Research paper

Effect of Electropulse on Dynamic Precipitation and Microstructure of AZ91 Magnesium Alloy During Warm Extrusion

  • WANG Binshan ,
  • XU Guang ,
  • REN Rui ,
  • ZHANG Qiang ,
  • SHAN Zhaohui ,
  • FAN Jianfeng
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  • 1 Key Laboratory of Interface Science and Engineering in Advanced Materials, Ministry of Education, Taiyuan University of Technology, Taiyuan 030024, China
    2 College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, China
    3 Shanxi Key Laboratory of Advanced Magnesium Based Materials, Taiyuan University of Technology, Taiyuan 030024, China
    4 College of Physics and Optoelectronics, Taiyuan University of Technology, Taiyuan 030024, China
FAN Jianfeng, professor, Tel: 13935107463, E-mail: fanjianfeng@tyut.edu.cn

Received date: 2024-08-14

  Revised date: 2024-10-28

  Online published: 2024-11-15

Supported by

Natural Science Foundation of Shanxi Province(20210302123134);Natural Science Foundation of Shanxi Province(202203021221071);Natural Science Foundation of Shanxi Province(202203021211157);Shanxi Scholarship Council of China(2022-045);Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering(2021SX-FR005)

Abstract

The electropulse-assisted forming process has been widely used in various plastic deformation applications owing to its advantages in improving formability and refining microstructure. However, the influence of electropulse on the dynamic extrusion deformation process remains unclear. In this study, the effects of electropulse on dynamic precipitation and microstructure evolution of AZ91 magnesium alloy during extrusion were investigated using electropulse-assisted extrusion (EPAE) technology. The results demonstrate that under critical deformation conditions for complete dynamic recrystallization, the EPAE process reduces the volume fraction of the β-Mg17Al12 phase, promotes its spheroidization, and enhances both the average grain size and the maximum basal texture intensity. These effects become more pronounced with increasing peak current density. Specifically, with a peak current density of 6.4 × 107 A/m2 during the EPAE process, the volume fraction of the β-Mg17Al12 phase decreased from 76.9% to 16.5%, the average grain size increased from 1.07 μm to 3.54 μm, and the maximum basal texture intensity increased from 3.39 to 5.92, compared to conventional hot extrusion. The bimodal structure observed in the EPAE-processed AZ91 alloy was attributed to the pinning effect caused by the inhomogeneous distribution of the β-Mg17Al12 phase. Experimental and theoretical analyses indicated that the increase of Gibbs free energy variation and atomic diffusion flux during extrusion of AZ91 alloy caused by the combined thermal and athermal effects of the pulsed current was the main reason for the experimental phenomena, which promoting the solution of β-Mg17Al12 phase and uniform distribution of Al solute atoms nearby while also increasing the grain boundary migration rate. Moreover, the electropulse strengthened the basal texture in β-Mg17Al12 particle-depleted regions by accelerating basal <a> slip.

Cite this article

WANG Binshan , XU Guang , REN Rui , ZHANG Qiang , SHAN Zhaohui , FAN Jianfeng . Effect of Electropulse on Dynamic Precipitation and Microstructure of AZ91 Magnesium Alloy During Warm Extrusion[J]. Acta Metall Sin, 2025 , 61(1) : 129 -142 . DOI: 10.11900/0412.1961.2024.00256

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