研究论文

搅拌头转速对2507双相不锈钢搅拌摩擦加工组织及性能的影响

  • 陈果 ,
  • 王新波 ,
  • 张仁晓 ,
  • 马成悦 ,
  • 杨海峰 ,
  • 周利 ,
  • 赵运强
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  • 1.哈尔滨工业大学 先进焊接与连接国家重点实验室 哈尔滨 150001
    2.哈尔滨工业大学(威海) 山东省特种焊接技术重点实验室 威海 264209
    3.广东省科学院中乌焊接研究所 广东省现代焊接技术重点实验室 广州 510651
陈 果,男,1996年生,硕士生

收稿日期: 2020-07-06

  修回日期: 2020-09-10

  网络出版日期: 2020-11-04

基金资助

山东省重大科技创新工程项目(2017CXGC0811);广州市科技计划项目(201704030038)

Effect of Tool Rotation Speed on Microstructure and Properties of Friction Stir Processed 2507 Duplex Stainless Steel

  • Guo CHEN ,
  • Xinbo WANG ,
  • Renxiao ZHANG ,
  • Chengyue MA ,
  • Haifeng YANG ,
  • Li ZHOU ,
  • Yunqiang ZHAO
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  • 1.State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin 150001, China
    2.Shandong Provincial Key Laboratory of Special Welding Technology, Harbin Institute of Technology at Weihai, Weihai 264209, China
    3.Guangdong Provincial Key Laboratory of Advanced Welding Technology, China-Ukraine Institute of Welding, Guangdong Academy of Sciences, Guangzhou 510651, China
ZHOU Li, professor, Tel: (0631)5687196, E-mail: zhou.li@hit.edu.cn

Received date: 2020-07-06

  Revised date: 2020-09-10

  Online published: 2020-11-04

Supported by

Key Research and Development Program in Shandong Province(2017CXGC0811);Science and Technology Plan Project of Guangzhou City(201704030038)

摘要

通过对5 mm厚2507双相不锈钢进行搅拌摩擦加工,研究了在加工速率为100 mm/min时搅拌头转速对加工区域组织、力学性能和腐蚀性能的影响。结果表明,随着搅拌头转速的增大,搅拌区晶粒尺寸呈现先减小后增大的趋势。加工热循环和应力变形对加工区铁素体与奥氏体组织比例的变化影响不大,其铁素体含量仍保持在标准规范40%~60%之间。仅在搅拌头转速为200 r/min时,在加工区底部发现σ相析出。加工区显微硬度分布呈现“盆状”,其硬度最高值出现在搅拌区前进侧的底部,对应搅拌区晶粒尺寸最细小处。随着搅拌头转速的增加,搅拌区纵向拉伸强度呈现先增大后减小的趋势,而塑性则呈现先减小后增大的趋势。搅拌头转速为400 r/min时,搅拌区具有最优腐蚀性能。

本文引用格式

陈果 , 王新波 , 张仁晓 , 马成悦 , 杨海峰 , 周利 , 赵运强 . 搅拌头转速对2507双相不锈钢搅拌摩擦加工组织及性能的影响[J]. 金属学报, 2021 , 57(6) : 725 -735 . DOI: 10.11900/0412.1961.2020.00239

Abstract

Duplex stainless steel with its exceptional corrosion resistance, mechanical properties, and proficient weldability has been widely used in ships and bridges, as well as petrochemical and seawater desalination industries. Friction stir processing (FSP) does not only induce dynamic recrystallization of the material but also achieves the purpose of repairing the crack automatically, which markedly improves the mechanical properties of duplex stainless steel. Thus, FSP is particularly useful for crack repair of duplex stainless steel structures. In the present study, microstructure, mechanical property, and corrosion property of FSP 2507 duplex stainless steel were investigated. FSP was performed at a constant welding speed of 100 mm/min and tool rotation speeds of 200, 300, 400, 500, and 600 r/min using a tungsten-rhenium-based tool. Due to the thermal and mechanical effects in the processing, the section of the processing zone can be divided into the thermo-mechanically affected zone (TMAZ) and the stir zone (SZ). Only under the sufficient parameters of thermoplastic flow, the internal faultless processing zone was obtained. In accordance with the increased tool rotating speed, the grain size of the SZ initially decreased and then increased. Processing heat cycle and stress deformation had an insignificant influence on the proportion of ferrite and austenite phases in the processing zone, and the ferrite content still remained between 40% and 60% in the standard specification. The σ phase was determined at the bottom of the processing zone, namely at the tool rotation speed of 200 r/min due to the low heat input. Microhardness distribution of the processing zone demonstrated a basin-like morphology, and the largest hardness value appeared at the bottom of the advanced side of the SZ, corresponding to the smallest grain size of the SZ. As the tool rotating speed increased, the longitudinal tensile strength of the SZ increased initially and then decreased, contrary to the elongation. According to the results of potentiometric polarization and electrochemical impedance spectroscopy, the refinement of grain enhanced the stability, compactness, and repassivation performance of surface passivation film. The corrosion resistance of the upper surface in the SZ exceeded that of the base material, rendering it more useful. When the tool rotation speed was 400 r/min, the SZ had the optimal corrosion properties.

