Critical Inclusion Size and Void Growth in Dual-Phase Ferrite-Bainite Steel During Ductile Fracture

  • ZHAO Yafeng ,
  • LIU Sujie ,
  • CHEN Yun ,
  • MA Hui ,
  • MA Guangcai ,
  • GUO Yi
Expand
  • 1Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
    2School of Materials Science and Engineering, Northeastern University, Shenyang 110819, China
    3Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

Received date: 2022-06-15

  Revised date: 2022-12-06

  Online published: 2023-03-16

Supported by

National Natural Science Foundation of China(52201149);National Science and Technology Major Project(J2019-VI-0019-0134);Strategic Priority Research Program of Chinese Academy of Sciences(XDC04000000);ERC CORREL-CT Project(695638)

Abstract

Ferrite-bainite dual-phase steel is widely used in the automotive industry owing to its high strength and excellent ductility. The impact of inclusions and void growth behavior in dual-phase steel is a major concern among researchers seeking to achieve better mechanical properties. To investigate this, a cross-length-scale multimodal method was employed to study the influence of local microstructures on void growth during ductile fracture of a dual-phase ferrite-bainite steel. During tensile testing, laboratory X-ray computed tomography (XCT) was used to measure the evolution of void volume. 3D-electron back scatter diffraction (3D-EBSD) provided information about the voids nucleated at both inclusion particles and bainite phases or their boundaries. Carefully controlled, broad-focused ion beam excavation was performed to reveal a new interface at a specific depth of the voids. Results showed that voids resulting from large inclusions are significantly bigger than either small inclusions or the bainite phase. Large inclusions lead to large voids even when the strain correlated with the growth of those voids is lower. An investigation of the dislocation densities surrounding the voids suggested that they may be related to the strain gradient around the different inclusion sizes. A critical inclusion size estimated to be around 1.85-2.86 μm was found below which nucleation occurs but with limited growth. The elevated rate of local dislocation multiplication due to local deformation gradient effects can impede the growth of smaller voids. The growth of voids is heterogeneous, and their shape correlates well with the deformability of the surrounding grains, as indicated by a Schmid factor weighted using the grain size. This weighted Schmid factor explains not only the shape of the voids but also sheds light on the ease of void coalescence based on the microstructures separating the voids.

Cite this article

ZHAO Yafeng , LIU Sujie , CHEN Yun , MA Hui , MA Guangcai , GUO Yi . Critical Inclusion Size and Void Growth in Dual-Phase Ferrite-Bainite Steel During Ductile Fracture[J]. Acta Metall Sin, 2023 , 59(5) : 611 -622 . DOI: 10.11900/0412.1961.2022.00293

