轧制态Mg-xZn-0.5Er合金板材组织及室温成形性能
收稿日期: 2021-12-13
修回日期: 2022-03-01
网络出版日期: 2022-08-18
基金资助
国家重点研发计划项目(2021YFB3701100);重庆市科研机构绩效激励引导专项项目(cstc2021jxjl50004);重庆市科研机构绩效激励引导专项项目(cstc2021jxjl50004)
Microstructures and Formability of the As-Rolled Mg- xZn-0.5Er Alloy Sheets at Room Temperature
Received date: 2021-12-13
Revised date: 2022-03-01
Online published: 2022-08-18
Supported by
National Key Research and Development Program of China(2021YFB3701100);Scientific Re-search Institution Performance Incentive and Guidance Special Project of Chongqing(cstc2021jxjl50004);Scientific Re-search Institution Performance Incentive and Guidance Special Project of Chongqing(cstc2021jxjl50004)
研究了Mg-xZn-0.5Er (x = 0.5、2.0、3.0、4.0,质量分数,%)合金板材在轧制过程中微观组织及织构的演变规律,并探讨了织构及第二相对合金室温成形性能的影响规律。结果表明,随着Zn含量的增加,合金提前发生了完全动态再结晶,在后续轧制过程中细小的动态再结晶晶粒长大并在应力的作用下被拉长,其显微组织由细小的等轴晶粒和粗大的变形晶粒组成,织构强度增大。当合金组织内仅存在细小弥散的第二相时,板材成形性能主要受板材基面织构影响;当合金组织内存在粗大第二相时,板材成形性能受板材基面织构和第二相共同影响,且当第二相含量较高时,第二相对成形性能的恶化作用会大于织构弱化所带来的积极作用。
关键词: Mg-Zn-Er合金; 动态再结晶; 织构; 第二相; 成形性能
娄峰 , 刘轲 , 刘金学 , 董含武 , 李淑波 , 杜文博 . 轧制态Mg-xZn-0.5Er合金板材组织及室温成形性能[J]. 金属学报, 2023 , 59(11) : 1439 -1447 . DOI: 10.11900/0412.1961.2021.00550
As lightweight requirements rise in transportation, aerospace, and other industries, magnesium alloys have a great application prospect. However, the low formability capabilities of magnesium alloys lead to a severe limit in applications. At present, there are many reports on the influences of texture and second phases on the formability of magnesium alloys at room temperature. Nevertheless, the dominant factors affecting the formability performance of magnesium alloys at room temperature are not clear. In this study, the development of the microstructures and texture of Mg-xZn-0.5Er (x = 0.5, 2.0, 3.0, 4.0, mass fraction, %) alloy sheets were studied, and the impact of the texture and second phases on the formability of these sheets were also investigated. The findings showed that the increase in Zn addition led to an early and complete dynamic recrystallization (DRX) in Mg-Zn-Er alloys sheets, and these recrystallized grains would expand significantly during subsequent hot rolling processes. These recrystallized grains with a large size were typically elongated and then helped to create a strong basal texture. Thus, it was discovered that the microstructures of these sheets were typically made up of equiaxed and elongated grains. The formability performance of these sheets was strongly related to the size of the second phases and the texture. The formability of the sheets containing microscopic second phases mainly depended on the basal texture, while the formability of the sheets which contained coarse second phases was mostly influenced by the second phases and basal texture. Particularly, when the component of the coarse second was larger, the formability would get more inferior due to the predominant role of the second phase at room temperature.
Key words: Mg-Zn-Er alloy; dynamic recrystallization; texture; second phase; formability
| 1 | You S H, Huang Y D, Kainer K U, et al. Recent research and developments on wrought magnesium alloys [J]. J. Magn. Alloy., 2017, 5: 239 |
| 2 | Liu X W, Liu Y, Jin B, et al. Microstructure evolution and mechanical properties of a SMATed Mg alloy under in situ SEM tensile testing [J]. J. Mater. Sci. Technol., 2017, 33: 224 |
| 3 | Zhang J, Joshi S P. Phenomenological crystal plasticity modeling and detailed micromechanical investigations of pure magnesium [J]. J. Mech. Phys. Solids, 2012, 60: 945 |
| 4 | Sabat R K, Brahme A P, Mishra R K, et al. Ductility enhancement in Mg-0.2%Ce alloys [J]. Acta Mater., 2018, 161: 246 |
| 5 | Ding W J, Jin L, Wu W X, et al. Texture and texture optimization of wrought Mg alloy [J]. Chin. J. Nonferrous Met., 2011, 21: 2371 |
| 丁文江, 靳 丽, 吴文祥 等. 变形镁合金中的织构及其优化设计 [J]. 中国有色金属学报, 2011, 21: 2371 | |
| 6 | Huang X S, Suzuki K, Chino Y, et al. Influence of aluminum content on the texture and sheet formability of AM series magnesium alloys [J]. Mater. Sci. Eng., 2015, A633: 144 |
| 7 | Nakata T, Xu C, Ohashi H, et al. New Mg-Al based alloy sheet with good room-temperature stretch formability and tensile properties [J]. Scr. Mater., 2020, 180: 16 |
