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Acta Metall Sin  2019, Vol. 55 Issue (9): 1221-1230    DOI: 10.11900/0412.1961.2019.00097
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Microstructure and High-Temperature Deformation Behavior of Dissimilar Superalloy Welded Joint of DD407/IN718
LIU Yang,WANG Lei(),SONG Xiu,LIANG Taosha
Key Laboratory for Anisotropy and Texture of Materials, Ministry of Education, Northeastern University, Shenyang 110819, China
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LIU Yang,WANG Lei,SONG Xiu,LIANG Taosha. Microstructure and High-Temperature Deformation Behavior of Dissimilar Superalloy Welded Joint of DD407/IN718. Acta Metall Sin, 2019, 55(9): 1221-1230.

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Abstract  

Welding is an important joining method to fabricate the dissimilar welding integral blisk structure of single crystal and polycrystalline superalloy. The microstructure and properties of the welded joint are the key factors to determine the reliability of the integral blisk structure of dissimilar superalloys. The single crystal superalloy of DD407 and polycrystalline superalloy of IN718 were butt welded by continuous fiber laser system. The evolution of microstructure and composition segregation of the welded joints fabricated under the optimized welding parameters as-welded (AW) and after post weld heat treatment (PWHT) were investigated. The high temperature tensile deformation behavior of the welded joint after PWHT was also examined. The results show that the microstructures of fusion zone (FZ) in the welded joint consist of planar crystal, cellular crystal, columnar crystal and equiax crystal. The difference of the dendrite microstructures between the two sides of the weld centerline is very obvious. In terms of the joint as-welded, the microhardness of the FZ is low and there exists obvious micro-segregation. After PWHT, the micro-segregation has been improved and the microhardness increases significantly in the FZ which is much more than those of both base metals (BMs) of DD407 and IN718 alloys. There exists local hardening zone in the heat-affected zone (HAZ) of DD407 single crystal alloy and narrow softening zone and grain boundary liquation phenomenon in the HAZ of IN718 polycrystalline alloy. The ultimate tensile strength and elongation of the welded joint after tensile test at 650 ℃ are 1111 MPa and 9.42%, respectively. And the tensile specimen of the welded joint fails in the BM of IN718 polycrystalline alloy. The main deformation mode of the laser welded joint at high temperature includes the multi-slips of dislocation in the BM and FZ of single crystal alloy, and the dislocation slip and grain-boundary sliding in the BM of polycrystalline alloy. The tensile fracture surface is characterized by multi-source cracking, and the dimple and crystal sugar shaped facture surface exist simultaneously in the crack source area, which is a mixed fracture of microvoid aggregation and intergranular fracture. So the tensile fracture mechanism contains micro-void accumulation fracture and inter-granular fracture. The grain boundary liquefaction in the HAZ of IN718 polycrystalline does not affect the short-time high temperature mechanical properties of the welded joints.

Key words:  fiber laser welding      dissimilar welded joint of single crystal and polycrystalline alloy      dissimilar welded joint of single crystal and polycrystalline alloymicro-segregation      high-temperature deformation      fracture behavior     
Received:  03 April 2019     
ZTFLH:  TG132.32  
  TG407  
Fund: Supported by National Natural Science Foundation of China(Nos.51571052、 U1708253,51874090);Fundamental Research Funds for the Central Universities of China(No.180213006)

URL: 

https://www.ams.org.cn/EN/10.11900/0412.1961.2019.00097     OR     https://www.ams.org.cn/EN/Y2019/V55/I9/1221

MaterialCCrCoWMoAlTiNbTaFeNi
DD4070.0078.0505.5005.0002.2505.9502.000-3.500-Bal.