References

1 Pierman A P, Bouaziz O, Pardoen T, et al. The influence of microstructure and composition on the plastic behaviour of dual-phase steels[J]. Acta Mater., 2014, 73: 298
2 Tasan C C, Diehl M, Yan D, et al. An overview of dual-phase steels: Advances in microstructure-oriented processing and micromechanically guided design[J]. Annu. Rev. Mater. Res., 2015, 45: 391
3 Matsuno T, Teodosiu C, Maeda D, et al. Mesoscale simulation of the early evolution of ductile fracture in dual-phase steels[J]. Int. J. Plast., 2015, 74: 17
4 Toda H, Takijiri A, Azuma M, et al. Damage micromechanisms in dual-phase steel investigated with combined phase- and absorption-contrast tomography[J]. Acta Mater., 2017, 126: 401
5 Pineau A, Benzerga A A, Pardoen T. Failure of metals I: Brittle and ductile fracture[J]. Acta Mater., 2016, 107: 424
6 Goods S H, Brown L M. Overview No. 1: The nucleation of cavities by plastic deformation[J]. Acta Metall., 1979, 27: 1
7 Babout L, Brechet Y, Maire E, et al. On the competition between particle fracture and particle decohesion in metal matrix composites[J]. Acta Mater., 2004, 52: 4517
8 Achouri M, Germain G, Dal Santo P, et al. Experimental characterization and numerical modeling of micromechanical damage under different stress states[J]. Mater. Des., 2013, 50: 207
9 Benzerga A A, Besson J, Pineau A. Anisotropic ductile fracture: Part I: Experiments[J]. Acta Mater., 2004, 52: 4623
10 Liang W, Yuan Q, Chen G H, et al. Fracture evolution in ferrite/martensite dual-phase flange steel[J]. Ironmak. Steelmak., 2021, 48: 88
11 Komori K. Simulation of the influence of Lode parameter on ductile fracture using an ellipsoidal void model[J]. Int. J. Solids Struct., 2021, 229: 111143
12 Marteleur M, Leclerc J, Colla M S, et al. Ductile fracture of high strength steels with morphological anisotropy, Part I: Characterization, testing, and void nucleation law[J]. Eng. Fract. Mech., 2021, 244: 107569
13 Kusche C F, Pütz F, Münstermann S, et al. On the effect of strain and triaxiality on void evolution in a heterogeneous microstructure—A statistical and single void study of damage in DP800 steel[J]. Mater. Sci. Eng., 2021, A799: 140332
14 Lubarda V A, Schneider M S, Kalantar D H, et al. Void growth by dislocation emission[J]. Acta Mater., 2004, 52: 1397
15 Greenwood G W, Harris J E. Note on vacancy condensation on particles[J]. Acta Metall., 1965, 13: 936
16 Ashby M F. Work hardening of dispersion-hardened crystals[J]. Philos. Mag., 1966, 14A: 1157
17 Bulatov V V, Wolfer W G, Kumar M. Shear impossibility: Comments on “Void growth by dislocation emission” and “Void growth in metals: Atomistic calculations”[J]. Scr. Mater., 2010, 63: 144
18 Gungor M R, Maroudas D, Zhou S J. Molecular-dynamics study of the mechanism and kinetics of void growth in ductile metallic thin films[J]. Appl. Phys. Lett., 2000, 77: 343
19 Segurado J, Llorca J. Discrete dislocation dynamics analysis of the effect of lattice orientation on void growth in single crystals[J]. Int. J. Plast., 2010, 26: 806
20 Scheyvaerts F, Pardoen T, Onck P R. A new model for void coalescence by internal necking[J]. Int. J. Damage Mech., 2010, 19: 95
21 Weck A, Wilkinson D S, Maire E, et al. Visualization by X-ray tomography of void growth and coalescence leading to fracture in model materials[J]. Acta Mater., 2008, 56: 2919
22 Pardoen T, Doghri I, Delannay F. Experimental and numerical comparison of void growth models and void coalescence criteria for the prediction of ductile fracture in copper bars[J]. Acta Mater., 1998, 46: 541
23 Tanaka K, Mori T, Nakamura T. Cavity formation at the interface of a spherical inclusion in a plastically deformed matrix[J]. Philos. Mag., 1970, 21A: 267
24 Gurson A L. Continuum theory of ductile rupture by void nucleation and growth: Part I—Yield criteria and flow rules for porous ductile media[J]. J. Eng. Mater. Technol., 1977, 99: 2
25 Tvergaard V. Influence of voids on shear band instabilities under plane strain conditions[J]. Int. J. Fract., 1981, 17: 389
26 Tvergaard V, Needleman A. Analysis of the cup-cone fracture in a round tensile bar[J]. Acta Metall., 1984, 32: 157
27 Burnett T L, McDonald S A, Gholinia A, et al. Correlative tomography[J]. Sci. Rep., 2014, 4: 4711
28 Slater T J A, Bradley R S, Bertali G, et al. Multiscale correlative tomography: An investigation of creep cavitation in 316 stainless steel[J]. Sci. Rep., 2017, 7: 7332
29 Daly M, Burnett T L, Pickering E J, et al. A multi-scale correlative investigation of ductile fracture[J]. Acta Mater., 2017, 130: 56
30 Ishikawa N, Yasuda K, Sueyoshi H, et al. Microscopic deformation and strain hardening analysis of ferrite-bainite dual-phase steels using micro-grid method[J]. Acta Mater., 2015, 97: 257
31 Burnett T L, Kelley R, Winiarski B, et al. Large volume serial section tomography by Xe plasma FIB dual beam microscopy[J]. Ultramicroscopy, 2016, 161: 119
