分层厚度对选区激光熔化成形Ti-5Al-2.5Sn合金组织与性能的影响规律

  • 高飘 ,
  • 魏恺文 ,
  • 喻寒琛 ,
  • 杨晶晶 ,
  • 王泽敏 ,
  • 曾晓雁
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  • 华中科技大学武汉光电国家实验室 武汉 430074

作者简介 高 飘,女,1994年生,博士生

收稿日期: 2017-09-13

  网络出版日期: 2018-01-02

基金资助

国家重点基础研究发展计划项目No.613281,中央高校基本科研业务费项目No.2016XYZD005,国防科工局技术基础科研项目No.JSCG2016204B001,以及民用航天预研项目《液体火箭发动机核心构件增材制造技术研究》

Influence of Layer Thickness on Microstructure and Mechanical Properties of Selective Laser Melted Ti-5Al-2.5Sn Alloy

  • Piao GAO ,
  • Kaiwen WEI ,
  • Hanchen YU ,
  • Jingjing YANG ,
  • Zemin WANG ,
  • Xiaoyan ZENG
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  • Wuhan National Laboratory for Optoelectronics, Huazhong University of Science and Technology, Wuhan 430074, China

Received date: 2017-09-13

  Online published: 2018-01-02

Supported by

Supported by National Basic Research Program of China (No.613281), Fundamental Research Funds for the Central Universities (No.2016XYZD005) and Technical Basis Project of State Administration of Science and Technology and Industry for National Defense (No.JSCG2016204B001)

摘要

研究了分层厚度对选区激光熔化(SLM)技术成形Ti-5Al-2.5Sn (TA7)钛合金试样致密度、显微组织和力学性能的影响规律。结果表明:在激光功率和扫描间距一定的条件下,当分层厚度≤40 μm时,致密度随激光体能量密度的下降不断提高;当分层厚度>40 μm时,致密度则随激光体能量密度的下降先升高后降低。随分层厚度的增大和扫描速率的降低,SLM成形过程中的冷却速率逐步下降,当冷却速率低于6.8×107 K/s时,显微组织由针状马氏体α′逐渐向岛状αm转变。通过优化工艺参数,在所有分层厚度(20~60 μm)下均能成形致密的TA7试样,其显微硬度、屈服强度和断裂强度超越铸件和锻件;且当分层厚度≤40 μm时,韧塑性超越铸件,达到锻件水平。成功探索出能够兼顾TA7样品成形效率、冶金质量及力学性能的优选分层厚度及SLM工艺参数组合。

本文引用格式

高飘 , 魏恺文 , 喻寒琛 , 杨晶晶 , 王泽敏 , 曾晓雁 . 分层厚度对选区激光熔化成形Ti-5Al-2.5Sn合金组织与性能的影响规律[J]. 金属学报, 2018 , 54(7) : 999 -1009 . DOI: 10.11900/0412.1961.2017.00384

Abstract

As an additive manufacturing technology, selective laser melting (SLM) process can solve the manufacturing difficulty of Ti-5Al-2.5Sn (TA7) easily. But the low building efficiency of SLM retards its wide applications in aviation, petrochemical and other fields. In order to solve the above problem, the influence of layer thickness on relative density, microstructure and mechanical properties of SLMed TA7 samples were studied in this work. The results show that when the laser power and hatching space are constant, the relative density gradually increases with the decrease of the laser volume energy density under the layer thicknesses less than or equal to 40 μm, whereas first increases and then declines with the decrease of the laser volume energy density under the layer thicknesses larger than 40 μm. At the same time, with the increase of layer thickness and the decrease of scanning velocity, the cooling rate gradually decreases during the SLM processing, when the cooling rate is lower than 6.8×107 K/s, the microstructure will gradually transform from acicular martensite α' to massive αm. Through the optimization of SLM parameters, the dense TA7 bulk specimens with higher microhardnesses, yield strengths and ultimate strengths in comparison to the as-cast and deformed TA7 alloys can be obtained under all layer thicknesses (20~60 μm). While when the layer thicknesses are not larger than 40 μm, the ductility of the SLMed TA7 is also superior to that of the as-cast TA7 and comparable to that of the deformed TA7. Finally, the optimal layer thickness and combination of SLM process parameters are successfully determined to balance the building efficiency, metallurgical quality and mechanical properties of the TA7 alloy parts.

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