TRIP型双相不锈钢Fe-19.6Cr-2Ni-2.9Mn-1.6Si的微裂纹形核及扩展
收稿日期: 2023-04-03
修回日期: 2023-06-10
网络出版日期: 2023-10-11
基金资助
国家自然科学基金项目(52275388, 52075474);河北省自然科学基金项目(E2022203206);燕山大学基础研究与创新人才培养项目(2021LGZD009, 2022BZZD002)
Microcrack Nucleation and Propagation of TRIP-Assisted Duplex Stainless Steel Fe-19.6Cr-2Ni-2.9Mn-1.6Si
Received date: 2023-04-03
Revised date: 2023-06-10
Online published: 2023-10-11
Supported by
National Natural Science Foundation of China(52275388, 52075474);Natural Science Foundation of Hebei Province(E2022203206);Cultivation Project for Basic Research and Innovation of Yanshan University(2021LGZD009, 2022BZZD002)
TRIP型双相钢由于马氏体相变可以平衡强度、提高延展性和提高成形性而受到广泛关注。然而,随着马氏体相变的演化,钢中微观组织和相分布特征不断变化,从而导致复杂的微裂纹形核和扩展。本工作利用SEM、EBSD观察TRIP型双相不锈钢Fe-19.6Cr-2Ni-2.9Mn-1.6Si在拉伸至工程应变为55%时的微裂纹特征,分析由材料微观组织特征(相分布、晶界或相界路径等)导致的微裂纹形核及扩展规律。结果表明,微裂纹主要分布在初始奥氏体与铁素体相界位置,约占总微裂纹数的70%,铁素体相内晶界位置的微裂纹数约占总数的20%,初始奥氏体相内晶界位置的微裂纹数仅占总数的10%左右。微裂纹的形核易发生在多类型界面的交汇位置,主要的微裂纹形核位置可分为3类:相变马氏体/铁素体/残余奥氏体三相的交汇点,相变马氏体/铁素体相界和铁素体晶界交叉点,及相变马氏体/铁素体相界和初始奥氏体晶界交叉点。这些裂纹源在相界附近相变马氏体的影响下,易沿初始奥氏体与铁素体相界或与相界夹角较小(< 30°)的铁素体晶界扩展,而由于马氏体相变松弛了奥氏体相内的应力集中,导致微裂纹不易沿奥氏体晶界扩展。
关键词: TRIP型双相不锈钢; 微裂纹; 裂纹形核; 裂纹扩展; 相变马氏体
张文彬 , 李小龙 , 郝硕 , 刘胜杰 , 蔡星周 , 陈雷 , 金淼 . TRIP型双相不锈钢Fe-19.6Cr-2Ni-2.9Mn-1.6Si的微裂纹形核及扩展[J]. 金属学报, 2025 , 61(4) : 608 -618 . DOI: 10.11900/0412.1961.2023.00149
The transformation-induced plasticity (TRIP) effect considerably enhances the material properties of TRIP-assisted duplex steel due to the martensitic transformation. However, as martensitic transformation progresses, a complex microstructure forms from the intermixing of three phases (i.e., austenite, ferrite, and martensite) in the steel, which results in complex damage behavior, crack nucleation, and propagation characteristics. In this study, under engineering strain up to 55%, TRIP-assisted duplex stainless steel Fe-19.6Cr-2Ni-2.9Mn-1.6Si was characterized to investigate microcrack characteristics. Herein, different types of microcracks were statistically categorized using SEM. Additionally, microcrack nucleation and propagation laws were analyzed in light of microscopic features characterized by EBSD, including phase distribution and grain and phase boundaries. The results show that the majority of microcracks are situated at the phase boundary between original austenite and ferrite, constituting about 70% of all microcracks. The number of microcracks located at the ferrite grain boundary accounts for about 20% of the total, while the number of microcracks located at the original austenite grain boundary accounts for only about 10% of the total. The interface between martensite and ferrite emerged as the primary site for microcrack nucleation. Furthermore, the study identifies three distinct microcrack nucleation sites influenced by various boundary types: at the intersection of martensite, ferrite, and austenite phases; at the junction of martensite/ferrite phase boundary and ferrite grain boundary; and at the cross point of martensite/ferrite phase boundary and the original austenite grain boundary. Therefore, microcracks might propagate along the original austenite/ferrite phase boundary or ferrite grain boundary with a smaller angle (< 30°) to the phase boundary. In addition, microcracks are less apt to propagate along the austenite grain boundary.
