Research paper

In Situ Analysis of Plastic Deformation of Lath Martensite During Tensile Process

  • Zengmin SHI ,
  • Jingyu LIANG ,
  • Jian LI ,
  • Maoqiu WANG ,
  • Zifan FANG
Expand
  • 1.Hubei Key Laboratory of Hydroelectric Machinery Design & Maintenance, China Three Gorges University, Yichang 443002, China
    2.School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan 430074, China
    3.Special Steel Institute, Central Iron and Steel Research Institute, Beijing 100081, China
LI Jian, professor, Tel: 15071161133, E-mail: lijian@hust.edu.cn
SHI Zengmin, professor, Tel: 18872517438, E-mail: shzm@ctgu.edu.cn

Received date: 2020-07-22

  Revised date: 2020-10-27

  Online published: 2020-11-16

Supported by

National Basic Research Program of China(2010CB630802);National Natural Science Foundation of China(51201093);Hubei Technology Innovation Project(2017AAA113)

Abstract

Lath martensitic steels are widely used in high strength structural materials. Coherency strains in quenched lath martensite induce huge dislocation densities, which are the sources of the alloys' strength, whereas the way its microstructure functions is still unclear. The plastic deformation behavior of lath martensite in ultrahigh strength steel was investigated using in situ neutron diffraction technology. Diffraction data were analyzed using the Z-Rietveld and convolutional multiple whole profile (CMWP) fitting procedures. Transformation dislocations in the as-quenched martensite were mixed with edge and screw components and showed characteristics of random distribution. Significant work hardening of lath martensite can be better understood by considering the increase in dislocation density along with changes in dislocation arrangement. With increased tensile strain, the total dislocation density increased with the increasing amount of edge-type components and the decreasing amount of screw-type components. The hard orientation packets showed characteristics of work hardening with an increased dislocation density, whereas the soft orientation packets showed characteristics of work softening with a decreased dislocation density. The partitioning of the applied load was carried out within two types of packets, which further promoted the formation of long-range internal stresses after deformation.

Cite this article

Zengmin SHI , Jingyu LIANG , Jian LI , Maoqiu WANG , Zifan FANG . In Situ Analysis of Plastic Deformation of Lath Martensite During Tensile Process[J]. Acta Metall Sin, 2021 , 57(5) : 595 -604 . DOI: 10.11900/0412.1961.2020.00275

