研究论文

两种高代次镍基单晶高温合金热机械疲劳中的再结晶行为

  • 赵鹏 ,
  • 谢光 ,
  • 段慧超 ,
  • 张健 ,
  • 杜奎
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  • 1中国科学院金属研究所 沈阳材料国家研究中心 沈阳 110016
    2中国科学技术大学 材料科学与工程学院 沈阳 110016
    3中国科学院金属研究所 师昌绪先进材料创新中心 沈阳 110016
赵 鹏,男,1995年生,博士生

收稿日期: 2023-04-18

  修回日期: 2023-05-20

  网络出版日期: 2023-06-30

基金资助

国家自然科学基金项目(91960202);国家自然科学基金项目(52171020);国家自然科学基金项目(51901229);国家自然科学基金项目(51911530154);国家自然科学基金项目(91860201);国家自然科学基金项目(52271042);国家科技重大专项项目(P2022-C-IV-001-001)

Recrystallization During Thermo-Mechanical Fatigue of Two High-Generation Ni-Based Single Crystal Superalloys

  • ZHAO Peng ,
  • XIE Guang ,
  • DUAN Huichao ,
  • ZHANG Jian ,
  • DU Kui
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  • 1Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
    2School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
    3Shi -changxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China

Received date: 2023-04-18

  Revised date: 2023-05-20

  Online published: 2023-06-30

Supported by

National Natural Science Foundation of China(91960202);National Natural Science Foundation of China(52171020);National Natural Science Foundation of China(51901229);National Natural Science Foundation of China(51911530154);National Natural Science Foundation of China(91860201);National Natural Science Foundation of China(52271042);National Science and Technology Major Project(P2022-C-IV-001-001)

摘要

通过SEM和TEM等手段研究了经热机械疲劳变形后的第三代和第四代单晶高温合金的显微组织,了解高温合金在近服役条件下的变形组织,分析单晶高温合金近服役条件下的变形机制。结果表明,第三代和第四代单晶高温合金样品中在不同{111}面上产生了大量的变形孪晶,且在平行的孪晶片层中或者孪晶片层交截周围发现大量再结晶晶粒。再结晶晶粒的界面主要由变形后的孪晶界、小角度晶界以及孪晶相交产生的大角度晶界组成。借助像差校正透射电镜解析了变形后的孪晶界结构以及孪晶诱发动态再结晶的过程,揭示了单晶高温合金热机械疲劳断裂机制。

本文引用格式

赵鹏 , 谢光 , 段慧超 , 张健 , 杜奎 . 两种高代次镍基单晶高温合金热机械疲劳中的再结晶行为[J]. 金属学报, 2023 , 59(9) : 1221 -1229 . DOI: 10.11900/0412.1961.2023.00173

Abstract

Ni-based single crystal superalloys are widely used for turbine engine blades because of their excellent high-temperature mechanical properties. Thermo-mechanical fatigue (TMF) is a complex deformation process that combines strain and temperature effects. This process is also considered as a deformation method related to the working conditions of aviation turbine blades. Therefore, understanding the deformation mechanism of materials undergoing TMF is important for extending the service life of aviation turbine blades. Here, third-generation and fourth-generation single crystal superalloys that experienced TMF deformation are investigated by SEM and TEM, including aberration-corrected STEM. The results show the formation of deformation twins on different {111} planes of the single crystal superalloys. In addition, a large number of recrystallized grains are found in parallel twin lamellae or around the intersection of twin lamellae. The grain boundary of recrystallized grains is primarily composed of twin boundaries, low-angle grain boundaries, and large-angle grain boundaries generated by twin intersections. Furthermore, the twinning boundaries after deformation are analyzed using aberration-corrected TEM. Consequently, the process of twinning-induced dynamic recrystallization is comprehensively understood, which improved the TMF fracture mechanism of single crystal high-temperature alloys. These results improve the understanding of the deformation mechanism of single crystal superalloys under service conditions.

