采用Gleeble-1500热模拟机对GH738镍基高温合金进行了高温热压缩变形实验, 分析了该合金在初始晶粒不同的情况下, 变形温度1000-1160 ℃,应变速率0.01-10 s-1, 工程变形量15%-70%条件下流变应力的变化规律及晶粒组织演化规律; 同时研究了变形温度1040-1120 ℃,应变速率0.1-10 s-1, 变形量15%-50%, 保温时间0-45 s条件下该合金的亚动态(静态)再结晶及保温温度980-1140 ℃, 保温时间0-4 h条件下的晶粒长大行为. 通过系统的物理热模拟实验, 构建了GH738高温合金在热变形过程中的晶粒组织演化模型及应力-应变模型, 所建立的GH738高温合金模型与实验结果相比均表现出较高的相关度.
The hot deformation behavior of GH738 superalloy with different initial grain sizes was studied using hot compression experiments via Gleeble–1500. Correlations between flow stress, process parameters and microstructure evolution were characterized in the temperature range of 1000—1160 ℃, strain rate range of 0.01—10 s−1 and engineering strain range of 15%—70%. Besides, metadynamic recrystallization and static recrystallization were studied in the temperature range of 1040—1120 ℃, strain rate range of 0.1—10 s−1 and engineering strain range of 15%—50% with soaking time for 0—45 s; grain growth behavior was researched in the temperature range 980—1140 with soaking time for 0—4 h. The results show that recrystallization behavior of GH738 superalloy was significantly affected by initial grain size, deformation temperature, strain and strain rate. Thermomechanical behavior and microstructural evolution models were systematically constructed based on the investigation of dynamic recrystallization, meta–dynamic recrystallization, static recrystallization and grain growth. The analyses indicate that these models shows a high correlation with actual results of GH738 superalloy.
[1] Yao Z H, Dong J X, Zhang M C, Zheng L. Rare Met Mater Eng, 2010; 39: 1565
(姚志浩, 董建新, 张麦仓, 郑磊. 稀有金属材料与工程, 2010; 39: 1565)
[2] Chang K M, Liu X B. Mater Sci Eng, 2001; A308: 1
[3] Semiatin S L, Fagin P N, Glavicic M G. Scr Mater, 2004; 50: 625
[4] Liu X B, Kang B, Chang K M. Mater Sci Eng, 2003; A340: 8
[5] Yao Z H, Dong J X, Zhang M C, Yu Q Y, Zheng L. Trans Mater Heat Treat, 2011; 32: 44
(姚志浩, 董建新, 张麦仓, 于秋颖, 郑磊. 材料热处理学报, 2011; 32: 44)
[6] Donachie M J, Pinkowish A A, Danesi W P, Radavich J F, Couts W H. Metall Trans, 1970; 1: 2623
[7] Guimaraes A A, Jonas J J. Metall Trans, 1981; A12: 1655
[8] Livesey D W, Sellars C M. Mater Sci Technol, 1985; 1: 136
[9] Li M Q, Yao X Y, Luo J, Lin Y Y, Su S B, Wang H R. Acta Metall Sin, 2007; 43: 937
(李淼泉, 姚晓燕, 罗皎, 林莺莺, 苏少博, 王海荣. 金属学报, 2007; 43: 937)
[10] Salehi A R, Serajzadeh S, Yazdipour N.Mater Chem Phys, 2007; 101: 153
[11] Gao H, Barber G C, Chen Q A, Lu Y Q. J Mater Process Technol, 2003; 142: 52
[12] Ganapathysubramanian S, Zabaras N. Int J Solid Struct, 2004; 41: 2011
[13] Wang B X, Liu X H, Wang G D. Mater Sci Eng, 2005; A393: 102
[14] Sui F L, Xu L X, Chen L Q, Liu X H. J Mater Process Technol, 2011; 211: 433
[15] Zhao M L, Sun W R, Yang S L, Qi F, Guo S R, Hu Z Q. Acta Metall Sin, 2009; 45: 79
(赵美兰, 孙文儒, 杨树林, 祁峰, 郭守仁, 胡壮麒. 金属学报, 2009; 45: 79)
[16] Sellars C M, McTegart W J. Acta Metall, 1966; 14: 1136
[17] McQueen H J, Ryan N D. Mater Sci Eng, 2002; A322: 43
[18] Sommitsch C, Mitter W. Acta Metall, 2006; 54: 357
[19] Gottstein G, Frommert M, Goerdeler M, Schafer N. Mater Sci Eng, 2004; A387–389: 604
[20] Solhjoo S. Mater Des, 2010; 31: 1360
[21] Poliak E I, Jonas J J. ISIJ Int, 2003; 43: 692
[22] Li G, Maccagno T M, Bai D Q. ISIJ Int, 1996; 36: 1479
[23] Bai D Q, Yue S, Jonas J J. ISIJ Int, 1996; 36: 1084
[24] Shen B Z, Fang N W, Shen H F, Liu B C. Mater Sci Technol, 2005; 13: 516
(沈丙振, 方能炜, 沈厚发, 柳百成. 材料科学与工艺, 2005; 13: 516)
[25] Li G, Maccagno T M, Bai D Q. ISIJ Int, 1996; 36: 1479
[26] Sellars C M, Whiteman J A. Met Sci, 1979; 13: 187
[27] Anelli E. ISIJ Int, 1992; 32: 440