IN7180.04019.000--3.0500.5000.9005.250-Bal.52.500
Table 1  Chemical compositions of DD407 and IN718 alloys
Fig.1  Schematic of samplling positions (a) and geometry dimension (b) of specimens for the tensile test of the laser welded joint of DD407 and IN718 alloys (BMDD407—base metal of DD407, BMIN718—base metal of IN718, FZ—fusion zone)
Fig.2  Top and bottom surface morphologies (left) and overall views (right) of the laser welded joints of DD407 and IN718 alloys under different laser welding parameters (R—welding speed, P—laser power)(a) R=2.5 mm/min, P=1.8 kW (b) R=2.5 mm/min, P=2.0 kW (c) R=2.1 mm/min, P=1.4 kW(d) R=2.1 mm/min, P=1.6 kW (e) R=2.1 mm/min, P=1.8 kW
Fig.3  Microstructures of laser welded DD407/IN718 joint (Focus lens is 250 mm, defocus is -8 mm, welding power is 1600 W, welding speed is 2.1 mm/min. HAZDD407—heat-affected zone at DD407 side, HAZIN718—heat-affected zone at IN718 side)(a) microstructure of HAZDD407 (b) overall view (c) microstructure of HAZIN718 (d) γ' of BMDD407(e) microstructure of FZ (f) Laves phase on the boundary liquation in the HAZIN718(g) γ' of HAZDD407 near BMDD407 (h) dendrite structure of position for I zone in Fig.3b(i) γ' of HAZDD407 near FZ (j) dendrite structure of position for II zone in Fig.3b
Fig.4  SEM images showing the microstructure of the laser welded joint of DD407/IN718 after post weld heat treatment(PWHT) (The insets show the selected locations of Figs.4a and b)(a) microstructure of FZ (b) microstructure of HAZIN718
Fig.5  Microhardness distributions of the laser welded joint of DD407 and IN718 alloys as-welded (AW) and PWHT in the positions for I zone (a) and II zone (b) in Fig.3b
Fig.6  Element distributions of the welded joint of DD407 and IN718 alloys in the positions for I zone (a) and II zone (b) in Fig.3b
Fig.7  Stress-strain curves (a) and tensile properties (b) of the laser welded joint of DD407 and IN718 alloys and the corresponding BMs
Fig.8  SEM images showing tensile failure location and fracture morphology of laser welded joint of DD407/IN718 and corresponding base metals(a) tensile failure location (b) tensile fracture morphology of the laser welded joint of DD407/IN718 alloys(c) tensile fracture morphology of the BMIN718 (d) dimple fracture morphology of the welded joint(e) intergranular fracture morphlolgy of the welded joint (f) intergranular fracture morphlolgy of the BMIN718
Fig.9  SEM images of the laser welded joint of DD407 and IN718 alloys at the location of fusion line of DD407 (a, b), FZ of DD407 (c, d), FZ of IN718 (e, f) and fusion line of IN718 (g) in the positions for I zone (a, c, e, g) and II zone (b, d, f)
Fig.10  Low (a) and high (b) magnified SEM images showing micro-cracks near the fracture surface of the tensile specimen of the laser welded joint of DD407 and IN718 alloys
[1] HuangQ Y, LiH K. Superalloy [M]. Beijing: Metallurgical Industry Press, 2000: 22
[1] 黄乾尧, 李汉康. 高温合金 [M]. 北京: 冶金工业出版社, 2000: 22)
[2] ChenL, XiaX T, QiuM. Analysis and control of fretting wear for blade bearing in wind turbine [J]. Appl. Mech. Mater., 2010, 26-28: 167
