研究论文

GH4720Li合金毫米级粗大晶粒热变形获得均匀等轴晶粒的可行性及工艺控制

  • 刘超 ,
  • 姚志浩 ,
  • 江河 ,
  • 董建新
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  • 北京科技大学 材料科学与工程学院 北京 100083
刘 超,男,1994年生,博士生

收稿日期: 2020-10-23

  修回日期: 2021-01-04

  网络出版日期: 2021-04-21

基金资助

国家自然科学基金项目(51771016)

The Feasibility and Process Control of Uniform Equiaxed Grains by Hot Deformation in GH4720Li Alloy with Millimeter-Level Coarse Grains

  • Chao LIU ,
  • Zhihao YAO ,
  • He JIANG ,
  • Jianxin DONG
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  • School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China
YAO Zhihao, associate professor, Tel: 13671347055, E-mail: zhihaoyao@ustb.edu.cn

Received date: 2020-10-23

  Revised date: 2021-01-04

  Online published: 2021-04-21

Supported by

National Natural Science Foundation of China(51771016)

摘要

为了阐明GH4720Li合金毫米级粗大晶粒再结晶和塑性协调的可行性,对毫米级晶粒的GH4720Li试样在不同的变形参数下(变形温度为1130、1160和1190℃,应变速率为0.001、0.01、0.1和1 s-1,工程应变为50%)的热变形行为进行研究,并与细晶GH4720Li合金的热变形行为进行对比。结果表明,具有毫米级粗大晶粒的GH4720Li试样对变形温度更加敏感,且在1160~1190℃、0.001~0.01 s-1的范围内可以获得完全再结晶组织,但综合考虑再结晶和热变形塑性的控制范围后,确定毫米级粗晶GH4720Li合金应在适中的变形温度下以较低的应变速率进行热变形才能获得均匀的等轴晶组织且不开裂,较好的变形工艺为1160℃、0.01 s-1

本文引用格式

刘超 , 姚志浩 , 江河 , 董建新 . GH4720Li合金毫米级粗大晶粒热变形获得均匀等轴晶粒的可行性及工艺控制[J]. 金属学报, 2021 , 57(10) : 1309 -1319 . DOI: 10.11900/0412.1961.2020.00415

Abstract

For nickel-based GH4720Li superalloys, fine-grained structures can be obtained via hot deformation in a two-phase area. However, obvious recrystallized grains' coarsening occurs because of the lack of prime γ' pinning grain boundary when hot deformation occurs in a single-phase area. Much attention is directed to the hot deformation of GH4720Li alloys with fine grains. Moreover, several studies have reported the hot deformation behavior of coarse-grained GH4720Li alloys, with maximum grain sizes of several hundred microns. However, only a few studies report about the hot deformation of GH4720Li alloy with millimeter-level coarse grains. Coarse grains recrystallize incompletely and can reduce the hot deformation plasticity of GH4720Li alloy. Thus, to clarify the coordination feasibility between recrystallization and the hot deformation plasticity of GH4720Li alloy with millimeter-level coarse grains, the hot deformation behavior of GH4720Li alloy with millimeter-level coarse grains was investigated under different deformation parameters (deformation temperature of 1130, 1160, and 1190°C; strain rates of 0.001, 0.01, 0.1, and 1 s-1; and engineering strain of 50%) and compared with the hot deformation behavior of fine-grained GH4720Li alloy. The results show that the GH4720Li sample with millimeter-level coarse grains is more sensitive to the deformation temperature, but the fine-grained GH4720Li alloy is more sensitive to strain rate. The completely recrystallized structure of the GH4720Li sample with millimeter-level coarse grains can be obtained in the range of 1160-1190°C and 0.001-0.01 s-1. However, a meager strain rate can cause an undesirable and obvious grain growth. After comprehensively combining the recrystallization control range and the hot deformation plasticity of millimeter-level coarse-grained GH4720Li alloy, it was found that the millimeter-level coarse-grained GH4720Li alloy should be thermally deformed at a moderate deformation temperature and a reduced strain rate of 1160oC and 0.01 s-1, respectively, to obtain the uniform equiaxed grains structure without cracking, and better deformation.