参考文献

1 Reed R C. The Superalloys: Fundamentals and Applications [M]. New York: Cambridge University Press, 2008: 1
2 Moverare J J, Johansson S, Reed R C. Deformation and damage mechanisms during thermal-mechanical fatigue of a single-crystal superalloy [J]. Acta Mater., 2009, 57: 2266
3 Marchionni M, Goldschmidt D, Maldini M. Evaluation of high-temperature behavior of CMSX4 + yttrium single-crystal nickel-base superalloy [J]. J. Mater. Eng. Perform., 1993, 2: 497
4 Zrnik J, Wang J A, Yu Y, et al. Influence of cycling frequency on cyclic creep characteristics of nickel base single-crystal superalloy [J]. Mater. Sci. Eng., 1997, A234-236: 884
5 MacLachlan D W, Knowles D M. Fatigue behaviour and lifing of two single crystal superalloys [J]. Fatigue Fract. Eng. Mater. Struct., 2001, 24: 503
6 Yu J J, Han G M, Chu Z K, et al. High temperature thermo-mechanical and low cycle fatigue behaviors of DD32 single crystal superalloy [J]. Mater. Sci. Eng., 2014, A592: 164
7 Fu B D, Zhang J X, Harada H. Interaction between crack and twins in TMS-82 superalloy during thermomechanical fatigue process [J]. Prog. Nat. Sci.: Mater. Int., 2013, 23: 508
8 Hong H U, Yoon J G, Choi B B, et al. Localized microtwin formation and failure during out-of-phase thermomechanical fatigue of a single crystal nickel-based superalloy [J]. Int. J. Fatigue, 2014, 69: 22
9 Kanesund J, Moverare J, Johansson S. The deformation and damage mechanisms during thermomechanical fatigue (TMF) in IN792 [J]. Procedia Eng., 2011, 10: 189
10 Kanesund J, Moverare J J, Johansson S. Deformation and damage mechanisms in IN792 during thermomechanical fatigue [J]. Mater. Sci. Eng., 2011, A528: 4658
11 Moverare J J, Segers?ll M, Sato A, et al. Thermomechanical fatigue of single-crystal superalloys: Influence of composition and microstructure [A]. Superalloys 2012 [C]. Hoboken: Wiley, 2012:369
12 Zhang J X, Harada H, Ro Y, et al. Thermomechanical fatigue mechanism in a modern single crystal nickel base superalloy TMS-82 [J]. Acta Mater., 2008, 56: 2975
13 Zhang J X, Harada H, Koizumi Y, et al. Crack appearance of single-crystal nickel-base superalloys after thermomechanical fatigue failure [J]. Scr. Mater., 2009, 61: 1105
14 Sun F, Zhang J X, Harada H. Deformation twinning and twinning-related fracture in nickel-base single-crystal superalloys during thermomechanical fatigue cycling [J]. Acta Mater., 2014, 67: 45
15 Zhang J X, Ro Y, Zhou H, et al. Deformation twins and failure due to thermo-mechanical cycling in TMS-75 superalloy [J]. Scr. Mater., 2006, 54: 655
16 Hong H U, Kang J G, Choi B G, et al. A comparative study on thermomechanical and low cycle fatigue failures of a single crystal nickel-based superalloy [J]. Int. J. Fatigue, 2011, 33: 1592
17 Wardle S, Phan I, Hug G. Analysis of twin intersections in TiAl [J]. Philos. Mag., 1993, 67A: 497
18 Zhang L C, Chen G L, Ye H Q. Substructures of deformation twins and twin intersections in a Ti-45Al-8Nb-2.5 Mn alloy heavily deformed at room temperature [J]. Mater. Sci. Eng., 2001, A299: 267
19 Yang G, Ma S Y, Du K, et al. Interactions between dislocations and twins in deformed titanium aluminide crystals [J]. J. Mater. Sci. Technol., 2019, 35: 402
20 Zhang L C, Chen G L, Wang J G, et al. Formation of a triangular striated structure in the twin intersection area in γ-TiAl during room-temperature deformation [J]. Intermetallics, 1999, 7: 1241
21 Ni S, Wang Y B, Liao X Z, et al. The effect of dislocation density on the interactions between dislocations and twin boundaries in nanocrystalline materials [J]. Acta Mater., 2012, 60: 3181