[3] LiuQ Q. Fracture analysis for rotor blade tenon of an aeroengine compressor [J]. J. Mater. Eng., 1997, (6): 9
[3] 刘庆瑔. 某发动机压气机四级转子叶片榫头断裂分析 [J]. 材料工程, 1997, (6): 9)
[4] MishraR K, ThomasJ, SrinivasanK, , et al. Failure analysis of an un-cooled turbine blade in an aero gas turbine engine [J]. Eng. Fail. Anal., 2017, 79: 836
[5] FuY Z, GaoH, WangX P, , et al. Machining the integral impeller and blisk of aero-Engines: A review of surface finishing and strengthening technologies [J]. Chin. J. Mech. Eng., 2017, 30: 528
[6] HuangC F. Modern aeroengine integral blisk and its manufacturing technology [J]. Aeronaut. Manuf. Technol., 2006, (4): 94
[6] 黄春峰. 现代航空发动机整体叶盘及其制造技术 [J]. 航空制造技术, 2006, (4): 94)
[7] AschenbruckJ, AdamczukR, SeumeJ R. Recent progress in turbine blade and compressor blisk regeneration [J]. Proc. CIRP, 2014, 22: 256
[8] MateoA. On the feasibility of BLISK produced by linear friction welding [J]. Rev. Metal., 2014, 50(3): e023
[9] ChenG Q, ZhangB G, LüT M, , et al. Causes and control of welding cracks in electron-beam-welded superalloy GH4169 joints [J]. Trans. Nonferrous Met. Soc. China, 2013, 23: 1971
[10] ZhangD Y, NiuW, CaoX Y, , et al. Effect of standard heat treatment on the microstructure and mechanical properties of selective laser melting manufactured Inconel 718 superalloy [J]. Mater. Sci. Eng., 2015, A644: 32
[11] DuS G, WangX F, GaoM. Characteristics of the friction welding interface between single crystal superalloy DD3 and fine grained superalloy GH4169 [J]. Acta Metall. Sin., 2015, 51: 951
[11] 杜随更, 王喜锋, 高 漫. 单晶DD3与细晶GH4169高温合金摩擦焊接界面表征 [J]. 金属学报, 2015, 51: 951
[12] PouranvariM, EkramiA, KokabiA H. Solidification and solid state phenomena during TLP bonding of IN718 superalloy using Ni-Si-B ternary filler alloy [J]. J. Alloys Compd., 2013, 563: 143
[13] YanF, WangC M, WangY J, , et al. A study of the mechanism of laser welding defects in low thermal expansion superalloy GH909 [J]. Mater. Charact., 2013, 78: 21
[14] HuangW P, YuH C, YinJ, , et al. Microstructure and mechanical properties of K4202 cast nickel base superalloy fabricated by selective laser melting [J]. Acta Metall. Sin., 2016, 52: 1089
[14] 黄文普, 喻寒琛, 殷 杰等. 激光选区熔化成形K4202镍基铸造高温合金的组织和性能 [J]. 金属学报, 2016, 52: 1089
[15] LiuS, MiG Y, YanF, , et al. Correlation of high power laser welding parameters with real weld geometry and microstructure [J]. Opt. Laser Technol., 2017, 94: 59
[16] DongD Y, LiuY, WangL, , et al. Effect of strain rate on dynamic deformation behavior of laser welded DP780 steel joints [J]. Acta Metall. Sin., 2013, 49: 1493
[16] 董丹阳, 刘 杨, 王 磊等. 应变速率对DP780钢激光焊接接头动态变形行为的影响 [J]. 金属学报, 2013, 49: 1493
[17] LiY J, WangJ, LiuP. Welding of Badly Welding Dissimilar and Application [M]. Beijing: Chemical Industry Press, 2004: 1
[17] 李亚江, 王 娟, 刘 鹏. 异种难焊材料的焊接及应用 [M]. 北京: 化学工业出版社, 2004: 1)
[18] YuG, ZhaoS S, ZhangY J, , et al. Research on key issues of laser welding of dissimilar metal [J]. Chin. J. Lasers, 2009, 36: 261
[18] 虞 钢, 赵树森, 张永杰等. 异种金属激光焊接关键问题研究 [J]. 中国激光, 2009, 36: 261
