研究论文

高强管线钢焊接临界再热粗晶区中逆转奥氏体的逆相变晶体学

  • 李学达 ,
  • 李春雨 ,
  • 曹宁 ,
  • 林学强 ,
  • 孙建波
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  • 中国石油大学(华东) 材料科学与工程学院 青岛 266580
李学达,男,1985年生,副教授,博士

收稿日期: 2020-07-31

  修回日期: 2020-09-24

  网络出版日期: 2021-03-03

基金资助

国家自然科学基金项目(51801233)

Crystallography of Reverted Austenite in the Intercritically Reheated Coarse-Grained Heat-Affected Zone of High Strength Pipeline Steel

  • Xueda LI ,
  • Chunyu LI ,
  • Ning CAO ,
  • Xueqiang LIN ,
  • Jianbo SUN
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  • School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao 266580, China
LI Xueda, associate professor, Tel: 15621003950, E-mail: lixuedachina@163.com

Received date: 2020-07-31

  Revised date: 2020-09-24

  Online published: 2021-03-03

Supported by

National Natural Science Foundation of China(51801233)

摘要

利用Gleeble热模拟以及电子背散射衍射(EBSD)技术,研究了高强管线钢焊接临界再热粗晶区(ICCGHAZ)中逆转奥氏体(γr)在不同第二道次峰值温度(760、800和840℃)下的逆相变规律及其晶体学关系。结果表明,在3个峰值温度下形成的γr体积分数依次为4.1%、8.9%和25.2%,γr优先在第一道次粗晶区的原奥氏体晶界(PAGB)处形核,其次是原奥氏体晶粒(γp)内板条束(block)的交界处。在极快的焊接加热速率下,γr倾向于以块状形式长大。晶体学研究表明,γr在PAGB处的逆相变不是自由形核,而是依托于PAGB一侧γp的晶体学取向按照近似K-S关系通过逆相变而形成,而与另一侧的γp没有确定的晶体学关系。第二道次峰值温度较低(760℃)时,γr在PAGB处形核后向非K-S关系一侧的晶粒内部长大,γr呈链状分布于PAGB处。随峰值温度的升高(800和840℃),γr向PAGB两侧同时生长。分析表明,γr在第二道次加热过程中的逆相变行为对其在后续冷却过程中的相变过程、终态组织及其韧性等有重要影响。

本文引用格式

李学达 , 李春雨 , 曹宁 , 林学强 , 孙建波 . 高强管线钢焊接临界再热粗晶区中逆转奥氏体的逆相变晶体学[J]. 金属学报, 2021 , 57(8) : 967 -976 . DOI: 10.11900/0412.1961.2020.00287

Abstract

Low carbon microalloyed high-strength pipeline steels processed by the thermomechanical controlled process have a good strength-toughness combination. However, after welding, the microstructure and mechanical properties of the heat-affected zone (HAZ) become deteriorated. Previous studies show that martensite-austenite (M-A) constituent formed in the HAZ is a key factor that lowers the toughness, especially necklace-type M-A constituent formed in the intercritically reheated coarse-grained HAZ (ICCGHAZ). However, the phase transformation mechanism of necklace-type M-A constituent in the ICCGHAZ is unclear. In this study, the crystallography of reverted austenite (γr) during the reversion phase transformation upon heating the ICCGHAZ of a high-strength pipeline steel was studied using Gleeble thermal simulation and electron backscatter diffraction (EBSD) technique. Two thermal cycles with peak temperatures of 1300oC and 760oC/800oC/840oC were conducted to simulate the phase transformation process in the ICCGHAZ. The samples were directly quenched to room temperature after been reheated to the second peak temperature, and the reversion behavior, distribution, and crystallography of γr were studied. The results showed that the volume fraction of γr formed at 760, 800, and 840oC was 4.1%, 8.9%, and 25.2%, respectively. γr preferred to nucleate along prior austenite grain boundaries (PAGB), and posterior the block boundaries within the prior austenite grains. γr preferred to grow to blocky type along the PAGB, and the acicular type γr between bainite laths was suppressed. The crystallographic study showed that the formation of γr at PAGB was not free nucleation. However, γr was formed based on the crystallographic orientation of PAGB alongside prior austenite grain complying with Kurdjuov-Sachs (K-S) relationship, while having non K-S relationship with the prior austenite grain on the other side. After nucleation at PAGB, and at a low second peak temperature (760oC), γr transformed to prior austenite grain with non K-S relationship, and the γr formed in blocky and necklace-type along the PAGB. With an increase in the second peak temperature (800-840oC), γr transformed to the prior austenite grains on both sides. The analysis showed that the reversion behavior and crystallography of γr during the second pass reheating have a big impact on the phase transformation upon cooling and the corresponding microstructure and mechanical properties.

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