参考文献

1 Sims C T, Stolof N S, Hangel W. Superalloys Ⅱ [M]. New York: John Wiley & Sons, Inc., 1987: 8
2 Furrer D, Fecht H. Ni-based superalloys for turbine discs [J]. JOM, 1999, 51(1): 14
3 Bryant D J, Mclntosh G. The manufacture and evaluation of a large turbine disc in cast and wrought alloy 720Li [A]. Superalloys 1996 [C]. Pittsburgh, PA: The Minerals, Metals, & Materials Society, 1996: 713
4 Gu Y F, Cui C Y, Yuan Y, et al. Research progress in a high performance cast & wrought superalloy for turbine disc applications [J]. Acta Metall. Sin., 2015, 51: 1191
4 谷月峰, 崔传勇, 袁 勇等. 一种高性能航空涡轮盘用铸锻合金的研究进展 [J]. 金属学报, 2015, 51: 1191
5 Matsui T, Takizawa H, Kikuchi H, et al. The microstructure prediction of alloy720Li for turbine disk applications [A]. Superalloys 2000 [C]. Pittsburgh, PA: The Minerals, Metals, & Materials Society, 2000: 127
6 Yu Q Y. Study on the correlation between γ' phases, grain size and deformation parameters for GH4720Li alloy [D]. Beijing: University of Science and Technology Beijing, 2013
6 于秋颖. GH4720Li合金γ'相、晶粒度和热加工参数关联性研究 [D]. 北京: 北京科技大学, 2013
7 Chang L T, Jin H, Sun W R. Solidification behavior of Ni-base superalloy Udimet 720Li [J]. J. Alloys Compd., 2015, 653: 266
8 Song X P, Li H Y, Gai J F, et al. The decomposition of metastable high temperature γ' precipitates in U720Li alloy [J]. Acta Metall. Sin., 2005, 41: 1233
8 宋西平, 李红宇, 盖靖峰等. U720Li合金高温析出γ′相的失稳分解 [J]. 金属学报, 2005, 41: 1233
9 Mao J, Chang K M, Yang W H, et al. Cooling precipitation and strengthening study in powder metallurgy superalloy U720Li [J]. Metall. Mater. Trans., 2001, 32A: 2441
10 Yu Q Y, Yao Z H, Dong J X. Hot deformation behavior of uniform fine-grained GH4720Li alloy based on its processing map [J]. Int. J. Min. Met. Mater., 2016, 23: 83
11 Chen J Y, Dong J X, Zhang M C, et al. Deformation mechanisms in a fine-grained Udimet 720Li nickel-base superalloy with high volume fractions of γ' phases [J]. Mater. Sci. Eng., 2016, A673: 122
12 Chen J Y, Zhang P D, Dong J X, et al. Relevance of primary γ' dissolution and abnormal grain growth in Udimet 720Li [J]. Mater. Trans., 2015, 56: 1968
13 Monajati H, Taheri A K, Jahazi M, et al. Deformation characteristics of isothermally forged Udimet 720 nickel-base superalloy [J]. Metall. Mater. Trans., 2005, 36A: 895
14 Liu F F, Chen J Y, Dong J X, et al. The hot deformation behaviors of coarse, fine and mixed grain for Udimet 720Li superalloy [J]. Mater. Sci. Eng., 2016, A651: 102
15 Wan Z P, Hu L X, Sun Y, et al. Hot deformation behavior and processing workability of a Ni-based alloy [J]. J. Alloys Compd., 2018, 769: 367
16 Wang T, Wan Z P, Sun Y, et al. Dynamic softening behavior and microstructure evolution of nickel base superalloy [J]. Acta Metall. Sin., 2018, 54: 83
16 王 涛, 万志鹏, 孙 宇等. 镍基变形高温合金动态软化行为与组织演变规律研究 [J]. 金属学报, 2018, 54: 83
17 Zhao Y X, Fu S H, Zhang S W, et al. An advanced cast/wrought technology for GH720Li alloy disk from fine grain ingot [A]. 7th International Symposium on Superalloy 718 and Derivatives [C]. Pittsburgh, PA: The Minerals, Metals, & Materials Society, 2010: 271
18 Fahrmann M, Suzuki A. Effect of cooling rate on gleeble hot ductility of Udimet alloy 720 billet [A]. Superalloys 2008 [C]. Pittsburgh, PA: The Minerals, Metals, & Materials Society, 2008: 311
19 Wan Z P, Wang T, Sun Y, et al. Dynamic softening mechanisms of GH4720Li alloy during hot deformation [J]. Acta Metall. Sin., 2019, 55: 213
19 万志鹏, 王 涛, 孙 宇等. GH4720Li合金热变形过程动态软化机制 [J]. Acta Metall. Sin., 2019, 55: 213
20 Qu J L, Bi Z N, Du J H, et al. Hot deformation behavior of nickel-based superalloy GH4720Li [J]. J. Iron Steel Res. Int., 2011, 18: 59
21 Preuss M, de Fonseca J Q, Grant B, et al. The effect of γ' particle size on the deformation mechanism in an advanced polycrystalline nickel-base superalloy [A]. Superalloys 2008 [C]. Pittsburgh, PA: The Minerals, Metals, & Materials Society, 2008: 405
22 Xie B C, Ning Y Q, Zhou C. Deformation behavior and microstructure evolution of two typical structures in Udimet 720Li ingot [J]. Proc. Eng., 2017, 207: 1093
23 Wang T, Wan Z P, Li Z, et al. Effect of heat treatment parameters on microstructure and hot workability of as-cast fine grain ingot of GH4720Li alloy [J]. Acta Metall. Sin., 2020, 56: 182
23 王 涛, 万志鹏, 李 钊等. 热处理工艺对GH4720Li合金细晶铸锭组织与热加工性能的影响 [J]. 金属学报, 2020, 56: 182
24 Hyzak J M, Singh R P, Morra J, et al. The microstructural response of as-hip P/M U-720 to thermomechanical processing [A]. Superalloys 1992 [C]. Pittsburgh, PA: The Minerals, Metals, & Materials Society, 1992: 93
25 Monajati H, Zarandi F, Jahazi M, et al. Strain induced γ' precipitation in nickel base superalloy Udimet 720 using a stress relaxation based technique [J]. Scr. Mater., 2005, 52: 771
26 Pang H T, Hardy M C, Hide N, et al. Comparison of fatigue crack propagation in nickel base superalloys RR1000 and Udimet 720Li [J]. Mater. Sci. Technol., 2016, 32: 22
27 Wang X Q, Peng Z C, Zhang M C. Hot deformation behavior of AA-FGH720Li superalloy [J]. Mater. Sci. Forum, 2017, 898: 528
28 Bozzolo N, Soua? N, Logé R E. Evolution of microstructure and twin density during thermomechanical processing in a γ-γ' nickel-based superalloy [J]. Acta Mater., 2012, 60: 5056
29 Yu Q Y, Yao Z H, Dong J X. Deformation and recrystallization behavior of a coarse-grain, nickel-base superalloy Udimet720Li ingot material [J]. Mater. Charact., 2015, 107: 398
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