| 1 | Li Y, Zhong S X, Luo H, et al. Intermediate stacking fault and twinning induced cooperative strain evolution of dual phase in lean duplex stainless steels with excellent cryogenic strength-ductility combinations [J]. Mater. Sci. Eng., 2022, A831: 142347 |
| 2 | Kang J Y, Kim H, Kim K I, et al. Effect of austenitic texture on tensile behavior of lean duplex stainless steel with transformation induced plasticity (TRIP) [J]. Mater. Sci. Eng., 2017, A681: 114 |
| 3 | Herrera C, Ponge D, Raabe D. Design of a novel Mn-based 1 GPa duplex stainless TRIP steel with 60% ductility by a reduction of austenite stability [J]. Acta Mater., 2011, 59: 4653 |
| 4 | Srivastava A, Ghassemi-Armaki H, Sung H, et al. Micromechanics of plastic deformation and phase transformation in a three-phase TRIP-assisted advanced high strength steel: Experiments and modeling [J]. J. Mech. Phys. Solids, 2015, 78: 46 |
| 5 | Soleimani M, Kalhor A, Mirzadeh H. Transformation-induced plasticity (TRIP) in advanced steels: A review [J]. Mater. Sci. Eng., 2020, A795: 140023 |
| 6 | Su X F, Chen H R, Kennedy D, et al. Effects of interphase strength on the damage modes and mechanical behaviour of metal-matrix composites [J]. Composites, 1999, 30A: 257 |
| 7 | Sun X, Choi K S, Soulami A, et al. On key factors influencing ductile fractures of dual phase (DP) steels [J]. Mater. Sci. Eng., 2009, A526: 140 |
| 8 | Saai A, Hopperstad O S, Granbom Y, et al. Influence of volume fraction and distribution of martensite phase on the strain localization in dual phase steels [J]. Proc. Mater. Sci., 2014, 3: 900 |
| 9 | Tasan C C, Hoefnagels J P M, Diehl M, et al. Strain localization and damage in dual phase steels investigated by coupled in-situ deformation experiments and crystal plasticity simulations [J]. Int. J. Plast., 2014, 63: 198 |
| 10 | Motoyashiki Y, Brückner-Foit A, Sugeta A. Microstructural influence on small fatigue cracks in a ferritic-martensitic steel [J]. Eng. Fract. Mech., 2008, 75: 768 |
| 11 | Xie Q G, Lian J H, Sun F W, et al. The lattice strain ratio in characterizing the grain-to-grain interaction effect and its specific insight on the plastic deformation of polycrystalline materials [J]. J. Strain Anal. Eng. Des., 2018, 53: 353 |
| 12 | Morsdorf L, Jeannin O, Barbier D, et al. Multiple mechanisms of lath martensite plasticity [J]. Acta Mater., 2016, 121: 202 |
| 13 | Du C, Hoefnagels J P M, Vaes R, et al. Plasticity of lath martensite by sliding of substructure boundaries [J]. Scr. Mater., 2016, 120: 37 |
| 14 | Calcagnotto M, Adachi Y, Ponge D, et al. Deformation and fracture mechanisms in fine- and ultrafine-grained ferrite/martensite dual-phase steels and the effect of aging [J]. Acta Mater., 2011, 59: 658 |
| 15 | Park K, Nishiyama M, Nakada N, et al. Effect of the martensite distribution on the strain hardening and ductile fracture behaviors in dual-phase steel [J]. Mater. Sci. Eng., 2014, A604: 135 |
| 16 | Paul S K. Real microstructure based micromechanical model to simulate microstructural level deformation behavior and failure initiation in DP 590 steel [J]. Mater. Des., 2013, 44: 397 |
| 17 | Marvi-Mashhadi M, Mazinani M, Rezaee-Bazzaz A. FEM modeling of the flow curves and failure modes of dual phase steels with different martensite volume fractions using actual microstructure as the representative volume [J]. Comput. Mater. Sci., 2012, 65: 197 |
| 18 | Cheloee Darabi A, Kadkhodapour J, Pourkamali Anaraki A, et al. Micromechanical modeling of damage mechanisms in dual-phase steel under different stress states [J]. Eng. Fract. Mech., 2021, 243: 107520 |