22 Zhu Y T, Wu X L, Liao X Z, et al. Dislocation-twin interactions in nanocrystalline fcc metals [J]. Acta Mater., 2011, 59: 812
23 Lv X Z, Zhang J X, Harada H. Twin-dislocation and twin-twin interactions during cyclic deformation of a nickel-base single crystal TMS-82 superalloy [J]. Int. J. Fatigue, 2014, 66: 246
24 Kontis P, Li Z M, Collins D M, et al. The effect of chromium and cobalt segregation at dislocations on nickel-based superalloys [J]. Scr. Mater., 2018, 145: 76
25 Wu X X, Makineni S K, Kontis P, et al. On the segregation of Re at dislocations in the γ' phase of Ni-based single crystal superalloys [J]. Materialia, 2018, 4: 109
26 Smith T M, Rao Y, Wang Y, et al. Diffusion processes during creep at intermediate temperatures in a Ni-based superalloy [J]. Acta Mater., 2017, 141: 261
27 Barba D, Pedrazzini S, Vilalta-clemente A, et al. On the composition of microtwins in a single crystal nickel-based superalloy [J]. Scr. Mater., 2017, 127: 37
28 Meid C, Eggeler M, Watermeyer P, et al. Stress-induced formation of TCP phases during high temperature low cycle fatigue loading of the single-crystal Ni-base superalloy ERBO/1 [J]. Acta Mater., 2019, 168: 343
29 He J Y, Zenk C H, Zhou X Y, et al. On the atomic solute diffusional mechanisms during compressive creep deformation of a Co-Al-W-Ta single crystal superalloy [J]. Acta Mater., 2020, 184: 86
30 Paul U, Sahm P R, Goldschmidt D. Inhomogeneities in single-crystal components [J]. Mater. Sci. Eng., 1993, A173: 49
31 Cox D C, Roebuck B, Rae C M F, et al. Recrystallisation of single crystal superalloy CMSX-4 [J]. Mater. Sci. Technol., 2003, 19: 440
32 Jo C Y, Cho H Y, Kim H M. Effect of recrystallisation on microstructural evolution and mechanical properties of single crystal nickel base superalloy CMSX-2 Part 1—Microstructural evolution during recrystallisation of single crystal [J]. Mat. Sci. Technol., 2003, 19: 1665
33 Yin D L, Zhang K F, Wang G F, et al. Warm deformation behavior of hot-rolled AZ31 Mg alloy [J]. Mater. Sci. Eng., 2005, A392: 320
34 Myshlyaev M M, McQueen H J, Mwembela A, et al. Twinning, dynamic recovery and recrystallization in hot worked Mg-Al-Zn alloy [J]. Mater. Sci. Eng., 2002, A337: 121
35 Chao H Y, Sun H F, Chen W Z, et al. Static recrystallization kinetics of a heavily cold drawn AZ31 magnesium alloy under annealing treatment [J]. Mater. Charact., 2011, 62: 312
36 Li Y P, Wu S, Bian H K, et al. Grain refinement due to complex twin formation in rapid hot forging of magnesium alloy [J]. Scr. Mater., 2013, 68: 171
37 Cao Y, Wang Y B, An X H, et al. Grain boundary formation by remnant dislocations from the de-twinning of thin nano-twins [J]. Scr. Mater., 2015, 100: 98
38 Zhao P, Xie G, Chen C J, et al. Interplay of chemistry and deformation-induced defects on facilitating topologically-close-packed phase precipitation in nickel-base superalloys [J]. Acta Mater., 2022, 236: 118109
39 Voronova L M, Degtyarev M V, Chashchukhina T I. Recrystallization of the ultradispersed structure of pure iron formed at different stages of the deformation-induced strain hardening [J]. Phys. Met. Metallogr., 2007, 104: 262
40 Zhang B, Lu X, Liu D L, et al. Influence of recrystallization on high-temperature stress rupture property and fracture behavior of single crystal superalloy [J]. Mater. Sci. Eng., 2012, A551: 149
41 Fang H C, Chao H, Chen K H. Effect of recrystallization on intergranular fracture and corrosion of Al-Zn-Mg-Cu-Zr alloy [J]. J. Alloys Compd., 2015, 622: 166
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