References

1 Morito S, Nishikawa J, Maki T. Dislocation density within lath martensite in Fe-C and Fe-Ni alloys [J]. ISIJ Int., 2003, 43: 1475
2 Shi Z M, Gong W, Tomota Y, et al. Study of tempering behavior of lath martensite using in situ neutron diffraction [J]. Mater. Charact., 2015, 107: 29
3 Krauss G. Martensite in steel: Strength and structure [J]. Mater. Sci. Eng., 1999, A273-275: 40
4 Morito S, Tanaka H, Konishi R, et al. The morphology and crystallography of lath martensite in Fe-C alloys [J]. Acta Mater., 2003, 51: 1789
5 Morito S, Huang X, Furuhara T, et al. The morphology and crystallography of lath martensite in alloy steels [J]. Acta Mater., 2006, 54: 5323
6 Krauss G. Steels: Heat Treatment and Processing Principles [M]. 2nd Ed., Materials Park, OH: ASM International, 1990: 149
7 Wang C F, Wang M Q, Shi J, et al. Effect of microstructural refinement on the toughness of low carbon martensitic steel [J]. Scr. Mater., 2008, 58: 492
8 Morito S, Yoshida H, Maki T, et al. Effect of block size on the strength of lath martensite in low carbon steels [J]. Mater. Sci. Eng., 2006, A438-440: 237
9 Shi Z M, Liu K, Wang M Q, et al. Effect of tensile deformation of austenite on the morphology and strength of lath martensite [J]. Met. Mater. Int., 2012, 18: 317
10 Wang C F, Wang M Q, Dong H. In-situ observation of deformation and fracture process for lath martensite steel [J]. J. Iron Steel Res., 2012, 24(3): 38
10 王春芳, 王毛球, 董 瀚. 板条马氏体钢变形与断裂过程的原位观察 [J]. 钢铁研究学报, 2012, 24(3): 38
11 Chen P, Wang G D, Ceguerra A V, et al. Yield strength enhancement by carbon trapping in ferrite of the quenching and partitioning steel [J]. Metall. Mater. Trans., 2018, 49A: 235
12 Morooka S, Tomota Y, Kamiyama T. Heterogeneous deformation behavior studied by in situ neutron diffraction during tensile deformation for ferrite, martensite and pearlite steels [J]. ISIJ Int., 2008, 48: 525
13 Wang Y, Zhang K, Guo Z H, et al. A new effect of retained austenite on ductility enhancement of low carbon Q-P-T steel [J]. Acta Metall. Sin., 2012, 48: 641
13 王 颖, 张 柯, 郭正洪等. 残余奥氏体增强低碳Q-P-T钢塑性的新效应 [J]. 金属学报, 2012, 48: 641
14 Zhang K, Liu P, Li W, et al. High strength-ductility Nb-microalloyed low martensitic carbon steel: Novel process and mechanism [J]. Acta Metall. Sin. (Engl. Lett.), 2015, 28: 1264
15 Tomota Y, Luká? P, Neov D, et al. In situ neutron diffraction during tensile deformation of a ferrite-cementite steel [J]. Acta Mater., 2003, 51: 805
16 Tomota Y, Xu P G, Oliver E C, et al. In situ neutron diffraction during thermo-mechanically controlled process for low alloy steels [A]. In-Situ Studies with Photons, Neutrons and Electrons Scattering [M]. Berlin: Springer-Verlag, 2010: 17
17 Xu P G, Tomota Y, Luká? P, et al. Austenite-to-ferrite transformation in low alloy steels during thermomechanically controlled process studied by in situ neutron diffraction [J]. Mater. Sci. Eng., 2006, A435-436: 46
18 Tomota Y, Wang Y X, Ohmura T, et al. In situ neutron diffraction study on ferrite and pearlite transformations for a 1.5Mn-1.5Si-0.2C steel [J]. ISIJ Int., 2018, 58: 2125
19 Aranas Jr C, Rodrigue S, Siciliano F, et al. In-situ X-ray diffraction evidence of dynamic transformation of austenite to ferrite during hot compression test in the single austenite phase field [J]. Scr. Mater., 2020, 177: 86
20 Ungár T, Gubicza J, Ribárik G, et al. Crystallite size distribution and dislocation structure determined by diffraction profile analysis: Principles and practical application to cubic and hexagonal crystals [J]. J. Appl. Cryst., 2001, 34: 298
21 Ribárik G, Gubicza J, Ungár T. Correlation between strength and microstructure of ball-milled Al-Mg alloys determined by X-ray diffraction [J]. Mater. Sci. Eng., 2004, A387-389: 343
22 Ungár T, Dragomir I, Révész á, et al. The contrast factors of dislocations in cubic crystals: The dislocation model of strain anisotropy in practice [J]. J. Appl. Cryst., 1999, 32: 992
