氙离子辐照后Hastelloy N合金的纳米硬度及其数值模拟

  • 刘继召 ,
  • 黄鹤飞 ,
  • 朱振博 ,
  • 刘阿文 ,
  • 李燕
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  • 1.中国科学院上海应用物理研究所 上海 201800
    2.中国科学院大学核科学与技术学院 北京 100049
    3.上海科技大学物质科学与技术学院 上海 201210
刘继召,男,1991年生,博士生

收稿日期: 2019-09-26

  修回日期: 2019-12-11

  网络出版日期: 2019-12-23

基金资助

国家自然科学基金项目(11605271);国家自然科学基金项目(11975304);国家自然科学基金项目(91126012)

Numerical Simulation of Nanohardness in Hastelloy N Alloy After Xenon Ion Irradiation

  • Jizhao LIU ,
  • Hefei HUANG ,
  • Zhenbo ZHU ,
  • Awen LIU ,
  • Yan LI
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  • 1.Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai 201800, China
    2.School of Nuclear Science and Technology, University of Chinese Academy of Sciences, Beijing 100049, China
    3.School of Physical Science and Technology, ShanghaiTech University, Shanghai 201210, China

Received date: 2019-09-26

  Revised date: 2019-12-11

  Online published: 2019-12-23

Supported by

National Natural Science Foundation of China(11605271);National Natural Science Foundation of China(11975304);National Natural Science Foundation of China(91126012)

摘要

利用纳米压痕仪的连续刚度测量模式测试了常温氙离子辐照后Hastelloy N合金的纳米硬度。结果表明,辐照样品的纳米硬度均大于未辐照样品的纳米硬度,且辐照剂量在0.5~3.0 dpa这一范围内时,辐照样品的纳米硬度处于饱和状态。在Nix-Gao模型的基础上,分离出未辐照样品和辐照样品的压痕尺寸效应,并通过VLM (volume law of mixture)模型来模拟实验测得的纳米硬度。由于随着压头压入深度的增加,塑性影响区中将同时包含辐照损伤层与基体,在VLM模型中引入“界面参数”(χ)以修正基体的形变量,改进后的模型能够更好地模拟纳米压痕的实验结果。

本文引用格式

刘继召 , 黄鹤飞 , 朱振博 , 刘阿文 , 李燕 . 氙离子辐照后Hastelloy N合金的纳米硬度及其数值模拟[J]. 金属学报, 2020 , 56(5) : 753 -759 . DOI: 10.11900/0412.1961.2019.00324

Abstract

Ion irradiation experiments are of importance for investigating irradiation damage of reactor structural materials. However, estimating the irradiation hardening of ion-irradiated materials is difficult due to the limitation of ion penetration depth. In recent years, nanoindentation test has been widely used to study the irradiation hardening of materials, because the continuous stiffness measurement (CSM) mode can obtain the relationship between nanohardness and indentation depth at a very small penetration depth. In this work, the average nanohardness of Hastelloy N alloy irradiated by xenon ion at room temperature was tested by this mode. The results showed that the nanohardness in the irradiated samples was larger than that in the unirradiated sample and this value of irradiated samples is saturated when the irradiation dose is in the range of 0.5~3.0 dpa. Based on the Nix-Gao model, the indentation size effects (ISE) of unirradiated and irradiated samples were separated from nanohardness measured by nanoindentation. The volume law of mixture model (VLM) was subsequently applied to simulate the measured nanohardness. As the depth of indentation increases, the plasticity affected region (PAR) includes both irradiation damage layer and matrix. Interface parameter was introduced to correct the volume of matrix deformation. The results indicated that the improved VLM model leads to a characteristic relation for the depth dependence of nanohardness that is in excellent agreement with nanoindentation experiments.

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