| 8 | Wang Q H, Shen Y Q, Jiang B, et al. A good balance between ductility and stretch formability of dilute Mg-Sn-Y sheet at room temperature [J]. Mater. Sci. Eng., 2018, A736: 404 |
| 9 | Bian M Z, Huang X S, Mabuchi M, et al. Compositional optimization of Mg-Zn-Sc sheet alloys for enhanced room temperature stretch formability [J]. J. Alloys Compd., 2020, 818: 152891 |
| 10 | Luo Z P, Zhang S Q, Tang Y L, et al. Thermodynamics of Mg-Zn-RE system solutions forming stable quasicrystals [J]. Scr. Metall. Mater., 1994, 30: 393 |
| 11 | Xu D K, Tang W N, Liu L, et al. Effect of W-phase on the mechanical properties of as-cast Mg-Zn-Y-Zr alloys [J]. J. Alloys Compd., 2008, 461: 248 |
| 12 | Kawamura Y, Hayashi K, Inoue A, et al. Rapidly solidified powder metallurgy Mg97Zn1Y2 alloys with excellent tensile yield strength above 600 MPa [J]. Mater. Trans., 2001, 42: 1172 |
| 13 | Al-Samman T. Modification of texture and microstructure of magnesium alloy extrusions by particle-stimulated recrystallization [J]. Mater. Sci. Eng., 2013, A560: 561 |
| 14 | Wang Q F, Du W B, Liu K, et al. Microstructure, texture and mechanical properties of as-extruded Mg-Zn-Er alloys [J]. Mater. Sci. Eng., 2013, A581: 31 |
| 15 | Meng Y Z, Yu J M, Liu K, et al. The evolution of long-period stacking ordered phase and its effect on dynamic recrystallization in Mg-Gd-Y-Zn-Zr alloy processed by repetitive upsetting-extrusion [J]. J. Alloys Compd., 2020, 828: 154454. |
| 16 | Humphreys F J. Recrystallization mechanisms in two-phase alloys [J]. Met. Sci., 1979, 13: 136 |
| 17 | Lou F, Liu K, Lui J X, et al. Microstructure and formability at room temperature of as-annealing Mg-xZn-0.5Er alloy sheets [J]. Chin. J. Nonferrous Met., 2022, 32: 365 |
| 娄 峰, 刘 轲, 刘金学 等. 退火态Mg-xZn-0.5Er合金板材组织及室温成形性能 [J]. 中国有色金属学报, 2022, 32: 365 | |
| 18 | Kaibyshev R. Dynamic recrystallization in magnesium alloys [A]. Advances in Wrought Magnesium Alloys [M]. Cambridge, UK: Woodhead Publishing, 2012: 186 |
| 19 | Fatemi-Varzaneh S M, Zarei-Hanzaki A, Beladi H. Dynamic recrystallization in AZ31 magnesium alloy [J]. Mater. Sci. Eng., 2007, A456: 52 |
| 20 | Al-Samman T, Gottstein G. Dynamic recrystallization during high temperature deformation of magnesium [J]. Mater. Sci. Eng., 2008, A490: 411 |
| 21 | Vaughan M W, Nasim W, Dogan E, et al. Interplay between the effects of deformation mechanisms and dynamic recrystallization on the failure of Mg-3Al-1Zn [J]. Acta Mater., 2019, 168: 448 |
| 22 | Chino Y, Huang X S, Suzuki K, et al. Influence of Zn concentration on stretch formability at room temperature of Mg-Zn-Ce alloy [J]. Mater. Sci. Eng., 2010, A528: 566 |
| 23 | Liu K, Lou F, Fu J J, et al. Microstructure and corrosion behaviors of as-rolled Mg-Zn-Er alloy sheets [J]. Trans. Nonferrous Met. Soc. China, 2022, 32: 1881 |
| 24 | Liu K, Sun C C, Wang Z H, et al. Microstructure, texture and mechanical properties of Mg-Zn-Er alloys containing I-phase and W-phase simultaneously [J]. J. Alloys Compd., 2016, 665: 76 |
| 25 | Qin D H, Wang M J, Sun C Y, et al. Interaction between texture evolution and dynamic recrystallization of extruded AZ80 magnesium alloy during hot deformation [J]. Mater. Sci. Eng., 2020, A788: 139537 |
| 26 | Suh B C, Kim J H, Hwang J H, et al. Twinning-mediated formability in Mg alloys [J]. Sci. Rep., 2016, 6: 22364 |
| 27 | Robson J D, Henry D T, Davis B. Particle effects on recrystallization in magnesium-manganese alloys: Particle-stimulated nucleation [J]. Acta Mater., 2009, 57: 2739 |
| 28 | Robson J D, Henry D T, Davis B. Particle effects on recrystallization in magnesium-manganese alloys: Particle pinning [J]. Mater. Sci. Eng., 2011, A528: 4239 |
| 29 | Liu P, Jiang H T, Duan X G, et al. Effects of yttrium (Y) and cerium (Ce) on microstructure and stretch formability of hot rolled Mg-1.5Zn magnesium sheet at room temperature [J]. J. Mater Eng., 2014, (12): 1 |
| 刘 鹏, 江海涛, 段晓鸽 等. 稀土元素Y和Ce对热轧Mg-1.5Zn镁合金组织和室温成形性能的影响 [J]. 材料工程, 2014, (12): 1 | |
| 30 | Cai Z X, Tang D, Jiang H T, et al. Influence of Gd concentration on texture and stretch formability of rolled Mg-Zn-Gd alloys at room temperature [J]. Rare Met. Mater. Eng., 2013, 42: 2073 |
| 蔡正旭, 唐 荻, 江海涛 等. 不同Gd含量对变形Mg-Zn-Gd合金织构和室温成形性能的影响 [J]. 稀有金属材料与工程, 2013, 42: 2073 |
/
| 〈 |
|
〉 |