研究论文

Ti6246钛合金 βα 相变中晶界 α 相生长行为及其对微织构的影响

  • 齐敏 ,
  • 王倩 ,
  • 马英杰 ,
  • 曹贺萌 ,
  • 黄森森 ,
  • 雷家峰 ,
  • 杨锐
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  • 1 中国科学技术大学 材料科学与工程学院 沈阳 110016
    2 中国科学院金属研究所 师昌绪先进材料创新中心 沈阳 110016
齐 敏,女,1995年生,博士生
马英杰,yjma@imr.ac.cn,主要从事结构钛合金研究

收稿日期: 2023-01-03

  修回日期: 2023-07-17

  网络出版日期: 2023-07-26

基金资助

国家重点研发计划项目(2021YFC2801801);国家自然科学基金项目(51871225)

Growth Behavior of Grain Boundary α Phase and Its Effect on the Microtexture During βα Phase Transformation in Ti6246 Titanium Alloys

  • QI Min ,
  • WANG Qian ,
  • MA Yingjie ,
  • CAO Hemeng ,
  • HUANG Sensen ,
  • LEI Jiafeng ,
  • YANG Riu
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  • 1 School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
    2 Shichangxu Innovation Center for Advanced Materials, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
MA Yingjie, professor, Tel: 13840026329, E-mail: yjma@imr.ac.cn

Received date: 2023-01-03

  Revised date: 2023-07-17

  Online published: 2023-07-26

Supported by

National Key Research and Development Program of China(2021YFC2801801);National Natural Science Foundation of China(51871225)

摘要

钛合金的初始α片层组织特征对其热机械加工过程中的显微组织演化及力学性能具有重要影响,掌握初始α片层组织演化规律是实现钛合金微观组织和力学性能精准调控的前提条件。本工作通过中断炉冷热处理方法研究了Ti6246钛合金βα相转变过程中初始α片层组织的演变规律,分析了晶界α相(αGB)的生长行为及其对后续晶内α片层生长、微织构强度的影响。结果表明,钛合金由β单相区缓冷至α + β两相区的过程中,与两侧β晶粒都符合Burgers取向关系(BOR)的αGB (2-BOR αGB)优先在β晶界处形核。而后,与2-BOR αGB取向相近的晶内α片层在αGB处形核并向两侧β晶粒内生长,2-BOR αGB与两侧α片层在晶界处形成较强的微织构。在α相生长早期,两侧β晶粒与2-BOR αGB的BOR偏差越小,较强的微织构形成越早。除2-BOR αGB优先发生βα相转变外,与单侧β晶粒符合BOR的αGB (1-BOR αGB)也形核生长,但是,与1-BOR αGB取向相近的晶内α片层仅在符合BOR的单侧β晶粒内形成,而在另一侧β晶粒中则形成取向不同的晶内α片层,在晶界处形成较弱的微织构。

本文引用格式

齐敏 , 王倩 , 马英杰 , 曹贺萌 , 黄森森 , 雷家峰 , 杨锐 . Ti6246钛合金 βα 相变中晶界 α 相生长行为及其对微织构的影响[J]. 金属学报, 2025 , 61(2) : 265 -277 . DOI: 10.11900/0412.1961.2023.00002

Abstract

The initial lamellar microstructure of titanium alloys significantly affects their microstructural evolution and mechanical property during thermo-mechanical treatments. Thus, the evolution of the initial lamellar microstructure must be explored to control the microstructure and enhance the mechanical property. The present work focuses on the evolution of the lamellar microstructure during βα phase transformation via interrupted furnace cooling experiments to analyze the growth behavior of the grain boundary α phase (αGB) and its effect on the subsequent growth of intragranular α lamellae and microtexture. Results show that when titanium alloy furnace cools from the β phase field to the α + β phase field, the αGB holding Burgers orientation relationship (BOR) with both sides of β grains (2-BOR αGB) has an advantage for early transformation at the β grain boundary. In particular, type II (49.5°/<110>) and type III (60°/<110>) β grain boundaries are preferential sites for the early nucleation of αGB particles. As the temperature decreases, α lamellae holding similar orientation to 2-BOR αGB grow to both sides of β grains. Thus, 2-BOR αGB and both sides of α lamellae form a strong microtexture at the grain boundary. At the early growth period of the α phase, the smaller the θ2-BOR (misorientation of the close-oriented αGB variant pair of parents β1 and β2) of 2-BOR αGB, the earlier the formation of a strong microtexture at the grain boundary. 2-BOR αGB preferentially precipitates, whereas the αGB holding BOR with only one side of the β grain (1-BOR αGB) nucleates. α lamellae holding a similar orientation to 1-BOR αGB grow to one side of the BOR-β grain (holding BOR with αGB), whereas α lamellae with a different orientation grow in the non-BOR-β grain. Thus, 1-BOR αGB and one side of α lamellae form a weak microtexture at the grain boundary.

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