聚变增殖包层用低活化9Cr-ODS钢的室温低周疲劳行为
收稿日期: 2023-01-31
修回日期: 2023-04-28
网络出版日期: 2023-08-21
基金资助
国家重点研发计划项目(2019YFE03130000);国家自然科学基金项目(51971217)
Low Cycle Fatigue Behavior of 9Cr-ODS Steel as a Fusion Blanket Structural Material at Room Temperature
Received date: 2023-01-31
Revised date: 2023-04-28
Online published: 2023-08-21
Supported by
National Key Research and Development Program of China(2019YFE03130000);National Natural Science Foundation of China(51971217)
在现有研究中,低活化9Cr-ODS钢虽然具有优异的高温性能,但其低周疲劳性能及微观组织演变规律尚未全面揭示,本工作旨在揭示其在不同应变幅下的循环响应和裂纹扩展特性。采用应变控制测试方法,研究了低活化9Cr-ODS钢在0.3%~0.8%应变幅范围内的室温低周疲劳性能,包括循环应力响应曲线、滞后回线、应变幅与寿命以及应力幅与塑性应变的关系,给出了相应的疲劳参数,并分析了疲劳过程中微观组织演变、疲劳断口形貌及裂纹扩展特性等。结果表明,9Cr-ODS钢的循环应力响应行为与应变幅有关。随应变幅增加,材料的峰值拉应力增加,疲劳寿命降低,循环应变-寿命满足Coffin-Manson关系。9Cr-ODS钢在所有应变幅下未出现明显的循环硬化,但在0.5%~0.8%较高应变幅范围内发生了一定的循环软化。微观组织分析表明,随循环应变幅增加,亚结构发生了回复,位错密度降低,平均晶粒尺寸及大角度晶界占比逐渐增加,从而导致9Cr-ODS钢的循环软化。疲劳裂纹起源于样品表面,但裂纹源附近均未发现明显的夹杂物或析出相。裂纹以穿晶方式扩展,9Cr-ODS钢细的原始奥氏体晶界及亚晶界对裂纹扩展具有强烈的抑制作用。此外,在相同低应变幅且不降低循环疲劳寿命条件下,9Cr-ODS钢所能承受的峰值拉应力达到低活化铁素体/马氏体钢的2倍,显示出较优越的低周疲劳强度。
王旗涛 , 李艳芬 , 张家榕 , 李尧志 , 付海阳 , 李新乐 , 严伟 , 单以银 . 聚变增殖包层用低活化9Cr-ODS钢的室温低周疲劳行为[J]. 金属学报, 2025 , 61(2) : 323 -335 . DOI: 10.11900/0412.1961.2023.00034
Adequate studies have not been conducted on the low cycle fatigue properties of oxide dispersion strengthened (ODS) steels that are typically used for fusion reactors worldwide. Moreover, the majority of the fatigue properties are examined with a small sample size due to the restricted manufacturing capacity, which is insufficient for determining the comprehensive properties of bulk materials. Research on the fatigue properties of Chinese ODS steels was conducted recently. However, it is quite uncommon to report the fatigue properties of self-produced 9Cr-ODS steel. Consequently, this work is the first to examine the effect of a cyclic strain on the low cycle fatigue behavior of a representative low-activation 9Cr-ODS martensitic steel. Hence, the strain control test method was employed here in a strain amplitude range of 0.3%-0.8% at room temperature. The cyclic stress response curves, hysteresis loops, relationships between strain amplitude and life, stress amplitude and plastic strain were obtained, and the corresponding fatigue parameters were summarized. Furthermore, the microstructural evolution, fatigue fracture morphology, and crack propagation characteristics during the fatigue process were analyzed. The results revealed that the cyclic stress response behavior of the 9Cr-ODS steel was related to the strain amplitude. With an increase in the strain amplitude, the peak stress in the tension zone of 9Cr-ODS steel increased and the fatigue life decreased. The relationship between cyclic strain and life agreed well with the Coffin-Manson model. Additionally, the 9Cr-ODS steel had no obvious cyclic hardening but revealed a cyclic softening under higher strain amplitudes of 0.5%-0.8%. The microstructure analysis showed that for higher cyclic strain amplitudes, the average grain size and the fraction of the large-angle grain boundaries increased gradually with a reduction in the dislocation density, leading to the cyclic softening of the material. The fatigue crack initiated at the surface and propagated inward by the transgranular mode. The fine grain boundaries and subgrain boundaries of the 9Cr-ODS steel could induce crack deflection, reduce crack propagation rate, and increase fatigue crack propagation life. Moreover, under the same strain amplitude, the peak stress in the tension zone of the steel was almost twice that of the China low activation martensitic (CLAM) steel without a reduction in the fatigue life, indicating a superior low cycle fatigue resistance of the 9Cr-ODS steel.
