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DETERMINATION OF σ-OR M_(23)C_6-PHASE IN STAINLESS STEEL BY STEP POTENTIAL ETCHING CURRENT METHOD |
MA Xiang Central Iron and Steel Research Institute;Ministry of Metallurgical Industry;Beijing |
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Cite this article:
MA Xiang Central Iron and Steel Research Institute;Ministry of Metallurgical Industry;Beijing. DETERMINATION OF σ-OR M_(23)C_6-PHASE IN STAINLESS STEEL BY STEP POTENTIAL ETCHING CURRENT METHOD. Acta Metall Sin, 1985, 21(4): 128-138.
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Abstract A new method,namely,the step potential etching current mehtod for theindividual determination of σ-or M_(23)C_6-phase which is a difficult problem to sepa-rate each other by conventional chemical manner has been developed.This simpli-fied and rapid method easy to give certain information about the composition,con-tent and morphology of precipitated phases in the steel has been applied to stain-less steel samples.In addition,a formula for quantitative analysis was derived onthe basis of a new model of electrode process.The formula has been confirmedby experiments.
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Received: 18 April 1985
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1 #12 2 #12 3 #12 4 #12 5 #12 6 #12 7 斋田义幸;筒井光范,日本金属学会志,42(1978) ,769. 8 马翔 徐澄宇;钢铁研究总院学报,4,(1984) ,№1,114. 9 马翔,分析化学,12(1984) ,№6,495. 10 马翔,分析化学,12(1984) ,№1,1. 11 黑泽文夫;田口勇;松本龙太郎,日本金属学会志,43(1979) ,1068. 12 Nicholson,R.S.;Shain,I.,Anal.Chem.,36(1964) ,706. |
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