参考文献

1 Verma J, Taiwade R V. Effect of welding processes and conditions on the microstructure, mechanical properties and corrosion resistance of duplex stainless steel weldments—A review [J]. J. Manuf. Proc., 2017, 25: 134
2 Sathiya P, Aravindan S, Soundararajan R, et al. Effect of shielding gases on mechanical and metallurgical properties of duplex stainless-steel welds [J]. J. Mater. Sci., 2009, 44: 114
3 Deng B, Jiang Y M, Gong J, et al. Critical pitting and repassivation temperatures for duplex stainless steel in chloride solutions [J]. Electrochim. Acta, 2008, 53: 5220
4 Tavares S S M, Silva V G, Pardal J M, et al. Investigation of stress corrosion cracks in a UNS S32750 superduplex stainless steel [J]. Eng. Fail. Anal., 2013, 35: 88
5 Ma Z Y. Friction stir processing technology: A review [J]. Metall. Mater. Trans., 2008, 39A: 642
6 Ji S D, Huang R F, Wu B S. Review on friction stir welding repair [J]. J. Shenyang Aero. Univ., 2017, 34(5): 1
6 姬书得, 黄若飞, 吴宝生. 搅拌摩擦焊修复技术的研究现状 [J]. 沈阳航空航天大学学报, 2017, 34(5): 1
7 Chen W L. The precipitation behavior of the σ phase and its effect on performance in 2707 duplex stainless steel [D]. Taiyuan: Taiyuan University of Technology, 2018
7 陈万里. 2707双相不锈钢中σ相析出行为及其对性能的影响 [D]. 太原: 太原理工大学, 2018
8 Liu X L. Study on the microstructure and properties of friction stir welded hyper stainless steel SAF2707 joint [D]. Taiyuan: Taiyuan University of Technology, 2017
8 刘兴龙. 特超级双相不锈钢SAF2707搅拌摩擦焊接头显微组织和性能研究 [D]. 太原: 太原理工大学, 2017
9 Esmailzadeh M, Shamanian M, Kermanpur A, et al. Microstructure and mechanical properties of friction stir welded lean duplex stainless steel [J]. Mater. Sci. Eng., 2013, A561: 486
10 Santos T F D A, Torres E A, Ramirez A J. Friction stir welding of duplex stainless steels [J]. Weld. Int., 2017, 32: 103
11 Mishra M K, Gunasekaran G, Rao A G, et al. Effect of multipass friction stir processing on mechanical and corrosion behavior of 2507 super duplex stainless steel [J]. J. Mater. Eng. Perform., 2017, 26: 849
12 Magnani M, Terada M, Lino A O, et al. Microstructural and electrochemical characterization of friction stir welded duplex stainless steels [J]. Int. J. Electrochem. Sci., 2014, 9: 2966
13 Li G H, Zhou L, Luo S F, et al. Microstructure and mechanical properties of self-reacting friction stir welded AA2219-T87 aluminium alloy [J]. Sci. Technol. Weld. Join., 2019, 25: 142
14 Sato Y S, Kokawa H, Ikeda K, et al. Microtexture in the friction-stir weld of an aluminum alloy [J]. Metall. Mater. Trans., 2001, 32A: 941
15 Saeid T, Abdollah-Zadeh A, Assadi H, et al. Effect of friction stir welding speed on the microstructure and mechanical properties of a duplex stainless steel [J]. Mater. Sci. Eng., 2008, A496: 262
16 Santos T F D A, López E A T, Da Fonseca E B, et al. Friction stir welding of duplex and superduplex stainless steels and some aspects of microstructural characterization and mechanical performance [J]. Mater. Res., 2016, 19: 117
17 Ma M. Hot deformation behavior and microstructural evolution of duplex stainless steels [D]. Shenyang: Northeastern University, 2016
17 马 明. 双相不锈钢热变形行为及组织演变 [D]. 沈阳: 东北大学, 2016
18 Zhang Z Y, Zhang H Z, Hu J, et al. Microstructure evolution and mechanical properties of briefly heat-treated SAF 2507 super duplex stainless steel welds [J]. Constr. Build. Mater., 2018, 168: 338
19 Giorj?o R A R, Pereira V F, Terada M, et al. Microstructure and mechanical properties of friction stir welded 8 mm pipe SAF 2507 super duplex stainless steel [J]. J. Mater. Res. Technol., 2018, 340: 1
20 Santos T F A, Marinho R R, Paes M T P, et al. Microstructure evaluation of UNS S32205 duplex stainless steel friction stir welds [J]. Rem Rev. Esc. Minas., 2013, 66: 187
21 Sato Y S, Nelson T W, Sterling C J, et al. Microstructure and mechanical properties of friction stir welded SAF 2507 super duplex stainless steel [J]. Mater. Sci. Eng., 2005, A397: 376
22 Steel R J, Sterling C J. Friction stir welding of 2205 duplex stainless and 3Cr12 steels [A]. The Fourteenth International Offshore and Polar Engineering Conference [C]. California: International Society of Offshore and Polar Engineers, 2004: 67
23 Ralston K D, Birbilis N, Davies C H J. Revealing the relationship between grain size and corrosion rate of metals [J]. Scr. Mater., 2010, 63: 1201
24 Atapour M, Sarlak H, Esmailzadeh M. Pitting corrosion susceptibility of friction stir welded lean duplex stainless steel joints [J]. Int. J. Adv. Manuf. Technol., 2016, 83: 721
25 Sarlak H, Atapour M, Esmailzadeh M. Corrosion behavior of friction stir welded lean duplex stainless steel [J]. Mater. Des., 2015, 66: 209
26 Wang X Y, Li D Y. Mechanical and electrochemical behavior of nanocrystalline surface of 304 stainless steel [J]. Electrochim. Acta, 2002, 47: 3939
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