Key words: ODS steel; low cycle fatigue; fatigue life; microstructure; fracture characteristic
| 1 | Marmy P, Kruml T. Low cycle fatigue of Eurofer 97 [J]. J. Nucl. Mater., 2008, 377: 52 |
| 2 | Nishimura A, Nagasaka T, Inoue N, et al. Low cycle fatigue properties of a low activation ferritic steel (JLF-1) at room temperature [J]. J. Nucl. Mater., 2000, 283-287: 677 |
| 3 | Stubbins J F, Gelles D S. Fatigue performance and cyclic softening of F82H, a ferritic-martensitic steel [J]. J. Nucl. Mater., 1996, 233-237: 331 |
| 4 | Hirose T, Tanigawa H, Ando M, et al. Radiation effects on low cycle fatigue properties of reduced activation ferritic/martensitic steels [J]. J. Nucl. Mater., 2002, 307-311: 304 |
| 5 | Lindau R, M?eslang A, Rieth M, et al. Present development status of EUROFER and ODS-EUROFER for application in blanket concepts [J]. Fusion Eng. Des., 2005, 75-79: 989 |
| 6 | Hu X, Huang L X, Wang W G, et al. Low cycle fatigue properties of CLAM steel at room temperature [J]. Fusion Eng. Des., 2013, 88: 3050 |
| 7 | Chauhan A, Litvinov D, de Carlan Y, et al. Study of the deformation and damage mechanisms of a 9Cr-ODS steel: Microstructure evolution and fracture characteristics [J]. Mater. Sci. Eng., 2016, A658: 123 |
| 8 | Cui C, Huang C, Su X P, et al. R&D on advanced cladding materials ODS alloys for fast reactor [J]. Nucl. Sci. Eng., 2011, 31: 305 |
| 崔 超, 黄 晨, 苏喜平 等. 快堆先进包壳材料ODS合金发展研究 [J]. 核科学与工程, 2011, 31: 305 | |
| 9 | Li S F. Study on oxide strengthened dispersion alloys for Generation Ⅳ advanced nuclear systems [D]. Beijing: University of Science and Technology Beijing, 2016 |
| 李少夫. 用于第四代先进核能系统的氧化物弥散强化合金的研究 [D]. 北京: 北京科技大学, 2016 | |
| 10 | Yamashita S, Watanabe S, Ohnuki S, et al. Effect of mechanical alloying parameters on irradiation damage in oxide dispersion strengthened ferritic steels [J]. J. Nucl. Mater., 2000, 283-287: 647 |
| 11 | Lv Z. Development and prospect of nano-structured ODS steels for fusion reactor first wall application [J]. Atom. Energy Sci. Technol., 2011, 45: 1105 |
| 吕 铮. 聚变堆第一壁用纳米结构ODS钢的发展与前瞻 [J]. 原子能科学技术, 2011, 45: 1105 | |
| 12 | Zinkle S J, Snead L L. Designing radiation resistance in materials for fusion energy [J]. Annu. Rev. Mater. Res., 2014, 44: 241 |
| 13 | Lucas G E. High chromium ferritic and martensitic steels for nuclear applications: R. Klueh and D. Harries [J]. J. Nucl. Mater., 2002, 302: 232 |
| 14 | Xu Y P, Lv Y M, Zhou H S, et al. A review on the development of the structural materials of the fusion blanket [J]. Mater. Rev., 2018, 32: 2897 |
| 徐玉平, 吕一鸣, 周海山 等. 核聚变堆包层结构材料研究进展及展望 [J]. 材料导报, 2018, 32: 2897 | |
| 15 | Chauhan A, Hoffmann J, Litvinov D, et al. High-temperature low-cycle fatigue behavior of a 9Cr-ODS steel: Part 2 - hold time influence, microstructural evolution and damage characteristics [J]. Mater. Sci. Eng., 2018, A730: 197 |
| 16 | Stra?berger L, Chauhan A, Czink S, et al. High-temperature low-cycle fatigue behavior and microstructural evolution of an ODS steel based on conventional T91 [J]. Int. J. Fatigue, 2017, 100: 50 |
