
289.90
0.32
0.04
0.15
0.39
0.33
0.37
6
Gas pore
102
210
20
52.04
0.09
0.02
0.03
0.66
0.51
0.55
Gas-shrinkage pore
87
622
20
115.61
0.23
0.02
0.07
0.50
0.41
0.46
Shrinkage pore
3
751
37
341.00
0.39
0.04
0.19
0.39
0.28
0.35
7
Gas pore
68
186
20
51.49
0.08
0.02
0.03
0.65
0.51
0.54
Gas-shrinkage pore
72
424
20
84.18
0.18
0.02
0.05
0.50
0.40
0.45
Shrinkage pore
11
1280
224
682.09
0.56
0.12
0.30
0.39
0.28
0.34
Table 1 Characterization informations of initial gas, gas-shrinkage and shrinkage pores in specimens 4~7
Fig.4 Morphologies and characteristics of representative micro/meso pores in G20Mn5N cast steel(a~c) gas pore (d~f) gas-shrinkage pore (g~i) shrinkage pore
Fig.5 Measured and fitted void density (N) in specimen 4 under the uniaxial tensile loading (εAxial—axial strain)
Fig.6 Evolution of average radius (Rarv) for different numbers of examined pores in the gauge section of specimen 4 during the uniaxial tensile loading
Fig.7 Scanning slices of the specimen 4 gauge section during the uniaxial tensile loading(a) εAxial=0.214 (b) εAxial=0.343 (c) εAxial=0.422 (d) εAxial=0.460
Fig.8 Pores inspected with 3D X-ray tomography technology in the gauge section of specimen 4 during the uniaxial tensile loading(a) εAxial=0.214 (b) εAxial=0.343 (c) εAxial=0.422 (d) εAxial=0.460
Fig.9 Low (a) and high (b) magnified fractured surface SEM image of specimen 4
[1]
Bao W, Xing L T, Qiu J H. The use of cast steel in steel structure [J]. Adv. Mater. Res., 2011, 183-185: 1918
[2]
Chen Y Y, Zhao X Z, Tong L W. Research and application of connections of structural steel casting [J]. Adv. Struct. Eng., 2010, 13: 441
[3]
Lee P D, Hunt J D. Hydrogen porosity in directionally solidified aluminium-copper alloys: A mathematical model [J]. Acta Mater., 2001, 49: 1383
[4]
Blair M, Monroe R, Beckermann C, et al. Predicting the occurrence and effects of defects in castings [J]. JOM, 2005, 57(5): 29
[5]
Liu C Y, Wu X, Wu N, et al. Structural damage identification based on rough sets and artificial neural network [J]. Sci. World J., 2014, 2014: 193284
[6]
Sigl K M, Hardin R A, Stephens R I, et al. Fatigue of 8630 cast steel in the presence of porosity [J]. Int. J. Cast Met. Res., 2004, 17: 130
[7]
Hardin R A, Beckermann C. Prediction of the fatigue life of cast steel containing shrinkage porosity [J]. Metall. Mater. Trans., 2009, 40A: 581.
[8]
Hardin R A, Beckermann C. Effect of porosity on deformation, damage, and fracture of cast steel [J]. Metall. Mater. Trans., 2013, 44A: 5316
[9]
Wang S G, Wang S C, Zhang L. Application of high resolution transmission X-ray tomography in material science [J]. Acta Metall. Sin., 2013, 49: 897
Wan Q, Zhao H D, Zou C. Three-dimensional characterization and distribution of micropores in aluminum alloy high pressure die castings [J]. Acta Metall. Sin., 2013, 49: 284
Yu C, Wu S C, Hu Y N, et al. Three-dimensional imaging of gas pores in fusion welded Al alloys by synchrotron radiation X-ray microtomography [J]. Acta Metall. Sin., 2015, 51: 159
Maire E. X-ray tomography applied to the characterization of highly porous materials [J]. Annu. Rev. Mater. Res., 2012, 42: 163
[13]
Cao T S, Maire E, Verdu C, et al. Characterization of ductile damage for a high carbon steel using 3D X-ray micro-tomography and mechanical tests-application to the identification of a shear modified GTN model [J]. Comput. Mater. Sci., 2014, 84: 175
[14]
Lee S G, Gokhale A M, Patel G R, et al. Effect of process parameters on porosity distributions in high-pressure die-cast AM50 Mg-alloy [J]. Mater. Sci. Eng., 2006, A427: 99
[15]
Zió?kowski G, Chlebus E, Szymczyk P, et al. Application of X-ray CT method for discontinuity and porosity detection in 316L stainless steel parts produced with SLM technology [J]. Arch. Civ. Mech. Eng., 2014, 14: 608
[16]
Balasundaram A, Gokhale A M. Quantitative characterization of spatial arrangement of shrinkage and gas (air) pores in cast magnesium alloys [J]. Mater. Charact., 2001, 46: 419
[17]
Fansi J, Balan T, Lemoine X, et al. Numerical investigation and experimental validation of physically based advanced GTN model for DP steels [J]. Mater. Sci. Eng., 2013, A569: 1
[18]
Russell K C. The theory of void nucleation in metals [J]. Acta Metall., 1978, 26: 1615
[19]
Bieler T R, Crimp M A, Yang Y, et al. Strain heterogeneity and damage nucleation at grain boundaries during monotonic deformation in commercial purity titanium [J]. JOM, 2009, 61(12): 45
[20]
Landron C, Bouaziz O, Maire E, et al. Characterization and modeling of void nucleation by interface decohesion in dual phase steels [J]. Scr. Mater., 2010, 63: 973
[21]
Bouaziz O, Maire E, Giton M, et al. A model for initiation and growth of damage in dualphase steels identified by X-ray micro-tomography [J]. Metall. Res. Technol., 2008, 105: 102
[22]
Maire E, Bouaziz O, Di Michiel M, et al. Initiation and growth of damage in a dual-phase steel observed by X-ray microtomography [J]. Acta Mater., 2008, 56: 4954
[23]
Chu C C, Needleman A. Void nucleation effects in biaxially stretched sheets [J]. J. Eng. Mater. Technol., 1980, 102: 249
[24]
Zhao C F. Analysis method and application of multi-scale damage evolution of weld specimen with meso-defects [D]. Nanjing: Southeast University, 2016
Wang H. Evolution of microvoid and inclusion in metal materials [D]. Shanghai: Shanghai Jiao Tong University, 2005
[26]
王 华. 金属中微孔洞和夹杂的演变 [D]. 上海: 上海交通大学, 2005
[27]
Xin R S, Ma Q X, Li W Q. Microstructure and mechanical properties of internal crack healing in a low carbon steel [J]. Mater. Sci. Eng., 2016, A662: 65
[28]
Hu Z, Zhang Y, Teng H, et al. Research progress and prospect of crack healing in metal material [J]. Mater. Rev., 2014, 28(17): 47