[19] WeiC H, ZhangJ, YangS L, , et al. Microstructures and mechanical properties for laser tailor welded blanks of DP590 and low carbon steels [J]. J. Magn. Magn. Mater., 2013,42(suppl.2): 68
[20] OzakiH, KutsunaM. Laser-roll welding of a dissimilar metal joint of low carbon steel to aluminium alloy using 2 kW fibre laser [J]. Weld. Int., 2009, 23: 345
[21] LiuJ, ZhaoZ Y. Residual stress distribution of electron beam welded dissimilar superalloy sheet joints after heat treatment [J]. Trans. Mater. Heat Treat., 2016, 37(2): 245
[21] 刘 谨, 赵志毅. 异种高温合金板材电子束焊接及热处理后残余应力特征 [J]. 材料热处理学报, 2016, 37(2): 245)
[22] ChamanfarA, MonajatiH, RosenbaumA, , et al. Microstructure and mechanical properties of surface and subsurface layers in broached and shot-peened Inconel-718 gas turbine disc fir-trees [J]. Mater. Charact., 2017, 132: 53
[23] GuoJ T. Materials Science and Engineering for Superalloys (Book 1) [M]. Beijing: Science Press, 2008: 1
[23] 郭建亭. 高温合金材料学-上册 [M]. 北京: 科学出版社, 2008: 1)
[24] KhajaS, MehtaK K, BabuR V, , et al. Mechanical properties anisotropy of isothermally forged and precipitation hardened inconel 718 disk [J]. Metall. Mater. Trans., 2015, 46A: 1140
[25] WuD J, YinB, ZhangW Z, , et al. Nd: YAG laser beam welding invar36 alloy [J]. Chin. J. Lasers, 2008, 35: 1773
[25] 吴东江, 尹 波, 张维哲等. Nd: YAG激光焊接殷钢材料的工艺研究 [J]. 中国激光, 2008, 35: 1773
[26] KouS. Welding Metallurgy [M]. 2nd Ed., Hoboken: Wiley-Interscience, 2003: 56
[27] PangM, YuG, WangH H, , et al. Microstructure study of laser welding cast nickel-based superalloy K418 [J]. J. Mater. Process. Technol., 2008, 207: 271
[28] RamG D J, ReddyA V, RaoK P, , et al. Microstructure and tensile properties of inconel 718 pulsed Nd-YAG laser welds [J]. J. Mater. Process. Technol., 2005, 167: 73
[29] ThompsonE G. Hot-cracking studies of inconel 718 weld heat-affected zones [J]. Weld. J., 1969, 48: 70
[30] ThompsonR G, GenculuS. Microstructural evolution in the HAZ of inconel 718 and correlation with the hot ductility test [J]. Weld. J., 1983, 62: 337S
[31] ThompsonR G, CassimusJ J, MayoD E, , et al. The relationship between grain size and microfissuring in alloy 718 [J]. Weld. J., 1985, 64: 91
[32] LiuY C, GuoQ Y, LiC, , et al. Recent progress on evolution of precipi-tates in inconel 718 superalloy [J]. Acta Metall. Sin., 2016, 52: 1259
[32] 刘永长, 郭倩颖, 李 冲等. Inconel718高温合金中析出相演变研究进展 [J]. 金属学报, 2016, 52: 1259
[33] PengZ F, RenY Y, LuoY S, , et al. Characteristics of microstructure and element distribution of nickel-base single crystal superalloy CMSX-2 after high temperature creep [J]. Acta Metall. Sin., 2002, 38: 135
[33] 彭志方, 任遥遥, 骆宇时等. 镍基单晶合金CMSX-2高温蠕变后的显微组织及合金元素分布特征 [J]. 金属学报, 2002, 38: 135
[34] ShengL Y, YangF, GuoJ T, , et al. Anomalous yield and intermediate temperature brittleness behaviors of directionally solidified nickel-based superalloy [J]. Trans. Nonferrous Met. Soc. China, 2014, 24: 673
[35] HuG X, CaiX, RongY H. Fundamentals of Materials Science [M]. 3rd Ed., Shanghai: Shanghai Jiao Tong University Press, 2000: 172
[35] 胡庚祥, 蔡 珣, 戎咏华. 材料科学基础 [M]. 第3版, 上海: 上海交通大学出版社, 2000: 172)
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