研究论文

γ/ε双相Fe-19Mn合金在拉伸变形过程中的组织演变和加工硬化行为

  • 王世宏 ,
  • 李健 ,
  • 葛昕 ,
  • 柴锋 ,
  • 罗小兵 ,
  • 杨才福 ,
  • 苏航
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  • 1. 钢铁研究总院工程用钢研究所 北京 100081
    2. 安徽工业大学材料科学与工程学院 马鞍山 243002
王世宏,男,1991年生,博士生

收稿日期: 2019-06-03

  修回日期: 2019-07-05

  网络出版日期: 2019-09-27

基金资助

国家海军装备预研项目(302030122-0183-001)

Microstructural Evolution and Work Hardening Behavior of Fe-19Mn Alloy Containing Duplex Austenite and ε-Martensite

  • Shihong WANG ,
  • Jian LI ,
  • Xin GE ,
  • Feng CHAI ,
  • Xiaobing LUO ,
  • Caifu YANG ,
  • Hang SU
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  • 1. Department of Structure Steels, Central Iron and Steel Research Institute, Beijing 100081, China
    2. School of Materials Science and Engineering, Anhui University of Technology, Maanshan 243002, China

Received date: 2019-06-03

  Revised date: 2019-07-05

  Online published: 2019-09-27

Supported by

Naval Equipment Pre-research Foundation of China(302030122-0183-001)

摘要

采用OM、EBSD、TEM、XRD和拉伸实验等方法,研究了γ-奥氏体/ε-马氏体双相Fe-19Mn-0.0017C (质量分数,%)合金在拉伸变形过程中的组织演变和加工硬化行为。结果表明,Fe-19Mn发生了变形诱导马氏体相变,并且随着变形量的增加,相变过程由以γε相变为主转变为以εα'相变为主。对比分析加工硬化率的变化与相含量的变化,表明εα'相变比γε相变具有更高的加工硬化能力。同时,在变形过程中,ε-马氏体不仅发生了位错滑移,还形成了{101?2}<1?011>ε孪晶,以满足ε-马氏体的变形协调。在γεεα'双重相变引起的相变诱导塑性(TRIP)效应、γ-奥氏体/ε-马氏体/α'-马氏体中的位错滑移,以及ε-马氏体的孪生变形等机制的共同作用下,Fe-19Mn的抗拉强度和总延伸率分别达到722 MPa和31%,显示出良好的强塑性匹配。

本文引用格式

王世宏 , 李健 , 葛昕 , 柴锋 , 罗小兵 , 杨才福 , 苏航 . γ/ε双相Fe-19Mn合金在拉伸变形过程中的组织演变和加工硬化行为[J]. 金属学报, 2020 , 56(3) : 311 -320 . DOI: 10.11900/0412.1961.2019.00181

Abstract

As the excellent combination of strength and ductility, the high manganese steel has been used in the manufacturing field of automobile, liquefied natural gas (LNG) ship and oil and gas exploitation. On the other hand, due to the good damping capacity within a certain Mn content range, it has also been used to make components on the machines to reduce vibration and noise. So high manganese steel is considered to be a structural and functional integrated material with great application prospects. Many factors can affect the mechanical properties and damping capacity, such as chemical composition, grain size and heat treatments. Among these, carbon concentration has a complicated influence on them. For example, a high carbon concentration will improve mechanical properties, but in return deteriorate damping capacity. In order to acquire a material with good damping capacity and suitable strength and ductility, ultralow carbon Fe-19Mn-0.0017C (mass fraction, %) alloy was designed. The microstructural evolution and mechanical properties of the alloy during tensile process were investigated by means of OM, EBSD, TEM, XRD and tension test. The results show that Fe-19Mn shows deformation-induced martensite transformation, which changes from γ-austenite→ε-martensite transformation to ε-martensite→α'-martensite transformation as the amount of deformation increases. Analysis of the strain hardening rate (ln(dσtrue/dεtrue)) combined with the fraction of constituent phases reveals that the transformation of ε-martensite→α'-martensite is more effective in improving work hardening rate than that of γ-austenite→ε-martensite. This is, on one hand, because of the lower strength of ε-martensite which is caused by the lack of carbon solution strengthening; and on the other hand, α'-martensite has higher hardness than ε-martensite, which can impede dislocation movement more effectively. In addition, {101?2}<1?011>ε deformation twins are formed to accommodate deformation of ε-martensite except for dislocation slip during tensile process. The combined action of transformation induced plasticity (TRIP) effects of γ-austenite→ε-martensite→α'-martensite transformation, dislocation slip of γ-austenite/ε-martensite/α'-martensite and {101?2}<1?011>ε deformation twinning makes Fe-19Mn with ultralow carbon concentration have an excellent combination of strength and ductility, whose tensile strength and total elongation can reach 722 MPa and 31%, respectively.

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