| 17 | Xu H J. Research on microstructure and mechanical property of 15Cr-ODS ferritic alloys [D]. Shenyang: Northeastern University, 2017 |
| 徐海健. 15Cr-ODS铁素体合金微观结构及力学性能的研究 [D]. 沈阳: 东北大学, 2017 | |
| 18 | Chauhan A, Hoffmann J, Litvinov D, et al. High-temperature low-cycle fatigue behavior of a 9Cr-ODS steel: Part 1 - pure fatigue, microstructure evolution and damage characteristics [J]. Mater. Sci. Eng., 2017, A707: 207 |
| 19 | Klueh R L, Gelles D S, Jitsukawa S, et al. Ferritic/martensitic steels—Overview of recent results [J]. J. Nucl. Mater., 2002, 307-311: 455 |
| 20 | Mukhopadhyay D K, Froes F H, Gelles D S. Development of oxide dispersion strengthened ferritic steels for fusion [J]. J. Nucl. Mater., 1998, 258-263: 1209 |
| 21 | Zhang J R, Li Y F, Rui X, et al. Study on microstructure and mechanical properties of 9Cr-ODS steel prepared by a powder hot forging process [J]. J. Iron Steel Res., 2021, 33(11): 1171 |
| 张家榕, 李艳芬, 芮 祥 等. 粉末热锻制备9Cr-ODS钢的微观组织和力学性能研究 [J]. 钢铁研究学报, 2021, 33(11): 1171 | |
| 22 | Rui X, Li Y F, Zhang J R, et al. Microstructure and mechanical properties of a novel designed 9Cr-ODS steel synergically strengthened by nano precipitates [J]. Acta Metall Sin, 2023, 59: 1590 |
| 芮 祥, 李艳芬, 张家榕 等. 新型纳米复合强化9Cr-ODS钢的设计、组织与力学性能 [J]. 金属学报, 2023, 59: 1590 | |
| 23 | Coffin L F. A study of the effects of cyclic thermal stresses on a ductile metal [J]. J. Fluids Eng., 1954, 76: 931 |
| 24 | Kohyama A, Hishinuma A, Gelles D S, et al. Low-activation ferritic and martensitic steels for fusion application [J]. J. Nucl. Mater., 1996, 233-237: 138 |
| 25 | Srivatsan T S, Al-Hajri M, Troxell J D. The tensile deformation, cyclic fatigue and final fracture behavior of dispersion strengthened copper [J]. Mech. Mater., 2004, 36: 99 |
| 26 | Kuběna I, Kruml T, Sp?tig P, et al. Fatigue behaviour of ODS ferritic-martensitic Eurofer steel [J]. Procedia Eng., 2010, 2: 717 |
| 27 | Li H L, Nishimura A, Li Z X, et al. Low cycle fatigue behavior of JLF-1 steel at elevated temperatures [J]. Fusion Eng. Des., 2006, 81: 241 |
| 28 | Hu X, Huang L X, Yan W, et al. Microstructure evolution in CLAM steel under low cycle fatigue [J]. Mater. Sci. Eng., 2014, A607: 35 |
| 29 | Msolli S. Thermoelastoviscoplastic modeling of RAFM steel JLF-1 using tensile and low cycle fatigue experiments [J]. J. Nucl. Mater., 2014, 451: 336 |
| 30 | Bhattacharya A, Zinkle S J, Henry J, et al. Irradiation damage concurrent challenges with RAFM and ODS steels for fusion reactor first-wall/blanket: A review [J]. J. Phys. Energy, 2022, 4: 034003 |
| 31 | Zhou H W, Bai F M, Yang L, et al. Low-cycle fatigue behavior of 1100 MPa grade high-strength steel [J]. Acta Metall. Sin., 2020, 56: 937 |
| 周红伟, 白凤梅, 杨 磊 等. 1100 MPa级高强钢的低周疲劳行为 [J]. 金属学报, 2020, 56: 937 | |
| 32 | Zhao C, Huang J F, Zhang J, et al. Low-cycle fatigue behavior of 4Cr5MoSiV1 hot-work die steel at 700 oC [J]. Chin. J. Eng., 2020, 42: 602 |
| 赵 超, 黄进峰, 张 津 等. 4Cr5MoSiV1热作模具钢700 ℃的低周疲劳行为 [J]. 工程科学学报, 2020, 42: 602 |
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