SrZrO3掺杂引入的晶格畸变对Bi0.5Na0.5TiO3无铅铁电陶瓷结构和储能性能的影响研究

  • 朱明歌 ,
  • 朱孝培 ,
  • 张梦迪 ,
  • 丁茜 ,
  • 田娜 ,
  • 游才印
展开
  • 西安理工大学 材料科学与工程学院  西安 710049

收稿日期: 2025-07-29

  修回日期: 2025-10-20

  网络出版日期: 2025-12-31

基金资助

国家自然科学基金项目;中国博士后科学基金资助项目;西安市科学技术协会青年人才托举计划项目;西安理工大学研究生校企协同创新基金;陕西省教育厅科研计划项目;陕西省博士后科研项目

Study on the Effect of Lattice Distortion Induced by SrZrO3 Doping on the Structure and Energy Storage Properties of Bi0.5Na0.5TiO3 Lead-free Ferroelectric Ceramics

  • ZHU Meng-Ge ,
  • ZHU Xiao-Pei ,
  • ZHANG Meng-Di ,
  • ZHENG Qian ,
  • TIAN Na ,
  • YOU Cai-Yi
Expand
  • School of Materials Science and Engineering, Xi’an University of Technology, Xi’an 710048, China

Received date: 2025-07-29

  Revised date: 2025-10-20

  Online published: 2025-12-31

Supported by

the National Natural Science Foundation of China;the China Postdoctoral Science Foundation under Grant Number;the Shanxi Province Postdoctoral Research Project

摘要

无铅弛豫铁电陶瓷电容器因其超快放电速率和超高功率密度而在脉冲功率器件中应用非常广泛。然而,传统的Bi0.5Na0.5TiO3基陶瓷受制于高剩余极化和低击穿场强,导致储能密度严重不足。本工作系统地研究了(1-x)Bi0.5Na0.5TiO3-xSrZrO3(x=0、0.025、0.05、0.075,简写为BNT-xSZ)无铅铁电陶瓷的固溶特性以及晶格畸变对其结构和储能性能的影响规律。研究发现,SrZrO3掺杂引入的晶格畸变使陶瓷的c/a逐渐趋近于1,增强的局域结构无序抑制了长程极性有序,故陶瓷的弛豫系数γ从1.62增至1.86,但是过量的掺杂易引起结构失稳。此外,SrZrO3的掺杂阻碍了元素扩散并抑制了晶界迁移,故陶瓷的晶粒尺寸由未掺杂时的5.79μm降低至1.83μm(x=0.025)。阻抗分析结果表明,BNT-0.025SZ的电阻和活化能Ea远高于BNT。BNT-0.025SZ优异的绝缘性和高的活化能有助于增大氧空位传输阻力,从而提高击穿电场Eb。最终,BNT-0.025SZ在300 kV/cm场强下实现了2.08 J/cm3的高储能密度和83.14%的优异能量效率。该工作清晰地阐明了晶格畸变对BNT-xSZ二元固溶体结构稳定性的影响规律,也为设计高储能性能无铅铁电陶瓷提供了理论指导。

本文引用格式

朱明歌 , 朱孝培 , 张梦迪 , 丁茜 , 田娜 , 游才印 . SrZrO3掺杂引入的晶格畸变对Bi0.5Na0.5TiO3无铅铁电陶瓷结构和储能性能的影响研究[J]. 金属学报, 0 : 0 -0 . DOI: 10.11900/0412.1961.2025.00210

Abstract

Lead-free relaxor ferroelectric ceramic capacitors, owing to ultrafast discharge rates and ultrahigh power density, find widespread application in pulsed power devices. However, conventional Bi0.5Na0.5TiO3-based ceramics are limited in their commercial applications due to the severe lack of energy storage density caused by high remnant polarization and low breakdown electric field strength. In this study, the solid solution properties of (1-x)Bi0.5Na0.5TiO3-xSrZrO3 (x=0, 0.025, 0.05, 0.075, abbreviated as BNT-xSZ) lead-free ferroelectric ceramics were systematically investigated, and the effect of lattice distortion on their structure and energy storage performance was explored. The study revealed that the lattice distortion introduced by SrZrO3 doping caused the c/a ratio of the ceramic to gradually approach unity. This enhanced local structural disorder suppressed long-range polar ordering, resulting in an increase in the ceramic's relaxation coefficient γ from 1.62 to 1.86. However, excessive doping can readily induce structural instability. Furthermore, SrZrO3 doping hindered elemental diffusion and inhibited grain boundary migration, which reduced the grain size from 5.79 μm (pure) to 1.83 μm (x = 0.025). Impedance analysis revealed that the resistance and activation energy Ea of BNT-0.025SZ were significantly higher than those of BNT. The excellent insulating properties and high Ea of BNT-0.025SZ contributed to increased oxygen vacancy migration resistance, thus improving the breakdown electric field. Therefore, BNT-0.025SZ achieved a high energy storage density of 2.08 J/cm3 and an outstanding efficiency of 83.14% under an electric field of 300 kV/cm. These findings clearly elucidate the effect of lattice distortion on the structural stability of BNT-xSZ binary solid solutions and provide theoretical guidance for designing lead-free ferroelectric ceramics with high energy storage performance.
文章导航

/