提出了一种简单的高熵合金加工工艺，即对Fe-Mn系高熵合金采用中等形变量冷轧和中温短时退火相结合的方法，获得了由晶粒尺寸为数十微米的形变晶粒和超细尺度再结晶晶粒组成的非均匀结构。通过向合金中同时引入由高密度位错、晶粒细化、析出相、ε-马氏体、α-马氏体和回复孪晶等微观结构特征及变形过程中持续发生的形变孪生、ε-马氏体相变引起的多种强化机制，使屈服强度较充分再结晶态显著提升并达到825 MPa。同时，在塑性变形过程中由于发生了显著的形变孪生和一定的由形变诱发的奥氏体向ε-马氏体转变，合金仍具有约28.6%的均匀延伸率，合金的综合力学性能得到有效提升。该工艺为优化以fcc结构为主的低层错能合金的力学性能提供了新思路。

Growing attention has been placed on high-entropy alloys (HEAs) owing to their promising mechanical properties. Particularly, HEAs in which the main crystal structure is fcc are attracting significant attention. Although such alloys exhibit a good combination of strength and ductility, they cannot meet the increasing demands of applications because of limited yield strengths. In recent years, researchers have tried to improve yield strengths of HEAs by refining grains and introducing interstitial atoms. However, the processing cost is high and is often accompanied by the significant loss of ductility. In this study, we propose a simple processing route incorporating cold rolling at medium thickness reductions and short-time annealing at medium temperatures to obtain a heterogeneous structure in Fe-Mn based HEAs consisting of deformed grains with an average diameter of several tens of microns and recrystallized ultrafine grains. By simultaneously introducing multiple strengthening mechanisms, including the strengthening contributed by the microstructural characteristics of dense dislocations, grain refinement, precipitates, ε-martensite, α-martensite, and recovery twins, as well as the strengthening induced by deformation twinning and ε-martensite phase transition that occurs continuously during deformation, the yield strength of the alloy significantly increases compared with that of the fully recrystallized material and reaches 825 MPa. Simultaneously, due to the activation of significant deformation twinning and deformation-induced martensitic transformation, the uniform elongation of the alloy is about 28.6%. The proposed material fabrication method is simple, cost-effective, and can effectively improve the mechanical properties of Fe-Mn based HEAs, providing new insight into optimizing the mechanical properties of low stacking fault energy alloys of the fcc structure.