| 19 | Yuenyong J, Uthaisangsuk V. Micromechanics based modelling of fatigue crack initiation of high strength steel [J]. Int. J. Fatigue, 2020, 139: 105762 |
| 20 | Darabi A C, Guski V, Butz A, et al. A comparative study on mechanical behavior and damage scenario of DP600 and DP980 steels [J]. Mech. Mater., 2020, 143: 103339 |
| 21 | Alaie A, Ziaei Rad S, Kadkhodapour J, et al. Effect of microstructure pattern on the strain localization in DP600 steels analyzed using combined in-situ experimental test and numerical simulation [J]. Mater. Sci. Eng., 2015, A638: 251 |
| 22 | Zhang J C, Di H S, Deng Y G, et al. Effect of martensite morphology and volume fraction on strain hardening and fracture behavior of martensite-ferrite dual phase steel [J]. Mater. Sci. Eng., 2015, A627: 230 |
| 23 | Archie F, Li X L, Zaefferer S. Micro-damage initiation in ferrite-martensite DP microstructures: A statistical characterization of crystallographic and chemical parameters [J]. Mater. Sci. Eng., 2017, A701: 302 |
| 24 | Moallemi M, Kim S J, Zarei-Hanzaki A, et al. Strain hardening analysis and deformation micromechanisms in high strength-high ductility metastable duplex stainless steels: Role of sustained stacking faults in the work hardening [J]. Mater. Charact., 2023, 197: 112662 |
| 25 | Connolly D S, Kohar C P, Mishra R K, et al. A new coupled thermomechanical framework for modeling formability in transformation induced plasticity steels [J]. Int. J. Plast., 2018, 103: 39 |
| 26 | Kim E Y, Woo W C, Heo Y U, et al. Effect of kinematic stability of the austenite phase on phase transformation behavior and deformation heterogeneity in duplex stainless steel using the crystal plasticity finite element method [J]. Int. J. Plast., 2016, 79: 48 |
| 27 | Yasnikov I S, Vinogradov A, Estrin Y. Revisiting the Considère criterion from the viewpoint of dislocation theory fundamentals [J]. Scr. Mater., 2014, 76: 37 |
| 28 | Zhang H Y. Transformation-induced plasticity characteristics and temperature dependence of Cr20Mn3Cu2NiN lean duplex stainless steel [D]. Qinhuangdao: Yanshan University, 2023 |
| 张寰宇. Cr20Mn3Cu2NiN节约型双相不锈钢相变诱导塑性特征及其温度依赖性 [D]. 秦皇岛: 燕山大学, 2023 | |
| 29 | Gu G H, Seo M H, Suh D W, et al. Observation of multi-scale damage evolution in transformation-induced plasticity steel under bending condition [J]. Mater. Today Commun., 2023, 34: 105291 |
| 30 | Kang J, Ososkov Y, Embury J D, et al. Digital image correlation studies for microscopic strain distribution and damage in dual phase steels [J]. Scr. Mater., 2007, 56: 999 |
| 31 | Lian J H, Yang H Q, Vajragupta N, et al. A method to quantitatively upscale the damage initiation of dual-phase steels under various stress states from microscale to macroscale [J]. Comput. Mater. Sci., 2014, 94: 245 |
| 32 | Han Q H, Kang Y L, Hodgson P D, et al. Quantitative measurement of strain partitioning and slip systems in a dual-phase steel [J]. Scr. Mater., 2013, 69: 13 |
| 33 | Das A, Tarafder S, Sivaprasad S, et al. Influence of microstructure and strain rate on the strain partitioning behaviour of dual phase steels [J]. Mater. Sci. Eng., 2019, A754: 348 |
| 34 | Feng R, Zhang M H, Chen N L, et al. Finite element simulation of the effect of stress relaxation on strain-induced martensitic transformation [J]. Acta Metall. Sin., 2014, 50: 498 |
| 冯 瑞, 张美汉, 陈乃录 等. 应力松弛对应变诱发马氏体相变影响的有限元模拟 [J]. 金属学报, 2014, 50: 498 |
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