32 Burnett T L, Winiarski B, Kelley R, et al. Xe+ plasma FIB: 3D microstructures from nanometers to hundreds of micrometers[J]. Microsc. Today, 2016, 24: 32
33 Watanabe R. Possible slip systems in body centered cubic iron[J]. Mater. Trans., 2006, 47: 1886
34 Weinberger C R, Boyce B L, Battaile C C. Slip planes in bcc transition metals[J]. Int. Mater. Rev., 2013, 58: 296
35 Nye J F. Some geometrical relations in dislocated crystals[J]. Acta Metall., 1953, 1: 153
36 Pantleon W. Resolving the geometrically necessary dislocation content by conventional electron backscattering diffraction[J]. Scr. Mater., 2008, 58: 994
37 Wilkinson A J, Meaden G, Dingley D J. High-resolution elastic strain measurement from electron backscatter diffraction patterns: New levels of sensitivity[J]. Ultramicroscopy, 2006, 106: 307
38 Britton T B, Liang H, Dunne F P E, et al. The effect of crystal orientation on the indentation response of commercially pure titanium: Experiments and simulations[J]. Proc. Roy. Soc., 2010, 466A: 695
39 Britton T B, Wilkinson A J. Stress fields and geometrically necessary dislocation density distributions near the head of a blocked slip band[J]. Acta Mater., 2012, 60: 5773
40 Guo Y, Collins D M, Tarleton E, et al. Dislocation density distribution at slip band-grain boundary intersections[J]. Acta Mater., 2020, 182: 172
41 Brown L M, Stobbs W M. The work-hardening of copper-silica V. Equilibrium plastic relaxation by secondary dislocations[J]. Philos. Mag., 1976, 34A: 351
42 Traiviratana S, Bringa E M, Benson D J, et al. Void growth in metals: Atomistic calculations[J]. Acta Mater., 2008, 56: 3874
43 Lavrentev F F. The type of dislocation interaction as the factor determining work hardening[J]. Mater. Sci. Eng., 1980, 46: 191
44 Guo Y, Schwiedrzik J, Michler J, et al. On the nucleation and growth of twin in commercial purity titanium: In situ investigation of the local stress field and dislocation density distribution[J]. Acta Mater., 2016, 120: 292
45 Zhao Z T, Wang X S, Qiao G Y, et al. Effect of bainite morphology on deformation compatibility of mesostructure in ferrite/bainite dual-phase steel: Mesostructure-based finite element analysis[J]. Mater. Des., 2019, 180: 107870
46 Fillafer A, Krempaszky C, Werner E. On strain partitioning and micro-damage behavior of dual-phase steels[J]. Mater. Sci. Eng., 2014, A614: 180
47 Brands D, Balzani D, Scheunemann L, et al. Computational modeling of dual-phase steels based on representative three-dimensional microstructures obtained from EBSD data[J]. Arch. Appl. Mech., 2016, 86: 575
48 Liu Y, Fan D W, Arroyave R, et al. Microstructure-based modeling of the effect of inclusion on the bendability of advanced high strength dual-phase steels[J]. Metals, 2021, 11: 431
49 Klevebring B I, Bogren E, Mahrs R. Determination of the critical inclusion size with respect to void formation during hot working[J]. Metall. Trans., 1975, 6A: 319
50 Ye Y G. Cavity nucleation, growth and stress field in elastic-plastic medium[J]. Acta Mech. Sol. Sin., 1990, 11: 201
  叶裕恭. 弹塑性材料中孔洞成核、发展及应力场[J]. 固体力学学报, 1990, 11: 201
51 Bomas H, Mayr P, Linkewitz T. Inclusion size distribution and endurance limit of a hard steel[J]. Extremes, 1999, 2: 149
52 Lee M, Kang N, Liu S, et al. Effects of inclusion size and acicular ferrite on cold cracking for high-strength steel welds of YS 600 MPa grade[J]. Sci. Technol. Weld. Joining, 2016, 21: 711
53 Wang P, Wang B, Liu Y, et al. Effects of inclusion types on the high-cycle fatigue properties of high-strength steel[J]. Scr. Mater., 2022, 206: 114232
54 Gu C, Wang M, Bao Y P, et al. Quantitative analysis of inclusion engineering on the fatigue property improvement of bearing steel[J]. Metals, 2019, 9: 476
55 Peng Z X, Liu J, Huang F, et al. Comparative study of non-metallic inclusions on the critical size for HIC initiation and its influence on hydrogen trapping[J]. Int. J. Hydrogen Energy, 2020, 45: 12616
56 Prithivirajan V, Sangid M D. The role of defects and critical pore size analysis in the fatigue response of additively manufactured IN718 via crystal plasticity[J]. Mater. Des., 2018, 150: 139
57 Chen Y H, Park S U, Wei D, et al. A dictionary approach to electron backscatter diffraction indexing[J]. Microsc. Microanal., 2015, 21: 739
58 Singh S, Guo Y, Winiarski B, et al. High resolution low kV EBSD of heavily deformed and nanocrystalline aluminium by dictionary-based indexing[J]. Sci. Rep., 2018, 8: 10991
59 Ashby M F, Gelles S H, Tanner L E. The stress at which dislocations are generated at a particle-matrix interface[J]. Philos. Mag., 1969, 19A: 757
60 Babout L, Maire E, Fougères R. Damage initiation in model metallic materials: X-ray tomography and modelling[J]. Acta Mater., 2004, 52: 2475
Outlines

/