23 Wilkens M. The determination of density and distribution of dislocations in deformed single crystals from broadened X-Ray diffraction profiles [J]. Phys. Stat. Sol., 1970, 2A: 359
24 Iakoubovskii K, Mitsuishi K, Furuya K. High-resolution electron microscopy of detonation nanodiamond [J]. Nanotechnology, 2008, 19: 155705
25 Harjo S, Kawasaki T, Tomota Y, et al. Work hardening, dislocation structure, and load partitioning in lath martensite determined by in situ neutron diffraction line profile analysis [J]. Metall. Mater. Trans., 2017, 48A: 4080
26 Hirsch P B, Howie A, Nicholson R B, et al. Electron Microscopy of Thin Crystals [M]. London: Butterworths, 1965: 462
27 Huang X, Morito S, Hansen N, et al. Ultra?ne structure and high strength in cold-rolled martensite [J]. Metall. Mater. Trans., 2012, 43A: 3517
28 Zhang K, Liu P, Li W, et al. Ultrahigh strength-ductility steel treated by a novel quenching- partitioning- tempering process [J]. Mater. Sci. Eng., 2014, A619: 205
29 He Y H, Rao Q H, Tan Y H. Investigation on the morphology of martensite in carbon steels [J]. J. Cent. South Univ. Technol., 1996, 3: 122
30 Jakobsen B, Poulsen H F, Lienert U, et al. Formation and subdivision of deformation structures during plastic deformation [J]. Science, 2006, 312: 889
31 Li Y Z, Huang M X. A method to calculate the dislocation density of a TWIP steel based on neutron diffraction and synchrotron X-ray diffraction [J]. Acta Metall. Sin., 2020, 56: 487
31 李亦庄, 黄明欣. 基于中子衍射和同步辐射X射线衍射的TWIP钢位错密度计算方法 [J]. 金属学报, 2020, 56: 487
32 Ungár T, Groma I, Wilkens M. Asymmetric X-ray line broadening of plastically deformed crystals. II. Evaluation procedure and application to [001]-Cu crystals [J]. J. Appl. Cryst., 1989, 22: 26
33 Ungár T, Harjo S, Kawasaki T, et al. Composite behavior of lath martensite steels induced by plastic strain, a new paradigm for the elastic-plastic response of martensitic steels [J]. Metall. Mater. Trans., 2017, 48A: 159
34 Daymond M R, Tomé C N, Bourke M A M. Measured and predicted intergranular strains in textured austenitic steel [J]. Acta Mater., 2000, 48: 553
35 Oliver E C, Daymond M R, Withers P J. Interphase and intergranular stress generation in carbon steels [J]. Acta Mater., 2004, 52: 1937
36 Muránsky O, ?ittner P, Zrník J, et al. In situ neutron diffraction investigation of the collaborative deformation -transformation mechanism in TRIP-assisted steels at room and elevated temperatures [J]. Acta Mater., 2008, 56: 3367
37 Zackay V F, Parker E R, Fahr D, et al. The enhancement of ductility in high-strength steels [J]. ASM Trans. Quart., 1967, 60: 252
38 Tomota Y, Tokuda H, Adachi Y, et al. Tensile behavior of TRIP-aided multi-phase steels studied by in situ neutron diffraction [J]. Acta Mater., 2004, 52: 5737
39 Mughrabi H. Dislocation wall and cell structures and long-range internal stresses in deformed metal crystals [J]. Acta Metall., 1983, 31: 1367
40 Ungár T, Mughrabi H, R?nnpagel D, et al. X-ray line-broadening study of the dislocation cell structure in deformed [001]-orientated copper single crystals [J]. Acta Metall., 1984, 32: 333
41 Mine Y, Hirashita K, Takashima H, et al. Micro-tension behaviour of lath martensite structures of carbon steel [J]. Mater. Sci. Eng., 2013, A560: 535
42 Ghassemi-Armaki H, Chen P, Bhat S, et al. Microscale-calibrated modeling of the deformation response of low-carbon martensite [J]. Acta Mater., 2013, 61: 3640
43 Essmann U, Mughrabi H. Annihilation of dislocations during tensile and cyclic deformation and limits of dislocation densities [J]. Philos. Mag., 1979, 40A: 731
44 Taylor G I. The mechanism of plastic deformation of crystals: Part I. -Theoretical [J]. Proc. Roy. Soc., 1934, 45A: 362
45 Jakobsen B, Poulsen H F, Lienert U, et al. Direct determination of elastic strains and dislocation densities in individual subgrains in deformation structures [J]. Acta Mater., 2007, 55: 3421
Outlines

/